Bitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation

This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions.
The method can also be used to obtain residue and oil distillate for further testing.
NOTE   The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens, cut-back and fluxed bituminous binders.
WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels Destillation

Diese Europäische Norm legt ein Verfahren zur quantitativen Bestimmung des verbleibenden Bindemittels und des Öldestillates in Bitumenemulsionen fest.
Das Verfahren kann auch angewendet werden, um den Rückstand und das Öldestillat für weitere Prüfungen zu erhalten.
ANMERKUNG   Die an dem mit diesem Verfahren gewonnenen Material ermittelten Stoffeigenschaften gleichen nicht notwendigerweise denen der Ausgangsstoffe, aus denen die Emulsion hergestellt wurde; dies gilt besonders für polymermodifizierte Bitumen, verschnittene und gefluxte bitumenhaltige Bindemittel.
WARNUNG - Die Anwendung dieser Norm kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Diese Norm beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieser Norm, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.

Bitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitume

La présente Norme européenne définit une méthode de détermination quantitative du liant résiduel et du distillat d'huile dans des émulsions bitumineuses.
La présente méthode d'essai peut également être utilisée pour obtenir du liant résiduel et du distillat d'huile pour des essais ultérieurs.
NOTE   Les propriétés du matériau récupéré par le présent essai ne sont pas nécessairement les mêmes que celles des matériaux d'origine à partir desquels on a produit l'émulsion, et ce plus particulièrement pour les bitumes modifiés par des polymères, les bitumes fluidifiés et les bitumes fluxés.
AVERTISSEMENT - L'utilisation de la présente Norme européenne peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n’est pas censée aborder tous les problèmes de sécurité associés à son usage. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje veziva in oljnega destilata v bitumenskih emulzijah z metodo destilacije

Ta evropski standard določa metodo za kvantitativno določevanje veziva in oljnega destilata v bitumenskih emulzijah. Metoda se lahko uporablja tudi za pridobivanje ostankov in oljnega destilata za nadaljnje preskušanje. OPOMBA: Lastnosti materiala, pridobljenega v preskusih, niso nujno enake lastnostim izvirnih materialov, iz katerih je bila emulzija izdelana. To še posebej velja za bitumne, modificirane s polimeri. OPOZORILO – Pri uporabi tega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega standarda.

General Information

Status
Published
Public Enquiry End Date
29-Apr-2016
Publication Date
16-May-2018
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
03-Apr-2018
Due Date
08-Jun-2018
Completion Date
17-May-2018

Relations

Overview

EN 1431:2018 (CEN) specifies a laboratory distillation method for the quantitative determination of residual binder and oil distillate in bitumen emulsions. The procedure separates water and low‑boiling oil fractions by distillation, collects the oil distillate in a graduated cylinder and yields the residual binder after distillation for mass determination or further testing. The standard notes that properties of the recovered residue may differ from the original product (notably for polymer‑modified, cut‑back or fluxed binders) and highlights health and safety responsibilities.

Key topics and requirements

  • Scope: quantitative determination of residual binder and oil distillate; also provides residue for additional tests.
  • Principle: distil water and oil from a weighed emulsion sample; measure oil volume (D) and weigh residue (Bm) to calculate mass percentages.
  • Sample & sample size: laboratory sampling per EN 58; typical test mass 200 g (tared still).
  • Apparatus & reagents:
    • aluminium or iron still, connection condenser, 100 ml graduated cylinder (1 ml divisions), sieves (300 µm), balance (±0.1 g), two temperature measuring devices (10–300 °C, ±1 °C).
    • sodium hydroxide solution 40 g/l (or other suitable basic solution) to aid separation for cationic emulsions.
    • heating by gas ring burner or controlled electric ring heater (electric heating permitted when only content determination is required).
  • Procedure essentials:
    • insert two thermometers at specified depths; heat until lower thermometer reaches ~215 °C then to (260 ± 5) °C for 15 min; complete distillation in ~60 ± 15 min (up to 120 min allowed with electrical heating in some cases).
    • cool, weigh residue and record oil distillate volume; determine oil density (EN ISO 3838 or supplier value) to convert volume to mass.
  • Calculations & results:
    • residual binder content (%) = (Bm / Am) × 100.
    • oil distillate content (%) = (ρ · D / Am) × 100.
    • express results to nearest 0.1%.

Applications

  • Quality control and production monitoring of bitumen emulsions in manufacturing plants.
  • Laboratory evaluation for pavement materials, specifications and acceptance testing in road construction.
  • Generating residue and distillate samples for further characterization (e.g., rheology, penetration) used by formulation engineers and researchers.
  • Verifying supplier declarations of binder and solvent content.

Who should use this standard

  • Materials/test laboratories, bitumen and emulsion manufacturers, pavement engineers, specification authors, regulators and researchers involved in binder analysis and quality assurance.

Related standards

  • EN 58 (sampling), EN 12594 (sample preparation), EN ISO 3838 (density), EN ISO 4788 (graduated cylinders), EN 1425 (material homogeneity), ISO 565 (sieves).

Note: Follow EN 1431:2018 safety warnings; establish appropriate lab safety and regulatory compliance before testing.

Standard
SIST EN 1431:2018 - BARVE
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Frequently Asked Questions

SIST EN 1431:2018 is a standard published by the Slovenian Institute for Standardization (SIST). Its full title is "Bitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation". This standard covers: This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions. The method can also be used to obtain residue and oil distillate for further testing. NOTE The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens, cut-back and fluxed bituminous binders. WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions. The method can also be used to obtain residue and oil distillate for further testing. NOTE The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens, cut-back and fluxed bituminous binders. WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIST EN 1431:2018 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.

SIST EN 1431:2018 has the following relationships with other standards: It is inter standard links to SIST EN 1431:2009. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase SIST EN 1431:2018 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of SIST standards.

Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels DestillationBitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitumeBitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 1431:2018SIST EN 1431:2018en,fr,de01-junij-2018SIST EN 1431:2018SLOVENSKI
STANDARDSIST EN 1431:20091DGRPHãþD

EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 1431
March
t r s z ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s v u sã t r r {English Version
Bitumen and bituminous binders æ Determination of residual binder and oil distillate from bitumen emulsions by distillation Bitumes et liants bitumineux æ Détermination par distillation du liant résiduel et du distillat d 5huile dans les émulsions de bitumes
Bitumen und bitumenhaltige Bindemittel æ Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels Destillation This European Standard was approved by CEN on
x November
t r s yä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Rue de la Science 23,
B-1040 Brussels
t r s z CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s v u sã t r s z ESIST EN 1431:2018

Characteristics of thermometer . 14 Bibliography . 15
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The article discusses SIST EN 1431:2018, a European standard that outlines a method for determining the amount of residual binder and oil distillate in bituminous emulsions. This method can be used to obtain samples for additional testing. It is important to note that the properties of the recovered material may not be the same as the original materials, particularly for polymer modified bitumens. The use of this standard may involve hazardous materials, operations, and equipment, so it is the user's responsibility to ensure appropriate safety measures are in place and comply with relevant regulations.

기사 제목: SIST EN 1431:2018 - 비트유민과 비트유수분자의 증류에 의한 비트유 관련물 및 오일 증류물의 정량 분석 기사 내용: 이 유럽 표준은 비트유민에 있는 잔류제 및 오일 증류물의 양을 정량 측정하는 방법을 명시합니다. 이 방법은 추가적인 실험을 위해 잔류물과 오일 증류물을 얻는 데에도 사용될 수 있습니다. 참고로, 이 실험에서 회수되는 물질의 특성은 특히 고분자 수정 비트유에서 원래 물질과 다를 수 있습니다. 주의 - 이 표준의 사용은 유해한 물질, 작업 및 장비를 포함할 수 있습니다. 이 표준은 사용에 관련된 모든 안전 문제를 다루지 않습니다. 이 표준의 사용자는 적절한 안전 및 보건 관행을 확립하고 규제 제한의 적용 가능성을 판단하기 전에 이 표준의 사용에 대한 책임이 있습니다.

記事タイトル: SIST EN 1431:2018 - ビチューメンとビチューメン結合材 - ビチューメンエマルションからの残留バインダーおよび油蒸留物の定量化に関する方法 記事内容: この欧州規格では、ビチューメンエマルション中の残留バインダーと油蒸留物の量を定量的に測定する方法を定めています。この方法は、追加のテストのために残留物と油蒸留物を取得するためにも使用することができます。なお、テストで回収される材料の特性は、特にポリマー改質ビチューメンの場合、元の材料とは異なる場合があります。警告 - この規格の使用には、有害物質、操作、および設備が関与する場合があります。この規格は、使用に関連するすべての安全上の問題については触れていません。この規格の使用者は、適切な安全および衛生慣行を確立し、使用前に規制制限の適用可能性を確認する責任があります。