Dielectric and resistive properties of solid insulating materials - Part 3-4: Determination of resistive properties (DC methods) - Volume resistance and volume resistivity at elevated temperatures

IEC 62631-3-4:2019 covers procedures for the determination of insulation resistance and volume resistivity of insulating materials by applying DC-voltage and temperatures up to 800 °C. The typical application materials include high temperature mica plate and alumina ceramics.
This edition of IEC 62631-3-4 cancels and replaces IEC 60345 “Method of test for electrical resistance and resistivity of insulating materials at elevated temperatures”, published in 1971. This edition constitutes a technical revision.
This edition includes the following significant technical changes with respect to IEC 60345:  
The revised standard becomes part of the series IEC 62631-3-x. Title of the standard is changed and adapted to the series as Part 3-4.
Clauses 2 "Normative references", 3 "Terms and definitions", and 4 "Significance" are added.
Subclauses 5.2 "Power supply, Voltage", 5.3.1.2 "Number of test specimens" and 5.3.1.3 "Conditioning and pre-treatment of test specimens" are added.
In 5.3.5 "Special precautions during measurements", errors analysis in the measurement of current are modified, and aligned with IEC 62631-3-1.
In 6.2 "Increasing the temperature by steps (method B)", the method for more than one specimen is removed.
The standard atmospheric conditions for testing and conditioning, especially the temperature, are replaced according to IEC 60212.
The circuit diagram of test apparatus is modified, and the structure diagram and pictures of test apparatus are added in Annex A.
The orders of part clauses are adjusted.

Propriétés diélectriques et résistives des matériaux isolants solides - Partie 3-4: Détermination des propriétés résistives (méthodes en courant continu) - Résistance transversale et résistivité transversale aux températures élevées

L'IEC 62631-3-4:2019 couvre les procédures de détermination de la résistance d'isolement et de la résistivité transversale des matériaux isolants en appliquant une tension continue et des températures jusqu'à 800°C. Les matériaux d'application classiques incluent les plaques de mica et les céramiques d'alumine haute température.
La présente édition de l'IEC 62631-3-4 annule et remplace l'IEC 60345 "Méthode d'essai pour la résistance d'isolement et la résistivité transversale des matériaux isolants à des températures élevées", parue en 1971. Cette édition constitue une révision technique.
Cette édition inclut les modifications techniques majeures suivantes par rapport à l'IEC 60345:  
La norme révisée devient une partie de la série IEC 62631-3-x. Le titre de la norme a été modifié et adapté à la série en tant que Partie 3-4.
L'Article 2 "Références normatives", l'Article 3 "Termes et définitions" et l'Article 4 "Signification" ont été ajoutés.
Le Paragraphe 5.2 "Alimentation et tensions d'essai", le Paragraphe 5.3.1.2 "Nombre d'éprouvettes d'essai" et le Paragraphe 5.3.1.3 "Conditionnement et prétraitement de l'éprouvette d'essai" ont été ajoutés.
En 5.3.5 "Précautions particulières à prendre pendant les mesurages", les erreurs d'analyse dans le mesurage du courant sont modifiées et alignées sur l'IEC 62631-3-1.
En 6.2 "Élévation de la température par échelons (méthode B)", la méthode pour plusieurs éprouvettes a été retirée.
Les conditions atmosphériques normales pour l'essai et le conditionnement (en particulier la température) ont été remplacées conformément à l'IEC 60212.
Le schéma des circuits de l'appareillage d'essai a été modifié, et le schéma structurel et les images de l'appareillage d'essai ont été ajoutés à l'Annexe A.
L'ordre des articles de la partie a été ajusté.

General Information

Status
Published
Publication Date
27-Mar-2019
Current Stage
PPUB - Publication issued
Start Date
25-Apr-2019
Completion Date
28-Mar-2019
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IEC 62631-3-4:2019 - Dielectric and resistive properties of solid insulating materials - Part 3-4: Determination of resistive properties (DC methods) - Volume resistance and volume resistivity at elevated temperatures
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IEC 62631-3-4 ®
Edition 1.0 2019-03
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
colour
inside
Dielectric and resistive properties of solid insulating materials –
Part 3-4: Determination of resistive properties (DC methods) – Volume
resistance and volume resistivity at elevated temperatures

Propriétés diélectriques et résistives des matériaux isolants solides –
Partie 3-4: Détermination des propriétés résistives (méthodes en courant
continu) – Résistance transversale et résistivité transversale aux températures
élevées
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IEC 62631-3-4 ®
Edition 1.0 2019-03
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
colour
inside
Dielectric and resistive properties of solid insulating materials –

Part 3-4: Determination of resistive properties (DC methods) – Volume

resistance and volume resistivity at elevated temperatures

Propriétés diélectriques et résistives des matériaux isolants solides –

Partie 3-4: Détermination des propriétés résistives (méthodes en courant

continu) – Résistance transversale et résistivité transversale aux températures

élevées
INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
INTERNATIONALE
ICS 17.220.99; 29.035.01 ISBN 978-2-8322-6688-5

– 2 – IEC 62631-3-4:2019 © IEC 2019
CONTENTS
FOREWORD . 3
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Significance . 6
5 Method of test . 6
5.1 General . 6
5.2 Power supply and test voltages . 6
5.3 Equipment . 6
5.3.1 Specimens and electrodes . 6
5.3.2 Heating chamber . 7
5.3.3 Measuring leads . 7
5.3.4 Temperature control . 7
5.3.5 Special precautions during measurements . 8
5.4 Calibration . 8
6 Procedure . 8
6.1 Continuously increasing temperature (method A) . 8
6.2 Increasing the temperature by steps (method B) . 8
6.3 Precautions to be taken . 9
6.4 Calculation of volume resistivity . 9
7 Report . 9
Annex A (informative) Principle of test apparatus . 11
Bibliography . 14

Figure A.1 – Circuit diagram of test apparatus . 11
Figure A.2 – Structure diagram of test apparatus . 12
Figure A.3 – Pictures of test apparatus . 13

INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
DIELECTRIC AND RESISTIVE PROPERTIES OF SOLID
INSULATING MATERIALS –
Part 3-4: Determination of resistive properties (DC methods) –
Volume resistance and volume resistivity at elevated temperatures

FOREWORD
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International Standard IEC 62631-3-4 has been prepared by IEC technical committee 112:
Evaluation and qualification of electrical insulating materials and systems.
This edition of IEC 62631-3-4 cancels and replaces IEC 60345 “Method of test for electrical
resistance and resistivity of insulating materials at elevated temperatures”, published in 1971.
This edition constitutes a technical revision.
This edition includes the following significant technical changes with respect to IEC 60345:
a) The revised standard becomes part of the series IEC 62631-3-x. Title of the standard is
changed and adapted to the series as Part 3-4.
b) Clauses 2 "Normative references", 3 "Terms and definitions", and 4 "Significance" are
added.
– 4 – IEC 62631-3-4:2019 © IEC 2019
c) Subclauses 5.2 "Power supply, Voltage", 5.3.1.2 "Number of test specimens" and 5.3.1.3
"Conditioning and pre-treatment of test specimens" are added.
d) In 5.3.5 "Special precautions during measurements", errors analysis in the measurement
of current are modified, and aligned with IEC 62631-3-1.
e) In 6.2 "Increasing the temperature by steps (method B)", the method for more than one
specimen is removed.
f) The standard atmospheric conditions for testing and conditioning, especially the
temperature, are replaced according to IEC 60212.
g) The circuit diagram of test apparatus is modified, and the str
...

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