Carbonaceous materials used in the production of aluminium - Calcined coke - Determination of particle size distribution

ISO 12984:2018 specifies a method for the determination of the particle size distribution of a sample of coke having a typical size distribution as normally produced by calcination of delayed petroleum coke. The same procedure is applicable to consignments of calcined anthracite. This document does not apply to fractions of carbon material prepared by sieving and crushing or to filter fines. This method is applicable to the determination of particle sizes ranging from 0,25 mm to 16 mm, as the sum of the percentages of the size distribution above and below this range is typically less than 10 %. This document does not apply to determining particle sizes below 0,25 mm where a specific test for dust is used.

Produits carbonés utilisés pour la production de l'aluminium — Coke calciné — Détermination de la granulométrie

General Information

Status
Published
Publication Date
21-Feb-2018
Current Stage
9093 - International Standard confirmed
Start Date
02-May-2024
Completion Date
13-Dec-2025

Relations

Effective Date
04-Nov-2015

Overview

ISO 12984:2018 establishes a standardized method for determining the particle size distribution of calcined coke used in aluminium production. This international standard applies specifically to coke derived from the calcination of delayed petroleum coke and is also suitable for calcined anthracite consignments. It defines procedures to measure particle sizes ranging between 0.25 mm and 16 mm, which represent the typical size range for such materials in industrial settings. The standard excludes the analysis of carbon fractions prepared through sieving and crushing, and does not cover particle sizes below 0.25 mm, where specialized dust testing methods are employed.

This method is essential for ensuring consistency and quality control in coke materials, which directly affect aluminium production efficiency and furnace performance. Developed by ISO Technical Committee ISO/TC 226, the document provides a rigorous approach involving dry sieve analysis to quantify the mass distribution of coke particles across specified sieve sizes.

Key Topics

  • Scope and Applicability
    Focuses on calcined petroleum coke and anthracite used in aluminium manufacturing, covering particle sizes between 0.25 mm and 16 mm.

  • Sample Preparation and Handling
    Emphasizes the importance of representative sampling consistent with ISO 6375, maintaining particle integrity during drying and handling to avoid altering size distribution.

  • Apparatus and Materials
    Utilizes a nest of wire cloth test sieves with openings of 16, 8, 4, 2, 1, 0.5, and 0.25 mm, compliant with ISO 565 and ISO 3310-1. A batch-type sieve shaker ensures efficient sieving with minimal particle breakage.

  • Procedure Details

    1. Dry the sample at 110°C until mass stability is reached.
    2. Weigh the test portion accurately to 0.1%.
    3. Assemble sieves in descending order; transfer the sample to the top sieve.
    4. Perform sieving using mechanical shaker for 10 minutes, then extend as necessary based on mass consistency criteria.
    5. Record mass retained on each sieve; check for overloading to ensure accuracy.
  • Calculation and Reporting
    Calculate the percentage of material retained by each sieve and cumulative mass fractions, reporting results with precision. Loss in mass during testing must be under 1% to validate results.

  • Precision and Repeatability
    Repeatability of particle size measurements within the 20%-80% cumulative range is ±3% absolute, and ±2% outside this range. Laboratory-to-laboratory reproducibility is not specified due to sample transport risks.

  • Documentation Requirements
    The test report includes sample identification, reference to ISO 12984:2018, test results, procedural deviations, unusual observations, and test date.

Applications

ISO 12984:2018 is crucial for:

  • Quality control in aluminium smelting operations
    Ensuring coke feedstock meets precise particle size requirements to optimize anode quality and furnace efficiency.

  • Supplier and buyer material verification
    Harmonizing particle size specifications across producers and consumers to prevent material rejection and production issues.

  • Research and development
    Facilitating investigation into the impact of coke particle size on electrochemical performance and process optimization.

  • Regulatory compliance
    Providing a recognized benchmark for material characterization within the carbonaceous materials and aluminium production industries.

Related Standards

  • ISO 6375 – Carbonaceous materials for aluminium production: Sampling of coke for electrodes
  • ISO 565 – Test sieves: Metal wire cloth and perforated metal plate: Nominal sizes of openings
  • ISO 3310-1 – Test sieves: Technical requirements and testing (metal wire cloth sieves)

These standards complement ISO 12984:2018 by defining sampling protocols and the specifications for test sieves essential for implementing the particle size distribution method effectively.


Using ISO 12984:2018 for calcined coke particle sizing supports consistent, reliable material evaluation, enhancing process control and product quality in the aluminium industry. By adhering to this standardized method, stakeholders ensure that material characteristics meet operational demands and regulatory expectations.

Standard

ISO 12984:2018 - Carbonaceous materials used in the production of aluminium — Calcined coke — Determination of particle size distribution Released:2/22/2018

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Frequently Asked Questions

ISO 12984:2018 is a standard published by the International Organization for Standardization (ISO). Its full title is "Carbonaceous materials used in the production of aluminium - Calcined coke - Determination of particle size distribution". This standard covers: ISO 12984:2018 specifies a method for the determination of the particle size distribution of a sample of coke having a typical size distribution as normally produced by calcination of delayed petroleum coke. The same procedure is applicable to consignments of calcined anthracite. This document does not apply to fractions of carbon material prepared by sieving and crushing or to filter fines. This method is applicable to the determination of particle sizes ranging from 0,25 mm to 16 mm, as the sum of the percentages of the size distribution above and below this range is typically less than 10 %. This document does not apply to determining particle sizes below 0,25 mm where a specific test for dust is used.

ISO 12984:2018 specifies a method for the determination of the particle size distribution of a sample of coke having a typical size distribution as normally produced by calcination of delayed petroleum coke. The same procedure is applicable to consignments of calcined anthracite. This document does not apply to fractions of carbon material prepared by sieving and crushing or to filter fines. This method is applicable to the determination of particle sizes ranging from 0,25 mm to 16 mm, as the sum of the percentages of the size distribution above and below this range is typically less than 10 %. This document does not apply to determining particle sizes below 0,25 mm where a specific test for dust is used.

ISO 12984:2018 is classified under the following ICS (International Classification for Standards) categories: 71.100.10 - Materials for aluminium production. The ICS classification helps identify the subject area and facilitates finding related standards.

ISO 12984:2018 has the following relationships with other standards: It is inter standard links to ISO 12984:2000. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase ISO 12984:2018 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of ISO standards.

Standards Content (Sample)


INTERNATIONAL ISO
STANDARD 12984
Second edition
2018-02
Carbonaceous materials used in the
production of aluminium — Calcined
coke — Determination of particle size
distribution
Produits carbonés utilisés pour la production de l'aluminium — Coke
calciné — Détermination de la granulométrie
Reference number
©
ISO 2018
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
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CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 2
6 Sampling and preparation of test portion . 2
7 Procedure. 2
8 Expression of results . 3
9 Precision . 4
9.1 Repeatability . 4
9.2 Reproducibility . 4
10 Test report . 4
Foreword
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bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
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any patent rights identified during the development of the document will be in the Introduction and/or
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URL: www .iso .org/ iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 226, Materials for the production of
primary aluminium.
This second edition cancels and replaces the first edition, ISO 12984:2000, of which it constitutes a
minor revision.
iv © ISO 2018 – All rights reserved

INTERNATIONAL STANDARD ISO 12984:2018(E)
Carbonaceous materials used in the production of
aluminium — Calcined coke — Determination of particle
size distribution
1 Scope
This document specifies a method for the determination of the particle size distribution of a sample of
coke having a typical size distribution as normally produced by calcination of delayed petroleum coke.
The same procedure is applicable to consignments of calcined anthracite. This document does not apply
to fractions of carbon material prepared by sieving and crushing or to filter fines.
This method is applicable to the determination of particle sizes ranging from 0,25 mm to 16 mm, as the
sum of the percentages of the size distribution above and below this range is typical
...

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