Standard Practice for Liquid Sampling of Noncryogenic Aerospace Propellants

ABSTRACT
This practice covers procedures for obtaining a sample of noncryogenic aerospace propellant. Two procedures are covered as follows: procedure 1 (closed system) and procedure 2 (open-end procedure).
SCOPE
1.1 This practice covers procedures for obtaining a sample of noncryogenic aerospace propellant. Two procedures are covered as follows:
Procedure 1—Closed System (Section 6), and
Procedure 2—Open-End Procedure (Section 7).  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For hazard statements see Sections 4 and 5.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
31-Aug-2018
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: F309 − 04 (Reapproved 2018)
Standard Practice for
Liquid Sampling of Noncryogenic Aerospace Propellants
ThisstandardisissuedunderthefixeddesignationF309;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4.1.1 Caution—Pressure sampling cylinders must be
marked for the liquid being sampled. Cylinders for one
1.1 This practice covers procedures for obtaining a sample
material must not be interchanged with sampling cylinders of
of noncryogenic aerospace propellant. Two procedures are
other materials because of the possibility of incompatibility.
covered as follows:
Procedure 1—Closed System (Section 6), and 4.2 Full Protective Suits.
Procedure 2—Open-End Procedure (Section 7). 4.2.1 Caution—Due to the toxic and corrosive nature of
most propellent fluids and their vapors, extreme care must be
1.2 This standard does not purport to address all of the
exercised in handling. Full protective suits must be worn when
safety concerns, if any, associated with its use. It is the
sampling these fluids.
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
4.3 Polyethylene Wash Bottle, 1-L capacity, filled with
mine the applicability of regulatory limitations prior to use.
demineralized water, filtered in the manner described in Prac-
For hazard statements see Sections 4 and 5.
tice F311.
1.3 This international standard was developed in accor-
4.4 Stainless Steel Bucket.
dance with internationally recognized principles on standard-
4.5 Miscellaneous Fittings, as needed for sample point
ization established in the Decision on Principles for the
adaption.
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
5. Hazards
Barriers to Trade (TBT) Committee.
5.1 Care should be taken when handling propellants since
2. Referenced Documents
most of them are toxic to some degree. Care should also be
taken when sampling fluids from a system under dynamic
2.1 ASTM Standards:
conditions.
F311 Practice for Processing Aerospace Liquid Samples for
Particulate Contamination Analysis Using Membrane Fil-
PROCEDURE 1—CLOSED SYSTEM
ters
6. Procedure
3. Summary of Practice
6.1 Samplingcylindersmustbeclean,particulate-controlled
3.1 Samples are withdrawn from the system by (1) a closed
in accordance with system requirements, and have a partial
vessel capture, and (2) an open-end vessel (see Fig. 1). Both
vacuum of 10 % of atmospheric pressure.
procedures are practical for most liquid aerospace propellants
6.2 Afterremovingprotectivecaps,connectbothendsofthe
not excessively corrosive or toxic.
sampling cylinder to the system sampling ports, using fittings
4. Apparatus
as necessary.
4.1 Stainless Steel Pressure Sampling Cylinders, 1-L
6.3 Open both sampling valves and both sampling cylinder
capacity, equipped with stainless steel valves on each end.
valves, and allow fluid to flow through the sampling cylinder
for 10 min.
This practice is under the jurisdiction of ASTM Committee E21 on Space 6.4 Close all four valves downstream side first, and remove
Simulation andApplications of Space Technology and is the direct respon
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: F309 − 04 (Reapproved 2010) F309 − 04 (Reapproved 2018)
Standard Practice for
Liquid Sampling of Noncryogenic Aerospace Propellants
This standard is issued under the fixed designation F309; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers procedures for obtaining a sample of noncryogenic aerospace propellant. Two procedures are covered
as follows:
Procedure 1—1Closed—Closed System (Section 6), and
Procedure 2—Open-End Procedure (Section 7).
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. For hazard statements see Sections 4 and 5.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
F311 Practice for Processing Aerospace Liquid Samples for Particulate Contamination Analysis Using Membrane Filters
3. Summary of Practice
3.1 Samples are withdrawn from the system by (1) a closed vessel capture, and (2) an open-end vessel (see Fig. 1). Both
procedures are practical for most liquid aerospace propellants not excessively corrosive or toxic.
4. Apparatus
4.1 Stainless Steel Pressure Sampling Cylinders, 1-L capacity, equipped with stainless steel valves on each end.
4.1.1 Caution—Pressure sampling cylinders must be marked for the liquid being sampled. Cylinders for one material must not
be interchanged with sampling cylinders of other materials because of the possibility of incompatibility.
4.2 Full Protective Suits.
4.2.1 Caution—Due to the toxic and corrosive nature of most propellent fluids and their vapors, extreme care must be exercised
in handling. Full protective suits must be worn when sampling these fluids.
4.3 Polyethylene Wash Bottle, 1-L capacity, filled with demineralized water, filtered in the manner described in Practice F311.
4.4 Stainless Steel Bucket.
4.5 Miscellaneous Fittings, as needed for sample point adaption.
5. Hazards
5.1 Care should be taken when handling propellants since most of them are toxic to some degree. Care should also be taken
when sampling fluids from a system under dynamic conditions.
This practice is under the jurisdiction of ASTM Committee E21 on Space Simulation and Applications of Space Technology and is the direct responsibility of
Subcommittee E21.05 on Contamination.
Current edition approved April 1, 2010Sept. 1, 2018. Published May 2010September 2018. Originally approved in 1966. Last previous edition approved in 20042010 as
F309 – 04.F309 – 04 (2010). DOI: 10.1520/F0309-04R10.10.1520/F0309-04R18.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of
...

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