D05.23 - Sampling

ABSTRACT
This specification covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite. These coals are mainly composed of vitrinite. The classification shall be based on gradational properties that depend on the degree of metamorphism. The classification shall also be according to fixed carbon and gross calorific value calculated to the mineral-matter-free basis.
SIGNIFICANCE AND USE
4.1 This classification establishes categories of coal based on gradational properties that depend principally on the degree of metamorphism to which the coal was subjected while buried. These categories indicate ranges of physical and chemical characteristics that are useful in making broad estimates of the behavior of coal in mining, preparation, and use.
SCOPE
1.1 This standard covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite.  
1.2 This classification is applicable to coals that are composed mainly of vitrinite.  
Note 1: Coals rich in inertinite or liptinite (exinite), or both, cannot be properly classified because, in those macerals, the properties that determine rank (calorific value, volatile matter, and agglomerating character) differ greatly from those of vitrinite in the same coal. Often, such coals can be recognized by megascopic examination. In North America, these coals are mostly nonbanded varieties that contain only a small proportion of vitrain and consist mainly of attrital materials. The degree of metamorphism of nonbanded and other vitrinite-poor coals can be estimated by determining the classification properties of isolated or concentrated vitrinite fractions, or by determining the reflectance of the vitrinite (see Test Method D2798 and Appendix X1 of this classification). However, in the use of these vitrinite-poor coals, some properties normally associated with rank, such as rheology, combustibility, hardness, and grindability (as well as the rank determining properties) may differ substantially from those of vitrinite-rich coals of the same degree of metamorphism.  
1.3 The accuracy of the classification of impure coal may be impaired by the effect of large amounts of mineral matter on the determination of volatile matter and calorific value, and on their calculation to the mineral-matter-free basis.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4.1 Exception—The values stated in British thermal units per pound (Btu/lb) are to be regarded as the standard. The SI equivalents of Btu/lb are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement, and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous Practices D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 35, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 A properly collected face channel sample that includes the total coal bed interval provides a sample that is a representative cross section of the coal bed at the point of sampling. Channel samples are taken for subsequent testing needed for evaluation of coal quality and characterization for commercial evaluations, for planning of mining operations to maintain coal quality, for the determination of coal rank in accordance with Classification D388, and for geologic coal resource studies.  
Note 1: Because of the potential for lateral variability, a sample may not represent the quality of the coal bed at another sample point. The reliability of the data generated from channel samples is dependent on the number and spacing of the sample points and the variability of the coal characteristics in a given area.
Note 2: Sampling of the mine product for these purposes is unsatisfactory because of contamination of the product with out-of-seam material, selective mining of parts of a seam, inability to obtain samples from one or more specific locations in the mine, or other incompatibility of the purpose of sampling with the mining practice. Conversely, channel samples should not be used for evaluation of the quality of commercial shipments of the mine product, which should be sampled in accordance with Methods D2234/D2234M.
SCOPE
1.1 This practice describes procedures for collecting a coal sample from a channel extending from top to bottom in the face of a coal seam in a mine.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary information, see Note 2.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 A properly collected sample that includes the total coal bed interval provides a sample that is a representative cross section of the coal bed at the point of sampling. Core samples are taken for subsequent testing needed for evaluation of coal quality and characterization for commercial evaluations, for planning of mining operations to maintain coal quality, for the determination of coal rank in accordance with Classification D388, and for geologic coal resource studies.  
Note 1: Because of the potential for lateral variability, a sample may not represent the quality of the coal bed at another sample point. The reliability of the data generated from core samples is dependent on the number and spacing of the sample points and the variability of the coal characteristics in a given area.  
5.2 Moisture determined directly from a core sample shall be considered questionable in any core sample because of possible contamination from drilling fluids and groundwater. If a more representative estimate of the inherent moisture content of the core sample (with the exception of certain low-rank coals) is desired, the sample should be analyzed according to Test Method D1412.
SCOPE
1.1 This practice describes procedures for collecting and handling a coal sample from a core recovered from a borehole.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013/D2013M provides instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.  
5.2 Division and reduction of a sample may occur at more than one location. Most often, the sample is collected, reduced, and divided (one or more times) by use of a mechanical sampling system. The remaining sample may be further divided on-site to facilitate transporting it to the laboratory where further reduction and division likely occurs before analysis.  
5.3 In places, this practice requires air drying the sample before subsequent reduction. Procedures for air drying and air-dry loss determination are provided in Test Method D3302/D3302M.  
5.4 Most often, samples are reduced and divided to an analysis sample. However, some tests may require a sample of different mass or top size. This procedure may be used to provide a sample of any mass and size consist from the gross or divided sample to, and including, the analysis sample.  
5.5 This practice also specifies how to prepare composite samples, if required.
SCOPE
1.1 This practice2 covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.  
1.2 Reduction and division procedures are prescribed for coals of the following groups:  
1.2.1 Group A includes coals that have been cleaned in all sizes.  
1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.  
1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of sampling equipment, caution should be used in all stages of sampling, from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.  
5.2 After further processing (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may affect the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice covers procedures for the collection of a sample under various conditions of sampling and directs the user to the appropriate ASTM standard for that sampling condition. The sample is to be crushed and further prepared for analysis in accordance with Practice D2013/D2013M. However, the procedures for dividing large samples before any crushing are given in this practice.  
1.2 This practice describes general and special purpose sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal) and (2) by sampling characteristics.  
1.3 Units—The values stated in either SI units or non-SI units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer: (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (for example, a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This practice may be used to provide a representative sample of the coke from which it is collected. Due to the variability of coke and the wide variety of sampling equipment, caution must be exercised in all stages of sampling, from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.  
3.2 This practice also provides an analysis sample of coke from the gross or divided sample. The analysis samples can be used to determine the value of the coke represented, its ability to meet specifications, as well as for other purposes.
SCOPE
1.1 This practice covers procedures for the collection and reduction of samples of coke to be used for physical tests, chemical analyses, and the determination of total moisture.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.2.1 Values in SI units [or inch-pound units] shall be obtained by measurement in SI units [or inch-pound units] or by appropriate conversion, using the Rules for Conversion and Rounding given in IEEE/ASTM SI 10, of measurements made in SI units [or other units]. Values are stated in SI units when inch-pound units are not used in practice.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This guide provides instructions for sampling by collecting individual increments from part of a cross section of a moving stream of coal, as opposed to collection of individual increments by removal of a full cross section of material. The use of part-stream sampling, and the detailed procedures for each case, should be agreed upon in advance by all parties concerned. Samples collected by use of this guide are not probability samples. The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to obtain any meaningful statistical inferences such as the sampling precision, standard error, or bias.  
5.2 All parties should be cautioned that manual sampling of coal from a moving stream might not enable sampling of the material that is furthermost from the point of entry into stream by the sampling device.
SCOPE
1.1 This guide covers general principles for obtaining a gross sample of coal by taking increments from part of a stream of coal rather than from the entire stream to be sampled. The usefulness of results from this guide will vary greatly depending on such factors as top size of the coal, size consistency of the coal, variability of the coal, and such logistical factors as the flow rate of the coal in process and physical accessibility of the sampling station.  
1.2 This guide should be used only when it is not possible to use a method of sampling that produces a probability sample.  
1.3 Sample preparation procedures involving crushing are contained in Practice D2013.  
1.4 The values stated in SI units are to be regarded as standard. The values in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory requirements prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 These guidelines provide procedures for manually collecting gross samples from beneath the exposed surface of coal in railroad cars, barges, trucks, or stockpiles taking into account the wide variety of conditions that may be encountered. The samples are further processed for the laboratory to provide estimations of the coal quality. The use of this practice is conditional upon agreement among all interested parties concerning all relevant details of sample collection before sampling begins. These include, but are not limited to: lot size; number and mass of increments; the size, shape, and manipulation of the increment collection devices; location of increment collection site or sites; circumstances under which increments are not to be collected or suspended; and safety precautions. It is preferable that such agreements be in writing. The user is cautioned that samples so obtained do not represent material below the point of penetration.
SCOPE
1.1 This practice covers procedures for obtaining a manual gross sample from beneath the surface of coal in railroad cars, barges, trucks, or stockpiles. These procedures are to be used to provide gross samples for estimating the quality of the coal. The gross samples are to be crushed, divided, and further prepared for analysis in accordance with Practice D2013.  
1.2 This practice provides instruction for sampling beneath the exposed surface coal to a depth of approximately 61 cm (24 in.). Collect samples at this depth to get below the surface of the material, since drying and oxidation may have occurred at, or near the surface. Changes in moisture, in particle size, and in other properties continue to occur deeper in the coal and, although not as drastic as near the surface, will cause the method to be biased. The user should review the conditions of the coal (weather conditions, prior transport, settling time, and so forth, see 8.1) so that the interested parties can agree that potential biases are not overly great or that some adjustment in specifications is warranted. Sample increments collected from the surface layer(s) of coal in railroad cars, barges, or stockpiles are classified condition “D” (see Practice D2234/D2234M, Increment Collection Classification). It is a good practice to require that “details of sampling procedure shall be agreed upon in advance by all parties concerned” whenever collection of sample increments falls under condition “D.” This practice offers a sampling procedure that parties may use to meet requirements of Practice D2234/D2234M for condition “D.” The practice does not produce samples that satisfy precision requirements of Practice D2234/D2234M general-purpose sampling, or Practice D2234/D2234M special-purpose sampling.  
1.3 The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to draw statistical inferences such as precision, standard error, or bias.  
1.4 This sampling method is intended for use only when sampling by more reliable methods that provide a probability sample is not possible.  
1.5 The quantities stated in either acceptable SI units or in inch-pound units are regarded separately as standard. The quantities stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining quantities in any way.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the ...

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement, and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous Practices D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 35, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement, and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous Practices D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 35, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013/D2013M provides instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.  
5.2 Division and reduction of a sample may occur at more than one location. Most often, the sample is collected, reduced, and divided (one or more times) by use of a mechanical sampling system. The remaining sample may be further divided on-site to facilitate transporting it to the laboratory where further reduction and division likely occurs before analysis.  
5.3 In places, this practice requires air drying the sample before subsequent reduction. Procedures for air drying and air-dry loss determination are provided in Test Method D3302/D3302M.  
5.4 Most often, samples are reduced and divided to an analysis sample. However, some tests may require a sample of different mass or top size. This procedure may be used to provide a sample of any mass and size consist from the gross or divided sample to, and including, the analysis sample.  
5.5 This practice also specifies how to prepare composite samples, if required.
SCOPE
1.1 This practice2 covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.  
1.2 Reduction and division procedures are prescribed for coals of the following groups:  
1.2.1 Group A includes coals that have been cleaned in all sizes.  
1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.  
1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer: (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (for example, a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of sampling equipment, caution should be used in all stages of sampling from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.  
5.2 After further processing (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may affect the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice covers procedures for the collection of a sample under various conditions of sampling and directs the user to the appropriate ASTM standard for that sampling condition. The sample is to be crushed and further prepared for analysis in accordance with Practice D2013/D2013M. However, the procedures for dividing large samples before any crushing are given in this practice.  
1.2 This practice describes general and special purpose sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal) and (2) by sampling characteristics.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite. These coals are mainly composed of vitrinite. The classification shall be based on gradational properties that depend on the degree of metamorphism. The classification shall also be according to fixed carbon and gross calorific value calculated to the mineral-matter-free basis.
SIGNIFICANCE AND USE
4.1 This classification establishes categories of coal based on gradational properties that depend principally on the degree of metamorphism to which the coal was subjected while buried. These categories indicate ranges of physical and chemical characteristics that are useful in making broad estimates of the behavior of coal in mining, preparation, and use.
SCOPE
1.1 This standard covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite.  
1.2 This classification is applicable to coals that are composed mainly of vitrinite.  
Note 1: Coals rich in inertinite or liptinite (exinite), or both, cannot be properly classified because, in those macerals, the properties that determine rank (calorific value, volatile matter, and agglomerating character) differ greatly from those of vitrinite in the same coal. Often, such coals can be recognized by megascopic examination. In North America, these coals are mostly nonbanded varieties that contain only a small proportion of vitrain and consist mainly of attrital materials. The degree of metamorphism of nonbanded and other vitrinite-poor coals can be estimated by determining the classification properties of isolated or concentrated vitrinite fractions, or by determining the reflectance of the vitrinite (see Test Method D2798 and Appendix X1 of this classification). However, in the use of these vitrinite-poor coals, some properties normally associated with rank, such as rheology, combustibility, hardness, and grindability (as well as the rank determining properties) may differ substantially from those of vitrinite-rich coals of the same degree of metamorphism.  
1.3 The accuracy of the classification of impure coal may be impaired by the effect of large amounts of mineral matter on the determination of volatile matter and calorific value, and on their calculation to the mineral-matter-free basis.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4.1 Exception—The values stated in British thermal units per pound (Btu/lb) are to be regarded as the standard. The SI equivalents of Btu/lb are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013 provides instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.  
5.2 Division and reduction of a sample may occur at more than one location. Most often, the sample is collected, reduced, and divided (one or more times) by use of a mechanical sampling system. The remaining sample may be further divided on-site to facilitate transporting it to the laboratory where further reduction and division likely occurs before analysis.  
5.3 In places, this practice requires air drying the sample before subsequent reduction. Procedures for air drying and air-dry loss determination are provided in Test Method D3302/D3302M.  
5.4 Most often, samples are reduced and divided to an analysis sample. However, some tests may require a sample of different mass or top size. This procedure may be used to provide a sample of any mass and size consist from the gross or divided sample to, and including, the analysis sample.  
5.5 This practice also specifies how to prepare composite samples, if required.
SCOPE
1.1 This practice2 covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.  
1.2 Reduction and division procedures are prescribed for coals of the following groups:  
1.2.1 Group A includes coals that have been cleaned in all sizes.  
1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.  
1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 11.2.2, 21, 1.4, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 11.2.2, 21, 1.4, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 11.2.2, 21, 1.4, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts A, B, C, and D. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 39.1.6, 21, 1.4, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of sampling equipment, caution should be used in all stages of sampling from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.  
5.2 After further processing (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may affect the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice covers procedures for the collection of a sample under various conditions of sampling. The sample is to be crushed and further prepared for analysis in accordance with Practice D2013/D2013M. However, the procedures for dividing large samples before any crushing are given in this practice. For the sampling of coal using mechanical sampling systems see D7430 Practice for the Mechanical Sampling of Coal.  
1.2 This practice describes general and special purpose sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal) and (2) by sampling characteristics.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts A, B, C, and D. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 39.1.6, 21, 1.4, and 38.1.1.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts A, B, C, and D. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 39.1.6, 21, 1.4, and 38.1.1.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts A, B, C, and D. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 31.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 34, and 37.1.1.

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts A, B, C, and D. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 31.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 34, and 37.1.1.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of sampling equipment, caution should be used in all stages of sampling from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.  
5.2 After further processing (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may affect the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice covers procedures for the collection of a sample under various conditions of sampling. The sample is to be crushed and further prepared for analysis in accordance with Practice D2013/D2013M. However, the procedures for dividing large samples before any crushing are given in this practice. For the sampling of coal using mechanical sampling systems see D7430 Practice for the Mechanical Sampling of Coal.  
1.2 This practice describes general and special purpose sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal) and (2) by sampling characteristics.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.
Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Part B  
1.3 Part B—Mechanical Auger Sampling—Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are in...

SIGNIFICANCE AND USE
4.1 A properly collected face channel sample that includes the total coal bed interval provides a sample that is a representative cross section of the coal bed at the point of sampling. Channel samples are taken for subsequent testing needed for evaluation of coal quality and characterization for commercial evaluations, for planning of mining operations to maintain coal quality, for the determination of coal rank in accordance with Classification D388, and for geologic coal resource studies.  
Note 1: Because of the potential for lateral variability, a sample may not represent the quality of the coal bed at another sample point. The reliability of the data generated from channel samples is dependent on the number and spacing of the sample points and the variability of the coal characteristics in a given area.
Note 2: Sampling of the mine product for these purposes is unsatisfactory because of contamination of the product with out-of-seam material, selective mining of parts of a seam, inability to obtain samples from one or more specific locations in the mine, or other incompatibility of the purpose of sampling with the mining practice. Conversely, channel samples should not be used for evaluation of the quality of commercial shipments of the mine product, which should be sampled in accordance with Methods D2234/D2234M.
SCOPE
1.1 This practice describes procedures for collecting a coal sample from a channel extending from top to bottom in the face of a coal seam in a mine.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary information, see Note 2.

SIGNIFICANCE AND USE
5.1 A properly collected sample that includes the total coal bed interval provides a sample that is a representative cross section of the coal bed at the point of sampling. Core samples are taken for subsequent testing needed for evaluation of coal quality and characterization for commercial evaluations, for planning of mining operations to maintain coal quality, for the determination of coal rank in accordance with Classification D388, and for geologic coal resource studies.  
Note 1: Because of the potential for lateral variability, a sample may not represent the quality of the coal bed at another sample point. The reliability of the data generated from core samples is dependent on the number and spacing of the sample points and the variability of the coal characteristics in a given area.  
5.2 Moisture determined directly from a core sample shall be considered questionable in any core sample because of possible contamination from drilling fluids and groundwater. If a more representative estimate of the inherent moisture content of the core sample (with the exception of certain low-rank coals) is desired, the sample should be analyzed according to Test Method D1412.
SCOPE
1.1 This practice describes procedures for collecting and handling a coal sample from a core recovered from a borehole.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.
Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are i...

SIGNIFICANCE AND USE
5.1 This guide provides instructions for sampling by collecting individual increments from part of a cross section of a moving stream of coal, as opposed to collection of individual increments by removal of a full cross section of material. The use of part-stream sampling, and the detailed procedures for each case, should be agreed upon in advance by all parties concerned. Samples collected by use of this guide are not probability samples. The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to obtain any meaningful statistical inferences such as the sampling precision, standard error, or bias.  
5.2 All parties should be cautioned that manual sampling of coal from a moving stream might not enable sampling of the material that is furthermost from the point of entry into stream by the sampling device.
SCOPE
1.1 This guide covers general principles for obtaining a gross sample of coal by taking increments from part of a stream of coal rather than from the entire stream to be sampled. The usefulness of results from this guide will vary greatly depending on such factors as top size of the coal, size consistency of the coal, variability of the coal, and such logistical factors as the flow rate of the coal in process and physical accessibility of the sampling station.  
1.2 This guide should be used only when it is not possible to use a method of sampling that produces a probability sample.  
1.3 Sample preparation procedures involving crushing are contained in Practice D2013.  
1.4 The values stated in SI units are to be regarded as standard. The values in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.
Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are i...

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included i...

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides the means of evaluating the analyzer system and the data produced.  
5.2 Become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test should be carefully designed to ensure the user’s requirements are met.  
5.3 The procedures defined in this guide can be used to estimate the accuracy and precision of an online analyzer, (1) to conduct acceptance testing following installation and (2) to monitor the accuracy and precision (a) during routine use (quality control), (b) when significant changes are made to the analyzer, and (c) when a significant change in the coal being analyzed occurs (e.g., a different seam at a mine, or a new coal source at a power plant). These procedures can also be used for calibration purposes.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included i...

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included i...

SIGNIFICANCE AND USE
5.1 These guidelines provide procedures for manually collecting gross samples from beneath the exposed surface of coal in railroad cars, barges, trucks, or stockpiles taking into account the wide variety of conditions that may be encountered. The samples are further processed for the laboratory to provide estimations of the coal quality. The use of this practice is conditional upon agreement among all interested parties concerning all relevant details of sample collection before sampling begins. These include, but are not limited to: lot size; number and mass of increments; the size, shape, and manipulation of the increment collection devices; location of increment collection site or sites; circumstances under which increments are not to be collected or suspended; and safety precautions. It is preferable that such agreements be in writing. The user is cautioned that samples so obtained do not represent material below the point of penetration.
SCOPE
1.1 This practice covers procedures for obtaining a manual gross sample from beneath the surface of coal in railroad cars, barges, trucks, or stockpiles. These procedures are to be used to provide gross samples for estimating the quality of the coal. The gross samples are to be crushed, divided, and further prepared for analysis in accordance with Practice D2013.  
1.2 This practice provides instruction for sampling beneath the exposed surface coal to a depth of approximately 61 cm (24 in.). Collect samples at this depth to get below the surface of the material, since drying and oxidation may have occurred at, or near the surface. Changes in moisture, in particle size, and in other properties continue to occur deeper in the coal and, although not as drastic as near the surface, will cause the method to be biased. The user should review the conditions of the coal (weather conditions, prior transport, settling time, and so forth, see 8.1) so that the interested parties can agree that potential biases are not overly great or that some adjustment in specifications is warranted. Sample increments collected from the surface layer(s) of coal in railroad cars, barges, or stockpiles are classified condition “D” (see Practice D2234/D2234M, Increment Collection Classification). It is a good practice to require that “details of sampling procedure shall be agreed upon in advance by all parties concerned” whenever collection of sample increments falls under condition “D.” This practice offers a sampling procedure that parties may use to meet requirements of Practice D2234/D2234M for condition “D.” The practice does not produce samples that satisfy precision requirements of Practice D2234/D2234M general-purpose sampling, or Practice D2234/D2234M special-purpose sampling.  
1.3 The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to draw statistical inferences such as precision, standard error, or bias.  
1.4 This sampling method is intended for use only when sampling by more reliable methods that provide a probability sample is not possible.  
1.5 The quantities stated in either acceptable SI units or in inch-pound units are regarded separately as standard. The quantities stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining quantities in any way.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.  
5.2 After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.Part A  
1.2 Part A—Mechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.  
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.  
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.Part B  
1.3 Part B—Mechanical Auger Sampling——Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.  
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.Part C  
1.4 Part C—Quality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.  
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.  
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.  
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.  
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.  
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included i...

SIGNIFICANCE AND USE
5.1 On-line analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides means of evaluating the system and data produced.  
5.2 The user should become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test design should be carefully considered so as to assure meeting the user's requirements.  
5.3 The procedures defined in this guide can be used to test the accuracy and precision of an on-line analyzer, for acceptance after its installation, to check precision and accuracy during routine use (quality control), when changes are made to the system, when the nature of the coal being tested changes, and to determine mathematical factors to be used for calibration of the on-line analyzer.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of on-line coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
5.1 Online analyzers are used to provide quality data on lots of coal. The resulting quality data are used as a production tool or for some contractual application. This guide provides means of evaluating the system and data produced.  
5.2 The user should become familiar with the document's terminology and layout. The section on test design and data collection will provide the means by which all the analysis data will be gathered. The test design should be carefully considered to assure meeting the user's requirements.  
5.3 The procedures defined in this guide can be used to test the accuracy and precision of an online analyzer, for acceptance after its installation, to check precision and accuracy during routine use (quality control), when changes are made to the system, when the nature of the coal being tested changes, and to determine mathematical factors to be used for calibration of the online analyzer.
SCOPE
1.1 This guide provides techniques to be used for the evaluation of the measurement performance of online coal analyzers.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.
After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
Top  
1.2 Part AMechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Part B  Top  
1.3 Part BMechanical Auger Sampling—Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Part C  Top  
1.4 Part CQuality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Part D  Top  
1.5 Part DBias Testing of a Mechanical Coal Sampling System—Presents sample collection and statistical evaluation procedures for testing mechanical sampling systems (including auger systems), subsystems, and individual system components for bias. It is the responsibility of the u...

SIGNIFICANCE AND USE
Other standards are used to collect the gross sample: Practice D2234/D2234M allows for one division of the gross sample before crushing. The mass and top size of the gross or divided sample collected by using these guides and practices are usually too large for chemical or physical testing. Practice D2013 provide instructions for reducing and dividing the gross or divided sample, by on-line or off-line processes, or both, to a top size and mass suitable to the performance of testing. Any bias in the gross or divided sample before adherence to this practice will remain in the final sample resulting from use of this practice. Therefore, carefully select the standard to be used to collect the gross sample.
Division and reduction of a sample may occur at more than one location. Most often, the sample is collected, reduced, and divided (one or more times) by use of a mechanical sampling system. The remaining sample may be further divided on-site to facilitate transporting it to the laboratory where further reduction and division likely occurs before analysis.
In places, this practice requires air drying the sample before subsequent reduction. Procedures for air drying and air-dry loss determination are provided in Test Method D3302.
Most often, samples are reduced and divided to an analysis sample. However, some tests may require a sample of different mass or top size. This procedure may be used to provide a sample of any mass and size consist from the gross or divided sample to, and including, the analysis sample.
This practice also specifies how to prepare composite samples, if required.
SCOPE
1.1 This practice covers the reduction and division of gross or divided samples, and the preparation of composite samples, up to and including the individual portions for laboratory analysis.
1.2 Reduction and division procedures are prescribed for coals of the following groups:
1.2.1 Group A includes coals that have been cleaned in all sizes.
1.2.2 Group B includes all other coals. Unknown coals are to be considered under Group B.
1.2.3 Group A allows smaller weight laboratory samples to be retained than Group B. These lower weights may be used for particular coals if they have been shown, by using the procedures of Annex A1.2, to give a sample preparation and analysis variance which is no more than 20 % of the total analysis variance.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement and the acceptance testing of installed equipment.
After removal from the sampling system and further preparation (Practice D2013), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into 4 parts. These 4 parts represent the previous standards D7256/D7256M, D4916, D4702, and D6518. These 4 standards are the 4 that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards. Part A  Top  
1.2 Part AMechanical Collection and Within-System Preparation of a Gross Sample of Coal from Moving Streams—Covers procedures for the mechanical collection of a sample under Classification I-B-1 and I-B-2 (Practice D2234/D2234M) and the within-system preparation (reduction and division) of gross samples utilizing various components of the mechanical sampling system.
1.2.1 Part A describes mechanical sampling procedures for coals (1) by size and condition of preparation (for example, mechanically cleaned coal or raw coal), and (2) by sampling characteristics.
1.2.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Part B  Top  
1.3 Part BMechanical Auger Sampling—Describes procedures for the collection of an increment, partial sample, or gross sample of material using mechanical augers. Reduction and division of the material by mechanical equipment at the auger is also covered. Further manual or mechanical reduction or division of the material elsewhere shall be performed in accordance with Practice D2013.
1.3.1 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Part C  Top  
1.4 Part CQuality Management of Mechanical Coal Sampling Systems—Is applicable to the quality management of cross-belt, falling stream, and auger sampling systems.
1.4.1 Spacing of increments pertains to the kind of interval between increments. Intervals can be defined in quantitative terms, such as units of time or mass, or in terms of position over the lot.
1.4.2 Spacing of Increments for Cross-Belt and Falling Stream Samplers—Cross-belt and falling stream type mechanical sampling systems take increments based on time, either at fixed time intervals or at random times during a fixed time strata. Some falling stream samplers can take increments based on equal mass of coal sampled as determined by scales. The sections of this practice that pertain to cross-belt and falling stream samplers describe procedures for only time-based sampling systems. This time-based inspection guideline will satisfy most criteria for mass-based or combination mass-based and time-based sampling systems. If there are items that are not covered, the inspector should refer to the manufacturer's literature.
1.4.3 Spacing of Increments for Auger Sampling—The spacing of increments collected by auger sampling systems is defined in terms of position over the lot.
1.4.4 It is essential that the inspector have the documentation listed in Section 2 of this practice when conducting an inspection.
1.4.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in t...

SIGNIFICANCE AND USE
This practice may be used to provide a representative sample of the coke from which it is collected. Because of the variability of coke and the wide variety of sampling equipment, caution must be exercised in all stages of sampling, from system specifications and equipment procurement to equipment acceptance testing and actually taking the final sample.
This practice also provides an analysis sample of coke from the gross or divided sample. The analysis samples can be used to determine the value of the coke represented, its ability to meet specifications, as well as for other purposes.
SCOPE
1.1 This practice covers procedures for the collection and reduction of samples of coke to be used for physical tests, chemical analyses, and the determination of total moisture.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.2.1 Values in SI units [or inch-pound units] shall be obtained my measurement in SI units [or inch-pound units] or by appropriate conversion, using the Rules for Conversion and Rounding given in , of measurements made in other units [or SI units]. Values are state ins SI units when inch-pound units are not used in practice.
1.3 This standard does not purport to address the safety concerns associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.