ASTM E2489-21
(Practice)Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
ABSTRACT
This practice describes methods for the statistical analysis of laboratory results obtained from interlaboratory proficiency testing programs. As in accordance with Practice E1301, proficiency testing is the use of inter-laboratory comparisons for the determination of laboratory testing or measurement performance. The methods provide direction for assessing and categorizing the performance of individual laboratories based on the relative likelihood of occurrence of their test results, and for determining estimates of testing variation associated with repeatability and reproducibility. Assumptions are that a majority of the participating laboratories execute the test method properly and that samples are of sufficient homogeneity that the testing results represent results obtained from each laboratory testing essentially the same material. Each laboratory receives the same instructions or protocol.
SIGNIFICANCE AND USE
5.1 This practice is specifically designed to describe simple robust statistical methods for use in proficiency testing programs.
5.2 Proficiency testing programs can use the methods in this practice for the purpose of comparing testing results obtained from a group of participating laboratories. The practice describes evaluation of individual laboratory results using the interquartile range and Tukey inner and outer fences.
5.3 In addition, the data obtained in proficiency testing programs may contain information regarding repeatability (within-lab) and reproducibility (between-lab) testing variation. Repeatability information is possible only if the program uses more than one sample. See Method B. Proficiency testing programs often have a greater number of participants than might be available for conducting an interlaboratory study to determine the precision of a test method (such as described in Practice E691). Precision estimates obtained for the larger number of participants in a proficiency testing program, along with the corresponding wider variation of test conditions, can provide useful information to standards developers regarding the precision of test results that can be expected for a test method when in actual use in the general testing community.
5.4 To estimate the precision of a test method, the participants must use the same test method to obtain their test results, and testing must be performed under the conditions required for repeatability and reproducibility. The precision estimates are applicable to the property levels and material types included in the testing program. The precision of a test method may vary considerably for different material types and at different property levels.
5.5 This practice may be useful to proficiency testing program administrators and provides examples of statistical methods along with explanations of some of the advantages of the suggested methods of analysis. The analyses resulting from the applicatio...
SCOPE
1.1 This practice describes methods for the statistical analysis of laboratory results obtained from interlaboratory proficiency testing programs. As in accordance with Practice E1301, proficiency testing is the use of interlaboratory comparisons for the determination of laboratory testing or measurement performance. Conversely, collaborative study (or collaborative trial) is the use of interlaboratory comparisons for the determination of the precision of a test method, as covered by Practice E691.
1.1.1 Method A covers testing programs using single test results obtained by testing a single sample (each laboratory submits a single test result).
1.1.2 Method B covers testing programs using paired test results obtained by testing two samples (each laboratory submits one test result for each of the two samples). The two samples should be of the same material or two materials similar enough to have approximately the same degree of variation in test results.
1.2 Methods A and B are applicable to proficiency test...
General Information
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Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:E2489 −21 An American National Standard
Standard Practice for
Statistical Analysis of One-Sample and Two-Sample
1
Interlaboratory Proficiency Testing Programs
This standard is issued under the fixed designation E2489; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 Thispracticedescribesmethodsforthestatisticalanaly-
1.5 This international standard was developed in accor-
sis of laboratory results obtained from interlaboratory profi-
dance with internationally recognized principles on standard-
ciency testing programs. As in accordance with Practice
ization established in the Decision on Principles for the
E1301, proficiency testing is the use of interlaboratory com-
Development of International Standards, Guides and Recom-
parisons for the determination of laboratory testing or mea-
mendations issued by the World Trade Organization Technical
surement performance. Conversely, collaborative study (or
Barriers to Trade (TBT) Committee.
collaborativetrial)istheuseofinterlaboratorycomparisonsfor
the determination of the precision of a test method, as covered
2. Referenced Documents
by Practice E691.
2
2.1 ASTM Standards:
1.1.1 Method A covers testing programs using single test
E177Practice for Use of the Terms Precision and Bias in
results obtained by testing a single sample (each laboratory
ASTM Test Methods
submits a single test result).
E178Practice for Dealing With Outlying Observations
1.1.2 Method B covers testing programs using paired test
E456Terminology Relating to Quality and Statistics
results obtained by testing two samples (each laboratory
E691Practice for Conducting an Interlaboratory Study to
submits one test result for each of the two samples). The two
Determine the Precision of a Test Method
samplesshouldbeofthesamematerialortwomaterialssimilar
E1301Guide for Proficiency Testing by Interlaboratory
enough to have approximately the same degree of variation in
3
Comparisons (Withdrawn 2012)
test results.
E2586Practice for Calculating and Using Basic Statistics
1.2 Methods A and B are applicable to proficiency testing
3. Terminology
programs containing a minimum of 10 participating laborato-
ries.
3.1 Definitions—Unlessotherwisenotedinthisstandard,all
terms relating to quality and statistics are defined in Terminol-
1.3 Themethodsprovidedirectionforassessingandcatego-
ogy E456.
rizing the performance of individual laboratories based on the
3.1.1 collaborative study, n—interlaboratory study in which
relative likelihood of occurrence of their test results, and for
each laboratory uses the defined method of analysis to analyze
determining estimates of testing variation associated with
identical portions of homogeneous materials to assess the
repeatability and reproducibility. Assumptions are that a ma-
performance characteristics obtained for that method of
jority of the participating laboratories execute the test method
4
analysis. Horwitz
properlyandthatsamplesareofsufficienthomogeneitythatthe
testing results represent results obtained from each laboratory
3.1.2 collaborative trial, n—see collaborative study.
testing essentially the same material. Each laboratory receives
3.1.3 interlaboratory comparison, n—organization,
the same instructions or protocol.
performance,andevaluationoftestsonthesameorsimilartest
1.4 This standard does not purport to address all of the
items by two or more laboratories in accordance with prede-
safety concerns, if any, associated with its use. It is the
termined conditions.
responsibility of the user of this standard to establish appro-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
1
ThispracticeisunderthejurisdictionofASTMCommitteeE11onQualityand Standards volume information, refer to the standard’s Document Summary page on
Statistics and is the direct responsibility of Subcommittee E11.20 on Test Method the ASTM website.
3
Evaluation and Quality Control. The last approved version of this historical standard is referenced on
Current edition approved Dec. 1, 2021. Published December 2021. Originally www.astm.org.
4
approved in 2006. Last previous edition approved in 2016 as E2489–16. DOI: Horwitz, W., “Protocol for the Design, Conduct and Interpretation of Collab-
10.15
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2489 − 16 E2489 − 21 An American National Standard
Standard Practice for
Statistical Analysis of One-Sample and Two-Sample
1
Interlaboratory Proficiency Testing Programs
This standard is issued under the fixed designation E2489; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This practice describes methods for the statistical analysis of laboratory results obtained from interlaboratory proficiency
testing programs. As in accordance with Practice E1301, proficiency testing is the use of interlaboratory comparisons for the
determination of laboratory testing or measurement performance. Conversely, collaborative study (or collaborative trial) is the use
of interlaboratory comparisons for the determination of the precision of a test method, as covered by Practice E691.
1.1.1 Method A covers testing programs using single test results obtained by testing a single sample (each laboratory submits a
single test result).
1.1.2 Method B covers testing programs using paired test results obtained by testing two samples (each laboratory submits one
test result for each of the two samples). The two samples should be of the same material or two materials similar enough to have
approximately the same degree of variation in test results.
1.2 Methods A and B are applicable to proficiency testing programs containing a minimum of 10 participating laboratories.
1.3 The methods provide direction for assessing and categorizing the performance of individual laboratories based on the relative
likelihood of occurrence of their test results, and for determining estimates of testing variation associated with repeatability and
reproducibility. Assumptions are that a majority of the participating laboratories execute the test method properly and that samples
are of sufficient homogeneity that the testing results represent results obtained from each laboratory testing essentially the same
material. Each laboratory receives the same instructions or protocol.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
1
This practice is under the jurisdiction of ASTM Committee E11 on Quality and Statistics and is the direct responsibility of Subcommittee E11.20 on Test Method
Evaluation and Quality Control.
Current edition approved Nov. 15, 2016Dec. 1, 2021. Published November 2016December 2021. Originally approved in 2006. Last previous edition approved in 20112016
as E2489 – 11.E2489 – 16. DOI: 10.1520/E2489-16.10.1520/E2489-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
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E2489 − 21
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E178 Practice for Dealing With Outlying Observations
E456 Terminology Relating to Quality and Statistics
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3
E1301 Guide for Proficiency Testing by Interlaboratory Comparisons (Withdrawn 2012)
E2586 Practice for Calculating and Using Basic Statistics
3. Terminology
3.1 Definitions—The terminology defined in Terminology—Unless otherwise noted in this E456 applies to this practice unless
modified herein.standard, all terms relating to quality and statistics are defined in Terminology E456.
3.1.1 collaborative study, n—interlaboratory study
...
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