Rubber - Determination of adhesion to rigid materials using conical shaped parts

This document specifies a method for the determination of the static vulcanized adhesion strength of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by a cylinder of rubber. The adhesion is obtained by a bonding system which can include not only the rigid material and the rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a single cement or both primer and cover cements. The bonding system for preparing the test pieces should be adequately specified by the user, but a provision is made in this document for the evaluation of different types of failure related to a complex bonding system. The method is designed primarily for test pieces prepared in the laboratory under standard conditions in order to provide data for development and control of bonding systems and their components, such as cements or special rubber compounds, and of methods of manufacture. While intended to be applied where the rubber is bonded to rigid supporting pieces, it can be inapplicable such cases where the support, although of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case of rubber bonded to metal wires, cords or thin sheets.

Caoutchouc — Détermination de l'adhérence aux matériaux rigides au moyen de pièces coniques

General Information

Status
Published
Publication Date
21-Apr-2024
Current Stage
6060 - International Standard published
Start Date
22-Apr-2024
Due Date
04-May-2025
Completion Date
22-Apr-2024
Ref Project

Relations

Overview

ISO 5600:2024 specifies a laboratory method to determine the static vulcanized adhesion strength of rubber compounds to rigid materials using test pieces with conical shaped parts. The standard covers preparation, conditioning, testing and reporting of a bonded assembly made from two rigid conical ends joined by a rubber cylinder. It is intended primarily for development and quality control of bonding systems (adhesives, primers, cover cements, coatings, surface treatments) and for assessing adhesion performance of rubber-to-metal or other rigid substrates.

Key topics and requirements

  • Test geometry: Standard test piece formed by two rigid cylindrical parts with opposite conical ends bonded to a rubber cylinder. Key dimensions:
    • Diameter: (25 ± 0.5) mm
    • Distance between cone tips: (12 ± 1) mm
    • Cone half-angle: (45 ± 1)°
    • Tip radius: ≤ 0.8 mm
  • Apparatus:
    • Tensile-testing machine conforming to ISO 5893:2019, class 1, with traverse rate (50 ± 5) mm/min.
    • Low-inertia dynamometers (electronic/optical) are preferred to avoid inertial error.
    • Fixtures that permit accurate centring of the load.
  • Preparation and conditioning:
    • Surface cleaning, specified primer/cover cement application and vulcanization in a transfer mould under specified time, temperature and pressure.
    • Condition test pieces per ISO 23529 for at least 16 h at (23 ± 2) °C or (27 ± 2) °C.
    • Minimum of three test pieces per series.
  • Procedure & results:
    • Record maximum force (newtons) causing rupture.
    • Report adhesion values and classify failure modes using codes: R (rubber bulk), RC (rubber/cover cement), CP (cover cement/primer), M (metal/primer). Each code accompanied by percentage of conical surface involved (nearest 5%).
  • Calibration & traceability:
    • Calibrate equipment according to Annex A and ISO 18899 guidance; maintain inspection and calibration records.

Practical applications and users

ISO 5600:2024 is used by:

  • Rubber compound formulators and adhesive manufacturers to evaluate bonding systems and optimize primers/cover cements.
  • Quality control and R&D laboratories in tyre, hose, automotive, aerospace and industrial elastomer manufacturing.
  • Manufacturers of rubber-to-metal assemblies and converters verifying process reproducibility and adhesion specifications. Practical benefits include standardized comparison of bonding systems, troubleshooting delamination modes, and data for process control and product specifications. Note: the method may be inapplicable where the rigid support has low rigidity due to small transverse dimensions (e.g., thin wires, cords, thin sheets).

Related standards

  • ISO 5893:2019 - Rubber and plastics test equipment (tensile machines)
  • ISO 18899:2013 - Guide to calibration of test equipment
  • ISO 23529 - Preparing and conditioning rubber test pieces

Keywords: ISO 5600:2024, rubber adhesion test, conical shaped parts, vulcanized adhesion strength, bonding system evaluation, adhesion failure types, tensile-testing machine.

Standard
ISO 5600:2024 - Rubber — Determination of adhesion to rigid materials using conical shaped parts Released:22. 04. 2024
English language
7 pages
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Frequently Asked Questions

ISO 5600:2024 is a standard published by the International Organization for Standardization (ISO). Its full title is "Rubber - Determination of adhesion to rigid materials using conical shaped parts". This standard covers: This document specifies a method for the determination of the static vulcanized adhesion strength of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by a cylinder of rubber. The adhesion is obtained by a bonding system which can include not only the rigid material and the rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a single cement or both primer and cover cements. The bonding system for preparing the test pieces should be adequately specified by the user, but a provision is made in this document for the evaluation of different types of failure related to a complex bonding system. The method is designed primarily for test pieces prepared in the laboratory under standard conditions in order to provide data for development and control of bonding systems and their components, such as cements or special rubber compounds, and of methods of manufacture. While intended to be applied where the rubber is bonded to rigid supporting pieces, it can be inapplicable such cases where the support, although of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case of rubber bonded to metal wires, cords or thin sheets.

This document specifies a method for the determination of the static vulcanized adhesion strength of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by a cylinder of rubber. The adhesion is obtained by a bonding system which can include not only the rigid material and the rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a single cement or both primer and cover cements. The bonding system for preparing the test pieces should be adequately specified by the user, but a provision is made in this document for the evaluation of different types of failure related to a complex bonding system. The method is designed primarily for test pieces prepared in the laboratory under standard conditions in order to provide data for development and control of bonding systems and their components, such as cements or special rubber compounds, and of methods of manufacture. While intended to be applied where the rubber is bonded to rigid supporting pieces, it can be inapplicable such cases where the support, although of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case of rubber bonded to metal wires, cords or thin sheets.

ISO 5600:2024 is classified under the following ICS (International Classification for Standards) categories: 83.060 - Rubber. The ICS classification helps identify the subject area and facilitates finding related standards.

ISO 5600:2024 has the following relationships with other standards: It is inter standard links to ISO 5600:2017. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase ISO 5600:2024 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of ISO standards.

Standards Content (Sample)


International
Standard
ISO 5600
Sixth edition
Rubber — Determination of
2024-04
adhesion to rigid materials using
conical shaped parts
Caoutchouc — Détermination de l'adhérence aux matériaux
rigides au moyen de pièces coniques
Reference number
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 2
6 Calibration . 2
7 Test piece . 2
7.1 Form and dimensions .2
7.2 Materials .2
7.3 Preparation .3
7.4 Number of test pieces .3
7.5 Conditioning of test pieces .4
8 Procedure . 4
9 Expression of results . 4
9.1 Adhesion value.4
9.2 Type of adhesion failure .4
10 Salvaging of bonded metal parts . 4
11 Test report . 5
Annex A (normative) Calibration schedule . 6

iii
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee
has been established has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely
with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are described
in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types
of ISO document should be noted. This document was drafted in accordance with the editorial rules of the
ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use of (a)
patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed patent
rights in respect thereof. As of the date of publication of this document, ISO had not received notice of (a)
patent(s) which may be required to implement this document. However, implementers are cautioned that
this may not represent the latest information, which may be obtained from the patent database available at
www.iso.org/patents. ISO shall not be held responsible for identifying any or all such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions
related to conformity assessment, as well as information about ISO’s adherence to the World Trade
Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 45, Rubber and rubber products, Subcommittee
SC 2, Testing and analysis.
This sixth edition cancels and replaces the fifth edition (ISO 5600:2017), which has been technically revised.
The main changes are as follows:
— the normative references have been updated in Clause 2, Clause 5 and Table A.1;
— the class of tensile-testing machine has been upgraded from class 2 to class 1 in Clause 5;
— the expression of the type of adhesion failure has been changed in 9.2.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.

iv
International Standard ISO 5600:2024(en)
Rubber — Determination of adhesion to rigid materials using
conical shaped parts
WARNING 1 — Persons using this document should be familiar with normal laboratory practice. This
document does not purport to address all of the safety problems, if any, associated with its use. It is
the responsibility of the user to establish appropriate safety and health practices and to determine
the applicability of any other restrictions.
WARNING 2 — Certain procedures specified in this document can involve the use or generation of
substances, or the generation of waste, that could constitute a local environmental hazard. Reference
should be made to appropriate documentation on safe handling and disposal after use.
1 Scope
This document specifies a method for the determination of the static vulcanized adhesion strength of rubber
compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by
a cylinder of rubber.
The adhesion is obtained by a bonding system which can include not only the rigid material and the rubber
compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a
single cement or both primer and cover cements. The bonding system for preparing the test pieces should
be adequately specified by the user, but a provision is made in this document for the evaluation of different
types of failure related to a complex bonding system.
The method is designed primarily for test pieces prepared in the laboratory under standard conditions
in order to provide data for development and control of bonding systems and their components, such as
cements or special rubber compounds, and of methods of manufacture. While intended to be applied where
the rubber is bonded to rigid supporting pieces, it can be inapplicable such cases where the support, although
of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case of rubber
bonded to metal wires, cords or thin sheets.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes
requirements of this document. For dated references, only the edition cited applies. For undated references,
the latest edition of the referenced document (including any amendments) applies.
ISO 5893:2019, Rubber and plastics test equipment — Tensile, flexural and compression types (constant rate of
traverse) — Specification
ISO 18899:2013, Rubber — Guide to the calibration of test equipment
ISO 23529, Rubber — General procedures for preparing and conditioning test pieces for physical test methods
3 Terms and definitions
No terms and definitions are l
...

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