ASTM D5248-04(2015)

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Designation: D5248 − 04 (Reapproved 2010) D5248 − 04 (Reapproved 2015)
Standard Specification for
Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
This standard is issued under the fixed designation D5248; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers the three grades of 1,1,2-trichloro 1,2,2-trifluoroethane typically needed in various industries. It
may be used as a reference document by purchasers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-trifluoroethane
recovery programs.
2. Referenced Documents
2.1 ASTM Standards:
D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acids and Other Related Products (Withdrawn 2002)
D2108 Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109 Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
D3401 Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
D3443 Test Method for Chloride in Trichlorotrifluoroethane
D3444 Test Method for Total Acid Number of Trichlorotrifluoroethane
D3741 Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
D6806 Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography
3. Classification
3.1 Type I—Generally recognized for use in precision applications.
3.2 Type II—Use for less demanding precision applications.
3.3 Type III—General-purpose technical grade.
4. Properties
4.1 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type I shall meet the requirements prescribed in Table 1.
4.2 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type II shall meet the requirements prescribed in Table 2.
4.3 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type III shall meet the requirements prescribed in Table 3.
5. Keywords
5.1 1,1,2-trichloro 1,2,2-trifluoroethane ; 1,2,2-trifluoroethane; CFC 113; Type I; Type II; Type III
This specification is under the jurisdiction of ASTM Committee D26 on Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct responsibility
of Subcommittee D26.02 on Vapor Degreasing.
Current edition approved Feb. 1, 2010June 1, 2015. Published March 2010June 2015. Originally approved in 1992. Last previous edition approved in 20042010 as
D5248 – 04.D5248 – 04(2010). DOI: 10.1520/D5248-04R10.10.1520/D5248-04R15.
1,1,2-trichloro 1,2,2-trifluoroethane: CAS No. 76-13-1.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
The last approved version of this historical standard is referenced on www.astm.org.
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D5248 − 04 (2015)
TABLE 1 Physical Properties Type I
Test
Property Specification
Method
Specific Gravity, 20/20 1.54 to 1.57 D2111
Chloride, ppm, max 0.1 D3443
Acid number 0.003 D3444
Non-volatile residue, ppm, max 10 D2109
Water, ppm, max 25 D3401 or
D1064
1,1,2-trichloro 1,2,2-trifluoroethane con
...