Paints and varnishes - Determination of non-volatile-matter content and spreading rate of coil coating materials

The method specifies the gravimetric procedure for determining the non-volatile-matter content as a percentage by mass of the majority of thermally cured coil coatings and subsequently for determining the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.

Beschichtungsstoffe - Bestimmung des Gehaltes an nichtflüchtigen Anteilen und der Ergiebigkeit von Bandbeschichtungsstoffen

Die Norm legt die gravimetrische Bestimmung des Gehaltes an nichtflüchtigen Anteilen als Massenanteil in Prozent der Mehrzahl von wärmehärtenden Bandbeschichtungsstoffen mit nachfolgender Bestimmung der theoretischen Ergiebigkeit fest. Das Verfahren ist nicht geeignet für Bandbeschichtungsstoffe, die reine Epoxidharze als Bindemittel enthalten.

Peintures et vernis - Détermination de la teneur en matière non volatile et du rendement superficiel spécifique de revêtements pour prélaquage

La présente méthode décrit le mode opératoire permettant de déterminer par gravimétrie la teneur en matière non volatile en pourcentage en masse de la majorité des revêtements pour prélaquage durcis par traitement thermique, et par conséquent de déterminer le rendement d’application théorique. Cette méthode ne convient pas aux revêtements pour prélaquage en époxy pur.

Barve in laki - Določevanje nehlapnih snovi in razlivnosti premazov za kovine, ki se navijajo

Metoda določa gravimetrični postopek za določanje masnega odstotka nehlapnih snovi večine toplotno strjenih premazov za kovine, ki se navijajo, in nato za teoretično določanje njihove razlivnosti. Metoda ni primerna za čiste epoksi premaze.

General Information

Status
Published
Publication Date
17-Sep-2019
Withdrawal Date
30-Mar-2020
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Start Date
04-Mar-2025
Completion Date
04-Mar-2025

Relations

Effective Date
08-Jun-2022

Overview

EN 16074:2019 is a European standard established by CEN that specifies a gravimetric method for determining the non-volatile matter (NV) content and theoretical spreading rate of coil coating materials, primarily those that are thermally cured. This method provides critical testing guidance for paints and varnishes applied to metals in coil coating processes. Notably, the standard excludes pure epoxy coil coatings from its scope.

The standard was published in 2019, updating the previous 2011 version, and includes improved alignment with international symbols and the addition of procedures such as density determination. Compliance with EN 16074:2019 is mandatory for all CEN member countries, impacting manufacturers, quality controllers, and laboratories involved in coatings testing.

Key Topics

  • Non-volatile matter (NV) content determination
    This is the percentage by mass of solid residues remaining after solvent evaporation and curing of a coil coating material sample. EN 16074:2019 defines procedures to accurately measure this through either the pan method or drawdown method.

  • Theoretical spreading rate calculation
    Based on the measured NV content and densities of the coating and its solvents, the standard prescribes a formula to calculate how much surface area a given weight of coating covers to achieve a 1 µm dry film thickness. This value is essential for estimating material usage and cost-efficiency.

  • Test procedures
    Two main testing approaches are described:

    • Pan Method: Directly drying and curing paint in a pan before weighing the residue.
    • Drawdown Method: Applying paint onto metal panels, curing, and weighing to determine NV content.
  • Density determination
    EN 16074:2019 incorporates density measurements of both the liquid coating material and its solvents, performed according to EN ISO 2811 series standards. This addition enhances accuracy in spreading rate calculations.

  • Specific considerations for PVC plastisols
    Separate prescribed procedures address the unique properties of PVC plastisol coil coatings, emphasizing temperature control and sample handling distinct from other coating types.

Applications

  • Quality control in coil coating production
    Manufacturers use EN 16074:2019 to ensure coating compositions meet specified NV content, which correlates with coating performance and durability.

  • Estimating material coverage and cost
    By reliably calculating the theoretical spreading rate, companies can optimize coating application parameters, improve resource efficiency, and reduce waste.

  • Product development and R&D
    Paint formulators rely on this standard to quantify coatings’ solid content and spreading capabilities during formulation adjustments.

  • Certification and compliance testing
    Laboratories conducting regulatory or customer-specified testing adopt the EN 16074:2019 method to provide standardized and reproducible results across the industry.

  • Supply chain verification
    Buyers and suppliers of coil coatings utilize standardized test results to verify product consistency and quality before acceptance.

Related Standards

  • EN ISO 1513 – Paints and varnishes: Examination and preparation of test samples
  • EN ISO 2811 series (1 to 4) – Paints and varnishes: Methods for determination of density including pycnometer, plummet, oscillation, and pressure cup methods
  • EN ISO 15528 – Sampling of paints, varnishes, and raw materials for coatings
  • EN 13523-0 – Coil coated metals: General introduction and terms

These referenced standards complement EN 16074:2019 by providing necessary sampling, sample preparation, and density measurement techniques integral to the accurate evaluation of coil coating materials.


Keywords: EN 16074:2019, non-volatile matter content, theoretical spreading rate, coil coating materials, gravimetric method, paints and varnishes, coil coating testing, density determination, PVC plastisol coatings, European standard for coatings, coil coating quality control.

Frequently Asked Questions

EN 16074:2019 is a standard published by the European Committee for Standardization (CEN). Its full title is "Paints and varnishes - Determination of non-volatile-matter content and spreading rate of coil coating materials". This standard covers: The method specifies the gravimetric procedure for determining the non-volatile-matter content as a percentage by mass of the majority of thermally cured coil coatings and subsequently for determining the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.

The method specifies the gravimetric procedure for determining the non-volatile-matter content as a percentage by mass of the majority of thermally cured coil coatings and subsequently for determining the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.

EN 16074:2019 is classified under the following ICS (International Classification for Standards) categories: 87.040 - Paints and varnishes. The ICS classification helps identify the subject area and facilitates finding related standards.

EN 16074:2019 has the following relationships with other standards: It is inter standard links to EN 16074:2011. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

You can purchase EN 16074:2019 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of CEN standards.

Standards Content (Sample)


SLOVENSKI STANDARD
01-november-2019
Nadomešča:
SIST EN 16074:2011
Barve in laki - Določevanje nehlapnih snovi in razlivnosti premazov za kovine, ki
se navijajo
Paints and varnishes - Determination of non-volatile-matter content and spreading rate of
coil coating materials
Beschichtungsstoffe - Bestimmung des Gehaltes an nichtflüchtigen Anteilen und der
Ergiebigkeit von Bandbeschichtungsstoffen
Peintures et vernis - Détermination de la teneur en matière non volatile et du rendement
superficiel spécifique de revêtements pour prélaquage
Ta slovenski standard je istoveten z: EN 16074:2019
ICS:
87.040 Barve in laki Paints and varnishes
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN 16074
EUROPEAN STANDARD
NORME EUROPÉENNE
September 2019
EUROPÄISCHE NORM
ICS 87.040 Supersedes EN 16074:2011
English Version
Paints and varnishes - Determination of non-volatile-
matter content and spreading rate of coil coating materials
Peintures et vernis - Détermination de la teneur en Beschichtungsstoffe - Bestimmung des Gehaltes an
matière non volatile et du rendement superficiel nichtflüchtigen Anteilen und der Ergiebigkeit von
spécifique de revêtements pour prélaquage Bandbeschichtungsstoffen
This European Standard was approved by CEN on 1 July 2019.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 16074:2019 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 5
5 Apparatus and materials . 5
6 Sampling . 6
7 Test procedure . 6
7.1 Accuracy of weighing . 6
7.2 Procedure for coatings with the exception of PVC plastisols and pure epoxy . 6
7.2.1 Pan method. 6
7.2.2 Drawdown method . 6
7.3 Procedure for PVC plastisol . 7
7.3.1 Pan method. 7
7.3.2 Drawdown method . 8
8 Determination of the density . 8
9 Calculation of spreading rate of the paint . 8
10 Validation of test results . 9
11 Precision . 9
12 Test report . 9
Bibliography . 10

European foreword
This document (EN 16074:2019) has been prepared by Technical Committee CEN/TC 139 “Paints and
varnishes”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by March 2020, and conflicting national standards shall
be withdrawn at the latest by March 2020.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 16074:2011.
The main changes compared to EN 16074:2011 are:
a) the symbols have been aligned with current standards [ISO 3251 and ISO 3233 (all parts)], i.e. m for
mass, s for spreading rate, NV for non-volatile matter and ρ for density;
b) Clause 8 on "Determination of the density" has been added;
c) the text has been editorially revised and the normative references have been updated.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
1 Scope
The method specifies the gravimetric procedure for determining the non-volatile-matter content as a
percentage by mass of the majority of thermally cured coil coatings and subsequently for determining
the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 13523-0, Coil coated metals — Test methods — Part 0: General introduction
EN ISO 1513, Paints and varnishes — Examination and preparation of test samples (ISO 1513)
EN ISO 2811-1, Paints and varnishes — Determination of density — Part 1: Pycnometer method
(ISO 2811-1)
EN ISO 2811-2, Paints and varnishes — Determination of density — Part 2: Immersed body (plummet)
method (ISO 2811-2)
EN ISO 2811-3, Paints and varnishes — Determination of density — Part 3: Oscillation method (ISO 2811-
3)
EN ISO 2811-4, Paints and varnishes — Determination of density — Part 4: Pressure cup method
(ISO 2811-4)
EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling (ISO 15528)
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 13523-0 and the following
apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at http://www.iso.org/obp
3.1
spreading rate
surface area that can be covered by a given quantity of coating material to give a dried film of requisite
thickness
2 2
Note 1 to entry: It is expressed in m /l or m /kg.
Note 2 to entry: See also theoretical spreading rate.
[SOURCE: EN ISO 4618:2014, 2.238, modified – Application rate and practical spreading rate were
deleted in Note 2.]
3.2
non-volatile matter
NV
residue by mass obtained by evaporation under specified conditions
Note 1 to entry: Instead of the term “non-volatile matter” different terms, such as solid, dry residue, dry matter,
solid matter, stoving residue are being used commonly with the respective abbreviations. The term “non-volatile
matter” which is also applied in ISO 3251 should be used together with the abbreviation “NV” instead of these
terms.
[SOURCE: EN ISO 4618:2014, 2.176]
3.3
theoretical spreading rate
spreading rate calculated solely from the volume of non-volatile matter
[SOURCE: ISO 4618:2014, 2.256]
4 Principle
The non-volatile-matter content determination is based on the mass of dry residue of a known quantity
of wet paint cured in a pan or applied on a metal panel. Th
...

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