Standard Test Method for Evaluating Pipeline Coating Patch Materials (Withdrawn 2007)

SCOPE
1.1 This test method provides an accelerated means of determining the relative sealing abilities of pipeline patching materials that are used to seal holidays in pipeline coatings on steel pipe. This test method is intended for utilization of specimens of pipeline coatings on small-diameter pipe, for representing coatings used for buried or submerged service, and where the purpose of the coating is to provide an electrical barrier between the steel pipe and its environment.  
1.2 This test method is not intended for evaluating patch materials that are overlapped upon themselves.
1.3 The values stated in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method provides an accelerated means of determining the relative sealing abilities of pipeline patching materials that are used to seal holidays in pipeline coatings on steel pipe. This test method is intended for utilization of specimens of pipeline coatings on small-diameter pipe, for representing coatings used for buried or submerged service, and where the purpose of the coating is to provide an electrical barrier between the steel pipe and its environment.
Formerly under the jurisdiction of Committee D01 on Paint and Related Coatings, Materials, and Applications, this test method was withdrawn in March 2007 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

General Information

Status
Historical
Publication Date
09-Jul-1998
Withdrawal Date
20-Mar-2007
Current Stage
Ref Project

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ASTM G55-88(1998) - Standard Test Method for Evaluating Pipeline Coating Patch Materials (Withdrawn 2007)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:G55–88 (Reapproved 1998)
Standard Test Method for
Evaluating Pipeline Coating Patch Materials
ThisstandardisissuedunderthefixeddesignationG55;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope materials. The user is cautioned against the use of this method
for absolute material properties characterization.
1.1 This test method provides an accelerated means of
3.3 This procedure provides an accelerated method by
determining the relative sealing abilities of pipeline patching
exposing the patch to a severe radius of curvature on small-
materials that are used to seal holidays in pipeline coatings on
diameterpipe.Thespecimenisalsoexposedtoastressvoltage
steel pipe. This test method is intended for utilization of
in the presence of a highly conductive electrolyte.
specimens of pipeline coatings on small-diameter pipe, for
representing coatings used for buried or submerged service,
4. Apparatus
and where the purpose of the coating is to provide an electrical
4.1 Test Vessel—A cylindrical glass battery jar (or equiva-
barrier between the steel pipe and its environment.
lent), approximately 300 mm (12 in.) in diameter and 300 mm
1.2 This test method is not intended for evaluating patch
in height. One magnesium anode shall be contained in each
materials that are overlapped upon themselves.
battery jar, with a maximum of eight pipe specimens, and with
1.3 The values stated in SI units are to be regarded as the
each specimen measuring about 25 mm (1 in.) in diameter by
standard.The values given in parenthes are for information
approximately 300 mm in length of coated pipe. (See 4.3 and
only.
Fig. 1 and Fig. 2.)
1.4 This standard does not purport to address all of the
4.2 Suspension—The suspension ring for supporting the
safety concerns, if any, associated with its use. It is the
pipe specimens shall be an electrically nonconductive circular
responsibility of the user of this standard to establish appro-
disk, measuring approximately 300 mm (12 in.) in diameter
priate safety and health practices and determine the applica-
and approximately 5 mm ( ⁄16 in.) in thickness. (See 6.4.) Drill
bility of regulatory limitations prior to use.
a 15-mm ( ⁄2-in.) diameter hole through the center of the ring
2. Summary of Test Method for external extension of the anode lead wire. Drill eight
suspension holes, about 45 mm (1 ⁄4 in.) in diameter, through
2.1 Patched pipeline coating specimens are suspended in an
thesuspensionringforthepipespecimens;theseholesshallbe
aqueous, alkaline, low-resistivity electrolyte. The specimens
centered 110 mm (4 ⁄2 in.) from the center of the suspension
areindividuallyconnectedtoamagnesiumanodeorrectifierat
ring and evenly spaced around the ring at 45° increments as
apointexternaltotheelectrolyte.Thecoated,patchedpipeline
measured from the center of the suspension ring.
specimens are sealed at the base and at all other areas except
4.3 Potential—A high-purity magnesium anode shall be
the patch boundaries, such that the only paths for current flow
used, weighing approximately 2.3 kg (5 lb), and having an
areattheboundariesofthepatches.Currentflowineachpatch
open-circuit potential of approximately 1.7 d-c V relative to a
area is averaged from monthly readings taken for one year.
copper-copper sulfate electrode, and complete with a factory-
3. Significance and Use
sealed lead wire. The magnesium anode may be replaced by a
controlledd-cvoltagefromarectifier,andthenmaintainingthe
3.1 Holidays in pipeline coatings may be repaired by
potential between the specimen having the least current flow
circumferential wrapping with a suitable pipe wrap tape.
and a copper-copper sulfate reference cell (with the cell being
However,thistechniqueisnotalwayspracticableandpatching
properlyimmersedintheelectrolyte)at1.5060.05d-cV.(See
mayberequired.Theeffectivenessofapatchmaterialdepends
Note 1.) The anode should be composed of a suitable noncon-
upon its adhesion to the original pipeline coating to effect
sumable material. This option will avoid the precipitation of
sealing.
magnesium salts on the specimens.
3.2 The results of this accelerated test have been found to
yield comparative data useful for the selection of patching
The sole source of supply of a nonconconsumable anode, Durachlor 51 anode,
This test method is under the jurisdiction of ASTM Committee D-1 on Paint Type B, 18-in. with cable, known to the committee at this time is Duriron Co., P.O.
and Related Coatings, Materials, andApplications,and is the direct responsibility of Box 1145, Dayton, OH 45401. If you are aware of alternative suppliers, please
Subcommittee D01.48on Deterioration of Pipeline Coatings and Linings. provide this information to ASTM Headquarters. Your comments will receive
Current edition approved May 27, 1988. Published July 1988. Originally careful consideration at a meeting of the responsible technical committee, which
published as G55–77. Last previous edition G55–83. you may attend.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
G55
5.2 Circuit Tap—A 5-mm ( ⁄16-in.) diameter hole shall be
drilled or tapped (or a self-tapping screw may be used) at a
point 13 mm ( ⁄2 in.) below the top of each specimen. This tap
is for a machine screw anode lead wire connection.
5.3 Pipe Suspension Support Holes—A 6-mm ( ⁄4-in.) di-
ameter hole shall be drilled completely through both walls of
thecoatedpipespecimenatapoint20mm( ⁄4in.)fromthetop
end of the specimen and located vertically beneath the circuit
tap hole.Ashort length of wooden dowel pin about 5 mm ( ⁄16
in.) in diameter shall be used as an insertion through the
suspension holes to support and level the pipe specimen on the
circular suspension ring when the suspension ring is mounted
on the battery jar.
5.4 Intentional Holidays—A 4-fluted 13-mm ( ⁄2-in.) diam-
eterfacingbitshallbeusedtodrillintentionalholidaysthrough
the original pipeline coating to the metal. Drilling such
holidays shall be practiced on scrap pieces of small-diameter
coatedpipe,priortodrillingtheholidaysinthetestspecimens.
Drilling shall not be any deeper than necessary into the metal
ofthepipe.Threeholidaysshallbepreparedoneachspecimen
in a vertical line directly underneath the circuit tap to corre-
spond to electrolyte immersions of 38 mm (1 ⁄2 in.), 114 mm
1 1
(4 ⁄2in.),and190mm(7 ⁄2in.),asmeasuredfromthetopofthe
holiday to the surface of the electrolyte. The thickness of the
suspension ring shall be considered for its effect in elevating
the pipe specimens in the electrolyte.
5.5 Patches—Asquare patch configuration of 25 by 25 mm
(1 by 1 in.), evenly centered about the holiday, shall be lightly
FIG. 1 Test Assembly for Evaluating Pipeline Coating Patch
marked. This will provide a minimum patch overlap of 6 mm
Materials
( ⁄4 in.) as measured perpendicular to the center of each patch
edge to the circumference of the holiday. The top and bottom
NOTE 1—The potential of the magnesium anode will approximate this
edges of each patch shall be in the horizontal plane. Each
range over the life of the test. If a calomel electrode is used for the
marked patch area shall be lightly buffed with 120-grit sand-
reference cell, the potential should be−1.43 6 0.05 d-c V.
paper. A primer shall be applied using clean cotton on a stick
4.4 Electrolyte—Use1%eachbyweightofanhydrouspure
to extend the primer to the edges of the marked patch area
gradesofsodiumchloride,sodiumsulfate,andsodiumcarbon-
when specified by the manufacturer of the patch. The manu-
ate, dissolved in either distilled water or demineralized water.
facturers’specifieddryingtimeshallbeusedforprimersbefore
ThiselectrolyteshallneverbelessalkalinethanpH 510.0and
applicationofthepatch.Scissorsoraknifeshallbeusedtocut
should be within a resistivity range from 20 to 35 V · cm.
tape p
...

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