Coal and coke - Determination of ash

This document specifies a method for the determination of the ash of coal and coke.

Charbon et coke — Détermination des cendres

General Information

Status
Published
Publication Date
12-Jun-2024
Current Stage
6060 - International Standard published
Start Date
13-Jun-2024
Due Date
20-May-2025
Completion Date
13-Jun-2024

Relations

Effective Date
27-May-2023

Overview

ISO 1171:2024 is an internationally recognized standard developed by the International Organization for Standardization (ISO) that specifies the method for the determination of ash content in coal and coke. This fifth edition updates and replaces the previous 2010 edition, bringing editorial clarity and alignment with ISO 80000-1 standards. The precise measurement of ash is essential for evaluating the quality and combustion properties of coal and coke, which are critical factors in the energy, metallurgy, and manufacturing sectors.

Key Topics

  • Scope: Defines the standardized procedure to measure ash residue after incineration of coal and coke samples.
  • Principle: Coal or coke samples are heated in air to 815 °C ± 10 °C until a constant mass of ash remains, representing the inorganic mineral residue.
  • Sample Preparation: Samples must be finely ground to a nominal top size of 212 µm and moisture-equilibrated, following ISO sampling protocols.
  • Apparatus:
    • Analytical balance with 0.1 mg precision
    • Furnaces capable of controlled air changes and accurate temperature profiles
    • Silica, porcelain, or platinum dishes for sample containment
    • Desiccators for controlled cooling to avoid moisture absorption
  • Procedure:
    • Heat samples gradually to 500 °C with hold times (30-60 minutes depending on coal type)
    • Continue heating to 815 °C for at least 60 minutes for complete incineration
    • Cool samples in a desiccator before weighing ash residue
  • Result Expression: Ash content is expressed as a percentage mass fraction on an air-dry basis, calculated from precise mass measurements.
  • Precision Criteria: Specifies repeatability and reproducibility limits ensuring consistent and reliable results across laboratories.
  • Test Reporting: Requires clear documentation including sample identification, method reference, test date, and analytical results.

Applications

ISO 1171:2024 is essential for industries relying on coal and coke, providing standardized ash determination critical for:

  • Energy Production: Assessing fuel quality and combustion efficiency in thermal power plants.
  • Metallurgical Processes: Monitoring coke quality for blast furnaces and steel manufacturing.
  • Environmental Compliance: Determining ash content helps estimate mineral contaminants and emissions.
  • Quality Control: Facilitates consistent material specifications and batch verification in mining and fuel supply chains.
  • Research and Development: Supports studies on coal properties and combustion characteristics for improved energy solutions.

Related Standards

  • ISO 1213-2: Vocabulary for solid mineral fuels including sampling and testing terms.
  • ISO 1170: Coal and coke - Calculation of analyses to different bases, which complements ash content reporting.
  • ISO 13909-4 and ISO 13909-6: Mechanical sampling and preparation of test samples for hard coal and coke.
  • ISO 18283: Manual sampling method for coal and coke ensuring representative sampling prior to analysis.

By following ISO 1171:2024, laboratories and industries worldwide achieve accurate, reproducible determination of ash in coal and coke, underpinning quality assurance and regulatory compliance. This standard is vital for optimizing fuel use, minimizing environmental impact, and supporting the global coal and coke market with reliable analytical data.

Standard

ISO 1171:2024 - Coal and coke — Determination of ash Released:13. 06. 2024

English language
4 pages
sale 15% off
Preview
sale 15% off
Preview

Frequently Asked Questions

ISO 1171:2024 is a standard published by the International Organization for Standardization (ISO). Its full title is "Coal and coke - Determination of ash". This standard covers: This document specifies a method for the determination of the ash of coal and coke.

This document specifies a method for the determination of the ash of coal and coke.

ISO 1171:2024 is classified under the following ICS (International Classification for Standards) categories: 75.160.10 - Solid fuels. The ICS classification helps identify the subject area and facilitates finding related standards.

ISO 1171:2024 has the following relationships with other standards: It is inter standard links to ISO 1171:2010. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase ISO 1171:2024 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of ISO standards.

Standards Content (Sample)


International
Standard
ISO 1171
Fifth edition
Coal and coke — Determination of ash
2024-06
Charbon et coke — Détermination des cendres
Reference number
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 1
6 Preparation of test sample . 2
7 Procedure . 2
7.1 General .2
7.2 Ash determination.2
8 Expression of results . 2
9 Precision . 3
9.1 Repeatability limit .3
9.2 Reproducibility limit .3
10 Test report . 3
Bibliography . 4

iii
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee
has been established has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely
with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are described
in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types
of ISO document should be noted. This document was drafted in accordance with the editorial rules of the
ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use of (a)
patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed patent
rights in respect thereof. As of the date of publication of this document, ISO had not received notice of (a)
patent(s) which may be required to implement this document. However, implementers are cautioned that
this may not represent the latest information, which may be obtained from the patent database available at
www.iso.org/patents. ISO shall not be held responsible for identifying any or all such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions
related to conformity assessment, as well as information about ISO's adherence to the World Trade
Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 27, Coal and coke, Subcommittee SC 5, Methods
of analysis.
This fifth edition cancels and replaces the fourth edition (ISO 1171:2010), which has been technically
revised.
The main changes are as follows:
— title and references changed to be consistent with the new name of ISO/TC 27
— editorial updates to be in line with ISO 80000-1
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.

iv
ISO 1171:2
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

Loading comments...