Milk-based infant foods - Determination of fat content - Gravimetric method (Reference method) (ISO 8381:2008)

ISO 8381¦IDF 123:2008 specifies the reference method for the determination of the fat content of milk-based infant foods.
The method is applicable to liquid, concentrated and dried milk-based infant foods with no, or not more than a mass fraction of 5 % (dry matter) of such added matter as starch, dextrin, vegetables, fruit and meat.
The method is not applicable to products which do not dissolve completely in ammonia owing to the presence of starch or dextrin at mass fractions of more than a few percent, or to the presence of hard lumps. The method is also not applicable to products which contain free fatty acids in significant quantities. The results obtained for these products will be too low.

Säuglingsnahrung auf Milchbasis - Bestimmung des Fettgehaltes - Gravimetrisches Verfahren (Referenzverfahren) (ISO 8381:2008)

Diese Internationale Norm legt das Referenzverfahren für die Bestimmung des Fettgehaltes von Säuglings-nahrung auf Milchbasis fest.
Das Verfahren gilt für flüssige, konzentrierte und getrocknete Säuglingsnahrung auf Milchbasis, die keine oder höchstens einen Massenanteil von 5 % (in der Trockenmasse) an Zusätzen wie Stärke, Dextrin, Gemüse, Früchte und Fleisch enthält.
ANMERKUNG 1   In Säuglingsnahrung häufig vorhandene Maltosedextrine, die keine Dextrine hoher molarer Masse enthalten, wirken sich nicht nachteilig auf die Röse-Gottlieb-Extraktion aus, selbst wenn diese in hoher Konzentration vorhanden sind.
Das Verfahren gilt nicht für Produkte, die Stärke oder Dextrin an Massenanteilen von mehr als nur wenige Prozent enthalten oder zur Bildung harter Klumpen neigen und sich deshalb nicht vollständig in Ammoniak lösen. Das Verfahren gilt ebenso nicht für Produkte, die freie Fettsäuren in signifikanten Mengen enthalten. Bei diesen Produkten fallen die Untersuchungsergebnisse zu niedrig aus.
ANMERKUNG 2   Bei derartigen Produkten ist ein Verfahren geeignet, das nach dem Weibull-Berntrop-Prinzip arbeitet
(siehe ISO 8262-1|IDF 124-1 [3]).

Aliments à base de lait pour enfants en bas âge - Détermination de la teneur en matière grasse - Méthode gravimétrique (Méthode de référence) (ISO 8381:2008)

L'ISO 8381|FIL 123:2008 spécifie la méthode de référence pour la détermination de la teneur en matière grasse des aliments à base de lait pour enfants en bas âge.
Cette méthode est applicable aux aliments à base de lait liquides, concentrés et séchés pour enfants en bas âge, ne contenant pas ou pas plus qu'une fraction massique de 5 % (de la matière sèche) d'amidon, de dextrines, de légumes, de fruits, de viandes, etc.
La méthode n'est applicable ni aux produits qui ne se dissolvent pas complètement dans l'ammoniaque, du fait de la présence d'amidon ou de dextrines à des fractions massiques supérieures à quelques pour cent, ou encore de la présence de grumeaux compacts, ni aux produits qui contiennent des acides gras libres en quantité significative; le résultat de la détermination sera trop faible.

Hrana za majhne otroke na osnovi mleka - Določevanje maščob - Gravimetrijska metoda (Referenčna metoda) (ISO 8381:2008)

General Information

Status
Published
Publication Date
14-Oct-2008
Withdrawal Date
29-Apr-2009
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
15-Oct-2008
Due Date
18-Oct-2009
Completion Date
15-Oct-2008

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SLOVENSKI STANDARD
01-februar-2009
1DGRPHãþD
SIST EN ISO 8381:2001
+UDQD]DPDMKQHRWURNHQDRVQRYLPOHND'RORþHYDQMHPDãþRE*UDYLPHWULMVND
PHWRGD 5HIHUHQþQDPHWRGD  ,62
Milk-based infant foods - Determination of fat content - Gravimetric method (Reference
method) (ISO 8381:2008)
Säuglingsnahrung auf Milchbasis - Bestimmung des Fettgehaltes - Gravimetrisches
Verfahren (Referenzverfahren) (ISO 8381:2008)
Aliments à base de lait pour enfants en bas âge - Détermination de la teneur en matière
grasse - Méthode gravimétrique (Méthode de référence) (ISO 8381:2008)
Ta slovenski standard je istoveten z: EN ISO 8381:2008
ICS:
67.100.99 'UXJLPOHþQLSURL]YRGL Other milk products
67.230 Predpakirana in pripravljena Prepackaged and prepared
hrana foods
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN ISO 8381
NORME EUROPÉENNE
EUROPÄISCHE NORM
October 2008
ICS 67.230 Supersedes EN ISO 8381:2000
English Version
Milk-based infant foods - Determination of fat content -
Gravimetric method (Reference method) (ISO 8381:2008)
Aliments à base de lait pour enfants en bas âge - Säuglingsnahrung auf Milchbasis - Bestimmung des
Détermination de la teneur en matière grasse - Méthode Fettgehaltes - Gravimetrisches Verfahren
gravimétrique (Méthode de référence) (ISO 8381:2008) (Referenzverfahren) (ISO 8381:2008)
This European Standard was approved by CEN on 14 October 2008.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2008 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 8381:2008: E
worldwide for CEN national Members.

Contents Page
Foreword.3

Foreword
This document (EN ISO 8381:2008) has been prepared by Technical Committee ISO/TC 34 "Agricultural food
products" in collaboration with Technical Committee CEN/TC 302 “Milk and milk products - Methods of
sampling and analysis” the secretariat of which is held by NEN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by April 2009, and conflicting national standards shall be withdrawn at the
latest by April 2009.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 8381:2000.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 8381:2008 has been approved by CEN as a EN ISO 8381:2008 without any modification.

INTERNATIONAL ISO
STANDARD 8381
IDF
Third edition
2008-10-15
Milk-based infant foods — Determination
of fat content — Gravimetric method
(Reference method)
Aliments à base de lait pour enfants en bas âge — Détermination de la
teneur en matière grasse — Méthode gravimétrique (Méthode de
référence)
Reference numbers
ISO 8381:2008(E)
IDF 123:2008(E)
©
ISO and IDF 2008
ISO 8381:2008(E)
IDF 123:2008(E)
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All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO or IDF at the respective
address below.
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Published in Switzerland
ii © ISO and IDF 2008 – All rights reserved

ISO 8381:2008(E)
IDF 123:2008(E)
Contents Page
Foreword. iv
Foreword. v
1 Scope .1
2 Normative references .1
3 Terms and definitions .1
4 Principle.2
5 Reagents.2
6 Apparatus .2
7 Sampling.3
8 Preparation of test sample.4
8.1 Liquid products.4
8.2 Viscous or pasty products.4
8.3 Dried products .4
9 Procedure .4
9.1 Test portion .4
9.2 Blank tests.5
9.3 Preparation of fat-collecting vessel.5
9.4 Determination.5
10 Calculation and expression of results.8
10.1 Calculation.8
10.2 Expression of results .8
11 Precision.8
11.1 Interlaboratory test .8
11.2 Repeatability.8
11.3 Reproducibility.9
12 Test report .9
Annex A (informative) Notes on procedures .10
Annex B (informative) Alternative procedure using fat-extraction tubes with siphon or wash-bottle
fittings .12
Bibliography .15
ISO 8381:2008(E)
IDF 123:2008(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee has
been established has the right to be represented on that committee. International organizations, governmental
and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 8381⎪IDF 123 was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee SC 5,
Milk and milk products, and the International Dairy Federation (IDF). It is being published jointly by ISO and
IDF.
This third edition of ISO 8381⎪IDF 123 cancels and replaces the second edition (ISO 8381:2000), of which it
constitutes a minor revision.
iv © ISO and IDF 2008 – All rights reserved

ISO 8381:2008(E)
IDF 123:2008(E)
Foreword
IDF (the International Dairy Federation) is a non-profit organization representing the dairy sector worldwide.
IDF membership comprises National Committees in every member country as well as regional dairy
associations having signed a formal agreement on cooperation with IDF. All members of IDF have the right to
be represented at the IDF Standing Committees carrying out the technical work. IDF collaborates with ISO in
the development of standard methods of analysis and sampling for milk and milk products.
Draft International Standards adopted by the Action Teams and Standing Committees are circulated to the
National Committees for voting. Publication as an International Standard requires approval by at least 50 % of
the IDF National Committees casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. IDF shall not be held responsible for identifying any or all such patent rights.
ISO 8381⎪IDF 123 was prepared by the International Dairy Federation (IDF) and Technical Committee
ISO/TC 34, Food products, Subcommittee SC
...

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