Textiles - Determination of the content of compounds based on chlorobenzenes and chlorotoluenes

This document specifies a method of analysis for determining the content of chlorobenzenes and chlorotoluenes in textile products made of components such as outer fabric, interlining, lining, plastic slide fasteners, plastic buttons, labels, threads and appliques.
The method applies to a mass fraction of 0,1 mg/kg to 10 mg/kg per single isomer. Both higher and lower concentrations can be determined if the mass of the sample is selected accordingly or if appropriate dilutions are made during the analysis.

Textilien - Bestimmung des Gehaltes von Verbindungen auf der Basis von Chlorbenzol und Chlortoluol

Dieses Dokument legt ein Analysenverfahren zur Bestimmung des Gehaltes an Chlorbenzolen und Chlortoluolen in textilen Erzeugnissen fest, hergestellt aus Komponenten wie z. B. Oberstoff, Einlagen, Futter, Reißverschlüssen aus Kunststoff, Knöpfen aus Kunststoff, Etiketten, Garnen und Applikationen.
Das Verfahren gilt für einen Massenanteil von 0,1 mg/kg bis 10 mg/kg je Einzelisomer. Höhere und niedrigere Konzentrationen können bestimmt werden, wenn die Einwaage der Probe entsprechend gewählt wird bzw. im Analysengang entsprechende Verdünnungen vorgenommen werden.

Textiles - Détermination de la teneur de composés à base de chlorobenzènes et chlorotoluènes

Le présent document spécifie une méthode d’analyse pour déterminer la teneur en chlorobenzènes et chlorotoluènes des produits textiles constitués de composants tels qu’une matière extérieure, une entredoublure, une doublure, des fermetures à glissière en plastique, des boutons en plastique, des étiquettes, des fils et des appliqués.
La méthode s’applique à une fraction massique de 0,1 mg/kg à 10 mg/kg par isomère unique. Des concentrations plus élevées et plus faibles peuvent être déterminées si la masse de l’échantillon est sélectionnée en conséquence ou si des dilutions appropriées sont réalisées au cours de l’analyse.

Tekstilije - Določevanje spojin na osnovi klorobenzenov in klorotoluenov

Ta standard določa metodo za analizo, s katero se določi vsebnost klorobenzenov in klorotoluenov v tekstilnih izdelkih ter sestavnih delih, kot so zgornja tkanina, vmesna podloga, podloga, gumbi, oznake, niti in njihove kombinacije. Metoda se uporablja za masni delež od 0,1 mg/kg do 10 mg/kg na posamezni izomer. Določiti je mogoče višje in nižje koncentracije, če je teža vzorca ustrezno izbrana ali če so med analizo pripravljene ustrezne raztopine.

General Information

Status
Published
Publication Date
20-Nov-2018
Withdrawal Date
30-May-2019
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
21-Nov-2018
Due Date
21-Feb-2019
Completion Date
21-Nov-2018

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.ROXHQRYTextilien - Bestimmung des Gehaltes von Verbindungen auf der Basis von Chlorbenzol und ChlortoluolTextiles - Détermination de la teneur de composés à base de chlorobenzènes et chlorotoluènesTextiles - Determination of the content of compounds based on chlorobenzenes and chlorotoluenes59.080.01Tekstilije na splošnoTextiles in generalICS:Ta slovenski standard je istoveten z:EN 17137:2018SIST EN 17137:2019en,fr,de01-januar-2019SIST EN 17137:2019SLOVENSKI
STANDARD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 17137
November
t r s z ICS
w {ä r z rä r s English Version
Textiles æ Determination of the content of compounds based on chlorobenzenes and chlorotoluenes Textiles æ Détermination de la teneur de composés à base de chlorobenzènes et chlorotoluènes
Textilien æ Bestimmung des Gehaltes von Verbindungen auf der Basis von Chlorbenzol und Chlortoluol This European Standard was approved by CEN on
u September
t r s zä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Rue de la Science 23,
B-1040 Brussels
t r s z CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s y s u yã t r s z ESIST EN 17137:2019

Chromatographic analyses . 8 A.1 Capillary gas chromatography/mass selective detector (GC-MS) . 8 Annex B (informative)
Reliability of the method . 11 B.1 General . 11 B.2 Accuracy . 11 B.3 Detection Limit (LOD) and Quantification Limit (LOQ) . 12 B.4 Repeatability . 13 B.5 Reproducibility . 14 B.6 Robustness. 15 B.7 Selectivity . 16 B.8 Extraction Efficiency . 17 Bibliography . 18
shall not be held responsible for identifying any or all such patent rights. This document is based on DIN 54 232, which was created by the Working Committee NA 062-05-12 AA “Textiles chemical test methods and fibre separation” of the Standard Committee Testing (NMP) in the DIN Deutsches Institut for Standardization. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 17137:2019

a Chemical Abstracts Service Number SIST EN 17137:2019

= 1 mg/ml). Then a mixed standard is prepared (e.g. 1 ml of each stock solution to 100
= 10 µg/ml). This mixed calibration standard is used to prepare calibration solutions of various concentrations (e.g. 10, 50, 100, 200, 400, 600, 800, 1 000 ng/ml). Finally 1 ml of each individual calibration solution is mixed with 10 µI of the internal standard solution (e.g. at concentration of 10µg/ml) and analysed. SIST EN 17137:2019

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