Method for the determination of the proof and the comparative tracking indices of solid insulating materials

IEC 60112:2025 specifies the method of test for the determination of the proof and comparative tracking indices of solid insulating materials on pieces taken from parts of equipment and on plaques of material using alternating voltage. This document provides a procedure for the determination of erosion when required. The proof tracking index is used as an acceptance criterion as well as a means for the quality control of materials and fabricated parts. The comparative tracking index is mainly used for the basic characterization and comparison of the properties of materials. This test method evaluates the composition of the material as well as the surface of the material being evaluated. Both the composition and surface condition directly influence the results of the evaluation and are considered when using the results in material selection process. The described test method is designed for a test voltage up to 600 V AC, because higher test voltages and DC voltage will lead to a reduced test severity. Test results are not directly suitable for the evaluation of safe creepage distances when designing electrical apparatus. The results of this method have been used for insulation coordination of equipment. It is important that use of these results also considers the overvoltage levels, creepage distances, and establishes the pollution degree to which the product insulation system will be expected to be subjected. This is in compliance with IEC 60664-1. This basic safety publication focusing on a safety test method is primarily intended for use by technical committees in the preparation of safety publications in accordance with the principles laid down in IEC Guide 104 and lSO/lEC Guide 51. One of the responsibilities of a technical committee is, wherever applicable, to make use of basic safety publications in the preparation of its publications. This sixth edition cancels and replaces the fifth edition published in 2020. This edition constitutes a technical revision.
This edition includes the following significant technical changes with respect to the previous edition:
- In 7.3, the term "resistivity" has been replaced by "conductivity".
It has the status of a basic safety publication in accordance with IEC Guide 104.

Méthode de détermination des indices de résistance et de tenue au cheminement des matériaux isolants solides

L'IEC 60112:2025 spécifie la méthode d’essai pour la détermination des indices de résistance et de tenue au cheminement des matériaux isolants solides sur des échantillons prélevés sur des parties d'équipement et des plaques de matériau en utilisant une tension alternative. Il fournit une procédure pour la détermination de la valeur de l’érosion quand cela est exigé. L'indice de tenue au cheminement est utilisé comme critère d'acceptation ainsi que comme critère de contrôle de la qualité des matériaux et parties fabriquées. L'indice de résistance au cheminement est principalement utilisé pour effectuer la comparaison et la caractérisation de base des propriétés des matériaux. Cette méthode d’essai évalue la composition et la surface du matériau soumis à l’essai. La composition et les conditions de surface influencent directement les résultats de l’évaluation et sont prises en considération lors de l’utilisation des résultats au moment de la sélection des matériaux. La méthode d'essai décrite est conçue pour une tension d'essai jusqu'à 600 V en courant alternatif, car des tensions d'essai supérieures et une tension continue conduisent à une moindre sévérité d'essai. Les résultats d’essai tels quels ne sont pas adaptés à l’évaluation des lignes de fuite de sécurité lors de la conception des appareillages électriques. Les résultats de cette méthode ont été utilisés pour la coordination de l'isolement des matériels. Il est important que l’utilisation de ces résultats prenne également en considération les niveaux de surtension et les lignes de fuite et définisse le degré de pollution auquel il est prévu de soumettre le système de l’isolement du produit. Ceci est conforme à l’IEC 60664-1. La présente publication fondamentale de sécurité qui porte essentiellement sur une méthode d'essai de sécurité est principalement destinée à être utilisée par les comités d’études pour l’établissement de leurs publications de sécurité, conformément aux principes exposés dans le Guide IEC 104 et dans le Guide ISO/IEC 51. L'une des responsabilités d'un comité d'études consiste, le cas échéant, à utiliser les publications fondamentales de sécurité dans le cadre de l'élaboration de ses publications. Cette sixième édition annule et remplace la cinquième édition parue en 2020. Cette édition constitue une révision technique.
Cette édition inclut les modifications techniques majeures suivantes par rapport à l'édition précédente:
- Au 7.3, le terme "résistivité" a été remplacé par "conductivité".
Elle a le statut d’une publication fondamentale de sécurité conformément au Guide 104 de l'IEC.

General Information

Status
Published
Publication Date
22-Jun-2025
Current Stage
PPUB - Publication issued
Start Date
23-Jun-2025
Completion Date
04-Jul-2025
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REDLINE IEC 60112:2025 CMV - Method for the determination of the proof and the comparative tracking indices of solid insulating materials Released:23. 06. 2025 Isbn:9782832705353
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IEC 60112 ®
Edition 6.0 2025-06
COMMENTED VERSION
INTERNATIONAL
STANDARD
BASIC SAFETY PUBLICATION
Method for the determination of the proof and the comparative tracking indices
of solid insulating materials
ICS 19.080, 29.035.01 ISBN 978-2-8327-0535-3
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CONTENTS
FOREWORD . 2
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 5
4 Principle . 6
5 Test specimen . 6
6 Test specimen conditioning . 7
6.1 Environmental conditioning . 7
6.2 Test specimen surface state . 7
7 Test apparatus . 7
7.1 Electrodes . 7
7.2 Test circuit . 10
7.3 Test solutions . 11
7.4 Dropping device . 12
7.5 Test specimen support platform . 12
7.6 Electrode assembly installation . 13
7.7 Conditioning chamber . 13
8 Basic test procedure . 13
8.1 General . 13
8.2 Preparation . 13
8.3 Test procedure. 14
9 Determination of erosion. 14
10 Proof tracking index test (PTI) . 14
10.1 Procedure . 14
10.2 Report . 15
11 Determination of comparative tracking index (CTI). 16
11.1 General . 16
11.2 Screening test . 16
11.3 Determination of the maximum 50 drop withstand voltage . 16
11.4 Determination of the 100 drop point . 17
11.5 Report . 18
Annex A (informative) List of factors that should be considered by product committees . 19
Annex B (informative) Solution B . 20
Annex C (informative) Electrode material selection . 21
C.1 Platinum electrodes . 21
C.2 Alternatives . 21
Bibliography . 22
List of comments. 23

Figure 1 – Electrode . 8
Figure 2 – Electrode / and specimen arrangement . 9
Figure 3 – Example of typical electrode mounting and specimen support . 10
Figure 4 – Example of test circuit . 11

INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
Method for the determination of the proof and the comparative tracking
indices of solid insulating materials

FOREWORD
1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising
all national electrotechnical committees (IEC National Committees). The object of IEC is to promote international
co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and
in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports,
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Standardization (ISO) in accordance with conditions determined by agreement between the two organizations.
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8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is
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9) IEC draws attention to the possibility that the implementation of this document may involve the use of (a)
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the latest information, which may be obtained from the patent database available at https://patents.iec.ch. IEC
shall not be held responsible for identifying any or all such patent rights.
This commented version (CMV) of the official standard IEC 60112:2025 edition 6.0 allows
the user to identify the changes made to the previous IEC 60112:2020
edition 5.0. Furthermore, comments from IEC TC 112 experts are provided to explain the
reasons of the most relevant changes, or to clarify any part of the content.
A vertical bar appears in the margin wherever a change has been made. Additions are in
green text, deletions are in strikethrough red text. Experts' comments are identified by a
blue-background number. Mouse over a number to display a pop-up note with the
comment.
This publication contains the CMV and the official standard. The full list of comments is
available at the end of the CMV.

IEC 60112 has been prepared by IEC technical committee 112: Evaluation and qualification of
electrical insulating materials and systems. It is an International Standard.
This sixth edition cancels and replaces the fifth edition published in 2020. This edition
constitutes a technical revision.
This edition includes the following significant technical changes with respect to the previous
edition:
a) In 7.3, the term "resistivity" has been replaced by "conductivity".
It has the status of a basic safety publication in accordance with IEC Guide 104.
The text of this International Standard is based on the following documents:
Draft Report on voting
112/679/FDIS 112/686/RVD
Full information on the voting for its approval can be found in the report on voting indicated in
the above table.
The language used for the development of this International Standard is English.
This document was drafted in accordance with ISO/IEC Directives, Part 2, and developed in
accordance with ISO/IEC Directives, Part 1 and ISO/IEC Directives, IEC Supplement, available
at www.iec.ch/members_experts/refdocs. The main document types developed by IEC are
described in greater detail at www.iec.ch/publications.
The committee has decided that the contents of this document will remain unchanged until the
stability date indicated on the IEC website under webstore.iec.ch in the data related to the
specific document. At this date, the document will be
• reconfirmed,
• withdrawn, or
• revised.
1 Scope
This document specifies the method of test for the determination of the proof and comparative
tracking indices of solid insulating materials on pieces taken from parts of equipment and on
plaques of material using alternating voltage.
This document provides a procedure for the determination of erosion when required.
NOTE 1 The proof tracking index is used as an acceptance criterion as well as a means for the
quality control of materials and fabricated parts. The comparative tracking index is mainly used
for the basic characterization and comparison of the properties of materials. 1
This test method evaluates the composition of the material as well as the surface of the material
being evaluated. Both the composition and surface condition directly influence the results of
the evaluation and are considered when using the results in material selection process.
The described test method is designed for a test voltage up to 600 V AC, because higher test
voltages and DC voltage will lead to a reduced test severity. 2
Test results are not directly suitable for the evaluation of safe creepage distances when
designing electrical apparatus.
NOTE 2 This is in compliance with IEC 60664-1, Insulation coordination for equipment within low-voltage systems –
Part 1: Principles, requirements and tests.
NOTE 3 This test discriminates between materials with relatively poor resistance to tracking, and those with
moderate or good resistance, for use in equipment which can be used under moist conditions. More severe tests of
longer duration are available for the assessment of performance of materials for outdoor use, utilizing higher voltages
and larger test specimens (see the inclined plane test of IEC 60587). Other test methods such as the inclined method
can rank materials in a different order from the drop test given in this document.
The results of this method have been used for insulation coordination of equipment. It is
important that use of these results also considers the overvoltage levels, creepage distances,
and establishes the pollution degree to which the product insulation system will be expected to
be subjected. This is in compliance with IEC 60664-1. 3
This basic safety publication focusing on a safety test method is primarily intended for use by
technical committees in the preparation of safety publications in accordance with the principles
laid down in IEC Guide 104 and lSO/lEC Guide 51.
One of the responsibilities of a technical committee is, wherever applicable, to make use of
basic safety publications in the preparation of its publications.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies.
For undated references, the latest edition of the referenced document (including any
amendments) applies.
ISO 4287, Geometrical Product Specification (GPS) – Surface texture: Profile method – Terms,
definitions and surface texture parameters
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following
addresses:
• IEC Electropedia: available at http://www.electropedia.org
• ISO Online browsing platform: available at http://www.iso.org/obp
3.1
tracking
progressive formation of conducting paths, which are produced on the surface or within a solid
insulating material or both, due to the combined effects of electric stress and electrolytic
contamination
3.2
tracking failure
failure of insulation due to tracking between conductive parts
Note 1 to entry: In the present test, tracking is indicated by operation of an over-current device due to the passage
of a current across the test surface or within the specimen or both.
3.3
electrical erosion
wearing away of insulating material by the action of electrical discharges
3.4
air arc
arc between the electrodes above the surface of the specimen
3.5
comparative tracking index
CTI
numerical value of the maximum voltage (in V) at which five test specimens withstand the test
period for 50 drops without tracking failure and without a persistent flame occurring and
including also a statement relating to the behaviour of the material when tested using 100 drops
(see 11.3)
Note 1 to entry: No tracking failure and no persistant flame are allowed at any lower test voltage.
Note 2 to entry: The criteria for CTI may can 4 also require a statement concerning the degree of erosion.
Note 3 to entry: Although a non-persistent flame is allowed in the test without constituting failure, materials which
generate no flame at all are preferred unless other factors are considered to be more important. See also Annex A.
Note 4 to entry: Some materials can withstand high test voltages, but fail at lower test voltages. See also 11.2.
3.6
persistent flame
flame which burns for more than 2 s
Note 1 to entry: In the present test, persistent flame is indicated by a visual check. 5
3.7
proof tracking index
PTI
numerical value of the proof voltage (in V) at which five test specimens withstand the test period
for 50 drops without tracking failure and without a persistent flame occurring
Note 1 to entry: Although a non-persistent flame is allowed in the test without constituting failure, materials which
generate no flame at all are preferred unless other factors are considered to be more important. See also Annex A.
3.8
de-ionized water
water for analytical laboratory use in accordance with ISO 3696, grade 3, or equivalent quality
4 Principle
The upper surface of the test specimen is supported in a horizontal plane and subjected to an
electrical stress via two electrodes. The surface between the electrodes is subjected to a
succession of drops of electrolyte either until the over-current device operates, or until a
persistent flame occurs, or until the test period has elapsed.
The individual tests are of short duration (less than 1 h) with up to 50 or 100 drops of about
20 mg of electrolyte falling at 30 s intervals between platinum electrodes, 4 mm apart on the
test specimen surface.
An AC voltage between 100 V and 600 V is applied to the electrodes during the test.
During the test, specimens may also erode or soften, thereby allowing the electrodes to
penetrate them. The formation of a hole through the test specimen during a test is to be reported
together with the hole depth (test specimen thickness). Retests may be made using thicker test
specimens, up to a maximum of 10 mm.
NOTE The number of drops needed to cause failure by tracking usually increases with decreasing applied voltage
and, below a critical value, tracking ceases to occur. For some materials, tracking also ceases to occur above an
upper critical value.
5 Test specimen
Any approximately flat surface may be used, provided that the area is sufficient to ensure that
during the test no liquid flows away from the test electrodes.
NOTE 1 In general, flat surfaces of not less than 20 mm × 20 mm are used to reduce the probability of electrolyte
flows away from the test electrodes although smaller sizes can be used, subject to no electrolyte loss, e.g. ISO 3167,
15 mm × 15 mm multi-purpose test specimens.
NOTE 2 In general separate test specimens for each test are used. If several tests are to be made on the same
test piece, testing points can be sufficiently far from each other so that splashes, fumes, or erosion, from the testing
point will not contaminate or influence the other areas to be tested.
The thickness of the test specimen shall be 3 mm or more. Individual pieces of material may be
stacked to obtain the required thickness of at least 3 mm.
NOTE 3 The values of the CTI obtained on specimens with a thickness below 3 mm cannot be comparable with
those obtained on thicker specimens because of greater heat transmission to the glass support through thinner test
specimens. For this reason, stacked specimens are possible.
Test specimens shall have uniformly smooth and untextured surfaces which are free from
surface imperfections such as scratches, blemishes, impurities, etc, unless otherwise stated in
the product standard. If this is impossible, the results shall be reported together with a statement
describing the surface of the specimen because certain characteristics on the surface of the
specimen could can 6 add to the dispersion of the results.
For tests on parts of products, where it is impossible to cut a suitable test specimen from a part
of a product, specimens cut from moulded plaques of the same insulating material may be used.
In these cases, care should be taken to ensure that both the part and the plaque are produced
by the same fabrication process, resulting in the same surface texture, wherever possible.
Where the details of the final fabrication process are unknown, methods given in ISO 293,
ISO 294-1 and ISO 294-3 and ISO 295 may can be appropriate.
NOTE 4 The use of different fabrication conditions/ or 7 processes can lead to different levels of performance in
the PTI and CTI test.
NOTE 5 Parts moulded using different flow directions can also exhibit different levels of performance in the PTI and
CTI test.
In special cases, the test specimen may be ground to obtain a flat surface. In this case, the
surface texture according ISO 4287 (e.g. R values) shall be reported (see 10.2 and 11.5).
z
NOTE 6 Any grinding can damage the specimen. In this case, material surface made by grinding has higher or
lower tracking value than the original surface.
Where the direction of the electrodes relative to any feature of the material is significant,
measurements shall be made in the direction of the feature and orthogonal to it. The direction
giving the lower CTI shall be reported, unless otherwise specified in a contract. 8
NOTE 7 Use of an aggressive electrolyte, such as solution C, is common, when the material has a hydrophobic
surface.
6 Test specimen conditioning
6.1 Environmental conditioning
Unless otherwise specified in a contract 9, the test specimens shall be conditioned for a
minimum of 24 h at (23 ± 5 2) °C 10, with (50 ± 10) % RH. Once the test specimen has been
removed from the conditioning chamber (see 7.7), the test shall be started within 30 minutes.
6.2 Test specimen surface state
Unless otherwise specified in a contract, 11
a) tests shall be made on clean surfaces;
b) any cleaning procedure used shall be reported. Wherever possible, the details shall be
agreed between supplier and customer.
Dust, dirt, fingerprints, grease, oil, mould release or other contaminants can influence the
results. When cleaning the test specimen, swelling, softening, abrasion or other damage to the
material shall be avoided.
7 Test apparatus
7.1 Electrodes
Two electrodes of platinum with a minimum purity of 99 % shall be used (see Annex C). The
two electrodes shall have a rectangular cross-section of (5 ± 0,1) mm × (2 ± 0,1) mm, with one
end chisel-edged with an angle of 30° ± 2° (see Figure 1). The sharp edge shall be removed to
produce an approximately flat surface, 0,01 mm to 0,1 mm wide.
NOTE 1 A microscope with a calibrated eyepiece has been found suitable for checking the size of the end surface.
NOTE 2 In general, mechanical means are used to re-furbish the electrode shape after a test to ensure that the
electrodes maintain the required tolerances, especially with respect to the edges and corners.
5 ±0,1
2 ±0,1
30° ±2°
Flattened edge
0,1
IEC
0 01
Dimensions in millimetres
Key
1 platinum electrode
Figure 1 – Electrode
At the start of the test, the electrodes shall be symmetrically arranged in a vertical plane, the
total angle between them being 60° ± 5° and with opposing electrode faces approximately
vertical on a flat horizontal surface of the test specimen (see Figure 2). Their separation along
the surface of the test specimen at the start of the test shall be (4,0 ± 0,1) mm.
≥ 12
Dimensions in millimetres
Key
1 platinum electrode
2 brass extension (optional)
3 table
4 tip of dropping device
5 specimen
6 glass specimen support
Figure 2 – Electrode/ and 12 specimen arrangement
A thin metal rectangular slip gauge shall be used to check the electrode separation. The
electrodes shall move freely and the force exerted by each electrode on the surface of the test
specimen at the start of the test shall be (1,00 ± 0,05) N. The design shall be such that the
force can be expected to remain at the initial level during the test.
One typical type of arrangement for applying the electrodes to the test specimen is shown in
Figure 3. The force shall be verified at appropriate intervals.
Key
1 platinum electrode
2 brass extension (optional)
3 table
4 tip of dropping device
5 specimen
6 glass specimen support
Figure 3 – Example of typical electrode mounting and specimen support
Where tests are made solely on those materials where the degree of electrode penetration is
small, the electrode force may be generated by the use of springs. However, gravity should be
used to generate the force on general purpose equipment (see Figure 3).
NOTE 3 With most, but not all designs of apparatus, if the electrodes move during a test due to softening or erosion
of the specimen, their tips will prescribe an arc and the electrode gap will change. The magnitude and direction of
the gap change will depend on the relative positions of the electrode pivots and the contact points between electrode/
and specimen contact points 13. The significance of these changes will probably be material dependent and has not
been determined. Differences in design could can 4 give rise to differences in inter-apparatus results.
7.2 Test circuit
The electrodes shall be supplied with a substantially sinusoidal voltage, variable between 100 V
and 600 V at a frequency of 48 Hz to 62 Hz. The voltage measuring device shall indicate a true
RMS value and shall have an accuracy of 1,5 % or better for the reading. The power of the
source shall be not less than 0,6 kVA. An example of a suitable test circuit is shown in Figure 4.
Key
1 switch
2 AC source 100 V to 600 V
3 delay over-current device
4 variable resistor
5 electrodes
6 specimen
Figure 4 – Example of test circuit
A variable resistor shall be capable of adjusting the current between the short-circuited
electrodes to (1,0 ± 0,1) A and the voltage indicated by the voltmeter shall not decrease by
more than 10 % when this current flows. The instrument used to measure the value of the short-
circuit current shall have an accuracy of ±3 % or better for the reading.
NOTE To achieve the tolerance requirement it may can 4 be necessary that the suppply voltage to the apparatus
is sufficiently stable.
The over-current device shall operate when a current with an RMS value of (0,50 ± 0,05) A has
persisted for (2,00 ± 0,20) s.
7.3 Test solutions
Solution A:
Dissolve approximately 0,1 % by mass of analytical reagent grade anhydrous ammonium
chloride (NH Cl), of a purity of not less than 99,8 %, in de-ionized water to give a resistivity of
(3,95 ± 0,05) Ωm conductivity of (253 ± 4) mS/m 14 at (23 ± 1) °C.
NOTE 1 The quantity of ammonium chloride is selected to give a solution in the required range of resistivity
conductivity.
NOTE 2 The conductivity of the solution A at 25 °C is (3,75 ± 0,05) Ωm (264 ± 4) mS/m, and (4,25 ± 0,05) Ωm
(238 ± 3) mS/m at 20 °C.
Solution B:
Description of this solution is given in Annex B (informative).
Solution C:
Dissolve approximately 0,2 % by mass of analytical reagent grade anhydrous ammonium
chloride (NH Cl) 15, of a purity of not less than 99,8 %, and (0,5 ± 0,02) % by mass of a non-
ionic surfactant (t-octylphenoxypolyethoxyethanol, CAS Registry Number 9002-93-1) in de-
ionized water to give a resistivity of (1,98 ± 0,05) Ωm conductivity of (505 ± 15) mS/m 14 at
(23 ± 1) °C and a surface tension of < 40 m N/m according to ISO 304.
NOTE 3 Select the quantity of ammonium chloride to give a solution in the required range of resistivity conductivity,
and the quantity of the surfactant to give a surface tension of the solution in the required range.
NOTE 4 The conductivity of the solution C at 25 °C is (550 ± 15) mS/m, and (450 ± 10) mS/m at 20 °C. 16
Solution A is normally used, but where a more aggressive contaminant is required, solution C
is recommended. To indicate that solution C was used, the CTI or PTI value shall be followed
by the letter "C". The use of solution B may be stipulated for comparability with prior results.
7.4 Dropping device
Drops of the test solution shall fall on to the specimen surface at intervals of (30 ± 5) s. The
drops shall fall approximately centrally between the two contact areas of the electrodes from a
height of (35 ± 5) mm.
The target time between single drops shall be 30 s. The total mass of a sequence of 50 drops
shall lie between 0,997 g and 1,147 g. The total mass of a sequence of 20 drops shall lie
between 0,380 g and 0,480 g.
NOTE 1 The mass of the drops can be determined by weighing with the appropriate laboratory balance.
NOTE 2 The target mass for 50 drops is 1,07 g and for 20 drops it is 0,43 g.
The mass of the drops shall be checked at appropriate time intervals.
NOTE 3 The appropriate time interval depends on the design of the dispensor and can be part of the use instruction
of the laboratory. 17
NOTE 3 4 For solution A, a length of thin walled stainless steel tubing (e.g. hypodermic needle tubing), having an
outer diameter of between 0,9 mm and 1,2 mm, dependent upon the dropping system, has been found to be suitable
for the tip of the dropping device. For solution B and solution C, tubes having outer diameters over the range 0,9 mm
to 3,45 mm have been found to be necessary with the different dropping systems in use.
NOTE 4 5 A drop detector or counter can be used to ascertain whether there are any double drops or whether drops
are missing.
7.5 Test specimen support platform
A glass plate or plates, having a total thickness of not less than 4 mm and of a suitable size
shall be used to support the test specimen during the test.
NOTE 1 In order to avoid the problem of cleaning the specimen support table, it is common that a disposable glass
microscope slide is placed on the specimen support table immediately under the test specimen.
NOTE 2 The use of thin metal foil conductors around the edge of the glass plate to detect electrolyte loss has been
found useful.
7.6 Electrode assembly installation
The specimen and the contacting electrodes shall be mounted in an essentially draught-free
space in a chamber.
NOTE To keep the chamber reasonably free of fumes, it can be necessary, for certain classes of materials, to have
a small air flow across the surface of the test specimen and between the electrodes. An air velocity of the order of
0,2 m/s before the start of the test and as far as possible during the test has been found suitable. The air velocity in
other areas of the chamber can be substantially higher to assist in fume removal. The air velocity can be measured
with an appropriately scaled hot wire anemometer.
A suitable fume extraction system shall be provided to allow safe venting of the chamber after
the test.
7.7 Conditioning chamber
The conditioning chamber shall be maintained for a minimum of 24 h 18 at (23 ± 2) °C and a
relative humidity of (50 ± 10) %.
NOTE Standard conditions for use prior to and during the testing of solid electrical insulating insulation materials 19
are specified in IEC 60212.
8 Basic test procedure
8.1 General
Where the material is substantially anisotropic, tests shall be made in the direction of the
features and orthogonal to them. Results from the direction giving the lower values shall be
used, unless otherwise specified in a contract. 20
Tests shall be made at an ambient temperature of (23 ± 5) °C.
Tests shall be made on uncontaminated test specimens, unless otherwise specified in a
contract. 21
The result of a test where a hole is formed is considered to be valid, irrespective of the test
specimen thickness, but the formation of the hole shall be reported together with the depth of
the hole (the thickness of the test specimen or stack).
8.2 Preparation
After each test, clean the electrodes with an appropriate solvent and then rinse with de-ionized
water and dry them. If necessary, restore their shape, polish if necessary, and give a final rinse
and dry before the next test.
Immediately before the test ensure, if necessary by cooling the electrodes, that their
temperature is sufficiently low so that they have no adverse effect on the specimen properties.
Ensure freedom from visual contamination and ensure that the solution to be used conforms to
the conductivity requirements either by regular testing, or by measurement immediately before
the test.
NOTE 1 Residues on the dropping device from an earlier test will probably contaminate the solution and evaporation
of the solution will increase its concentration – both of which may can 4 result in lower than true values. In such
cases the outside of the dropping device can be cleaned mechanically or with a solvent or both and the inside by
flushing through with conforming solution before each test. Flushing through some 10 to 20 drops depending upon
the delay between tests will normally remove any non-conforming liquid.
In case of dispute, the cleaning procedures used for the electrodes and dropper tube shall be
agreed between purchaser and supplier.
Place the test specimen, with the test surface uppermost and horizontal on the specimen
support table. Adjust the relative height of the test specimen and electrode mounting assembly,
such that on lowering the electrodes on to the specimen, the correct orientation is achieved
with a separation of (4,0 ± 0,1) mm. Ensure that the chisel edges make contact with the surface
of the specimen with the required force and over the full width of the chisel.
NOTE 2 It can be helpful to place a light behind the electrodes when making this check visually.
NOTE 3 The orientation of the specimen should can 4 ensure that the droplet stays between the electrodes.
Set the test voltage to the required value, which shall be an integer multiple of 25 V, and adjust
the circuit parameters so that the short-circuit current is within the permitted tolerance.
8.3 Test procedure
Start the dropping system so that drops fall on to the test surface and continue the test until
one of the following occurs:
a) the over-current device operates;
b) a persistent flame occurs;
c) at least 25 s have elapsed after the fiftieth (hundredth) drop has fallen without a) or b)
occurring.
NOTE If there is no requirement for the determination of erosion, the 100 drop tests can be made ahead of any 50
drop tests.
After completion of the test, vent the chamber of noxious fumes and remove the test specimen.
9 Determination of erosion
When required, specimens which have not failed at the 50 drop point shall be cleaned of any
debris or loosely attached degradation products and placed on the platform of a depth gauge.
The maximum depth of erosion of each specimen shall be measured in millimetres to an
accuracy of 0,1 mm, using a 1,0 mm nominal diameter probe having a hemispherical end. The
result is the maximum of the five measured values.
Erosion depths of less than 1 mm shall be reported as < 1 mm.
In the case of tests according to Clause 10, when required the erosion shall be measured on
the specimens which withstood 50 drops at the specified voltage.
In the case of tests according to Clause 11, when required the erosion shall be measured on
the five specimens tested at the maximum 50 drop voltage.
10 Proof tracking index test (PTI)
10.1 Procedure
Where, in IEC standards for material or for electrical equipment specifications, or in other
standards, a proof test only is required, 50 drop tests shall be made in accordance with Clause 8
but at the single voltage specified.
NOTE 1 The specified PTI voltage is a proof testing on a material or on an end product and that specified voltage
can be derived from full CTI testing according to IEC 60112, but not higher than the established CTI of the material. 22
Operation of the over-current device by air arcs does not constitute a tracking failure.
The minimum required number of specimens is five. If one of five specimens fails at a certain
test voltage, a new set of five samples may be tested unless otherwise specified in a contract 23.
If only one of the total of ten specimens fails, the result is "pass".
NOTE 2 A different number of specimens may can 4 be agreed by manufacturer and user, or defined in product
standards.
The proof voltage shall be an integer multiple of 25 V.
10.2 Report
The report shall include the following information:
a) Identification of the material tested and details of any conditioning.
b) Thickness of the specimens and the number of layers used to achieve this thickness.
c) Nature of the test specimen surface where the original surface was not tested:
1) details of any cleaning process;
2) details of any machining processes, e.g. grinding;
3) details of any coating on the tested specimen.
d) State of the surface before testing, with regard to surface imperfections, e.g. surface
scratches, blemishes, impurities, etc.
e) The cleaning procedure used for the electrodes and dropper.
f) Where the measurements were not made in an essentially draught free space, report on the
approximate air flow rate.
g) Orientation of the electrodes in relation to any known characteristics of the material.
h) Report on the result of the proof tracking index test where there is no requirement for the
determination of the degree of erosion as follows:
– Pass or fail at the specified voltage with an indication of the type of solution if Type C,
or Type B.
EXAMPLE for solution A 'Pass PTI 175', or 'Fail PTI 175'
EXAMPLE for solution B 'Pass PTI 225 M', or 'Fail PTI 225 M'
EXAMPLE for solution C 'Pass PTI 175 C', or 'Fail PTI 175 C'
i) Where there is an erosion requirement the result shall be reported as follows:
il at the specified voltage with an indication of the type of solution if Type C,
– Pass or fa
or Type B, and the maximum depth of erosion being in millimetres. 24
PASS EXAMPLE for solution A 'Pass PTI 250 – 3,0', or 'Fail PTI 250 – 3,0'
PASS EXAMPLE for solution B 'Pass PTI 375 M – 3,0', or 'Fail PTI 375 M – 3,0'
PASS EXAMPLE for solution C 'Pass PTI 250 C – 3,0' or Fail PTI 250 C – 3,0'.
– Where the erosion cannot be reported because the specimen flamed, both shall be
reported.
– Where a hole developed through the specimen, its formation shall be reported together
with an indication of its depth (specimen thickness).
– Where the tests were invalid due to air arcs, this shall be reported.
11 Determination of comparative tracking index (CTI)
11.1 General
Determination of the comparative tracking index requires the determination of the maximum
voltage at which five specimens withstand the test period for 50 drops without failure and
whether, at a voltage of 25 V lower than the maximum 50 drop figure, the specimen withstands
100 drops. If this is not the case, the maximum 100 drop withstand voltage shall be determined.
If one of five specimens fails at a certain test voltage, a new set of five samples may be tested.
If only one of the total of ten specimens fails, this result qualifies for continuing the procedure
with the next higher voltage. The maximum value of the test voltage shall not be associated
with the operating voltage of equipment in which the material to be tested is used. 25
11.2 Screening test
If the behaviour of the material is unknown, 26 A screening test shall start with at least
three specimens at a maximum starting voltage of 300 V with a minimum of 50 drops. If the
material withstands the initial test without tracking failure and without a persistent flame, always
still 27 using three specimens, increase the test voltage by 100 V steps until a tracking failure
or a persistent flame occurs. Then reduce the test voltage by 50 V, and finally increase or
reduce the test voltage by 25 V to identify the maximum test voltage for the determination of
the comparative tracking index.
If the material fails at the initial test voltage, reduce the test voltage by 100 V and follow the
same iterative procedure for the determination of the comparative tracking index, always still 27
using three specimens.
Complete the determination of the comparative tracking index according to the general
procedure, and procedures 11.1, 11.3 and 11.4.
NOTE Any result of the screening test can be used for completing the general procedure to evaluate the CTI value.
This procedure is necessary because some materials can withstand high test voltages, but fails
at lower test voltages.
11.3 Determination of the maximum 50 drop withstand voltage
By inference from the screening data, repeat the test p
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