ISO 12985-1:2018

Overview

ISO 12985-1:2018 is an international standard developed by ISO that specifies a dimensions method for determining the apparent density of carbonaceous materials used in aluminium production, specifically baked anodes and cathode blocks. This standard covers procedures for samples with simple or well-defined geometries such as cylindrical, rectangular parallelepiped, or cubic shapes with smooth surfaces.

The determination of apparent density using this method is critical for quality control in aluminium manufacturing, impacting the physical properties and performance of carbonaceous materials during smelting. Precise sampling and measurement techniques are essential to ensure accurate and reproducible density values, reflecting the material's compactness and integrity.

Key Topics

• Scope and Application
  Applicable to carbonaceous products with defined geometry and smooth surfaces used in aluminium electrolysis.

• Sampling Procedures
  Samples must be taken according to ISO 8007 series (ISO 8007-1 for cathode blocks and ISO 8007-2 for prebaked anodes) to guarantee representativeness.

• Measurement Equipment

  • Precision balance: Accuracy depends on sample weight, 0.1 g resolution for samples over 100 g, 0.01 g otherwise.
  • Callipers: Measuring to 0.05 mm or 0.01 mm depending on dimension size.

• Measurement Procedure
  Includes multiple dimension measurements of the sample to calculate volume, drying the specimen to constant mass (commonly at 110 ± 5 °C), and weighing under controlled conditions.

• Calculation Method
  Apparent density is calculated using the formula:
  [ \rho_a = \frac{m}{V} ]
  where ( m ) is the dry mass in grams and ( V ) is the sample volume in cubic centimeters (cm³). Results are reported to three decimal places.

• Precision and Reproducibility

  • Repeatability limit: 0.004 g/cm³
  • Reproducibility limit: 0.008 g/cm³
    These values ensure consistency of measurements within and across laboratories.

• Test Reporting Requirements
  Test reports must include sample identification, reference to the ISO standard, method description, test date, results, any deviations or unusual observations.

Applications

• Quality Control in Aluminium Industry
  Ensures carbonaceous baked anodes and cathode blocks meet density specifications critical for efficient electrolysis and operational lifespan.

• Material Development and Research
  Supports R&D in improving carbonaceous product manufacturing by providing a reliable density determination technique.

• Process Monitoring
  Assists in monitoring density variations that could indicate defects or inconsistencies in production batches.

• Supplier and Customer Compliance
  Enables benchmarks for verifying compliance with contractual and regulatory quality requirements in supply chains.

Related Standards

• ISO 8007-1 & ISO 8007-2
  Standards for sampling cathode blocks and prebaked anodes, respectively, complementing the density determination process.

• ISO 5725 Series
  Covers accuracy (trueness and precision) of measurement methods, providing foundational principles related to repeatability and reproducibility referenced in ISO 12985-1.

• ISO/IEC Directives, Part 1 & 2
  Editorial and procedural rules are important for document preparation and maintenance.

Keywords: ISO 12985-1:2018, carbonaceous materials, aluminium production, baked anodes, cathode blocks, apparent density, dimensions method, density determination, aluminium electrolysis, quality control, sample measurement, precision, reproducibility, ISO standards.