Oilseeds - Simultaneous determination of oil and water contents - Method using pulsed nuclear magnetic resonance spectrometry (ISO/DIS 10565:2025)

This International Standard specifies a rapid method for the determination of the oil and water contents of commercial oilseeds using pulsed nuclear magnetic resonance (NMR). It is applicable to rapeseeds, soya beans, linseeds and sunflower seeds with a water content less than 10 %. For seeds with higher water contents, drying is necessary before the oil content can be determined by pulsed NMR. NOTE 1 This method has been tested with rapeseeds, soya beans, linseeds and sunflower seeds. This does not, however, preclude its applicability to other commercial seeds whose oil is liquid at the temperature of measurement. NOTE 2 The reproducibility values are generally higher than those obtained by the drying method (ISO 665)

Ölsaaten - Gleichzeitige Bestimmung des Öl- und Wassergehalts - Verfahren mit gepulster Kernspinresonanzspektrometrie (ISO/DIS 10565:2025)

Graines oléagineuses - Détermination simultanée de la teneur en huile et en eau - Méthode par spectrométrie par résonance magnétique nucléaire pulsée (ISO/DIS 10565:2025)

La présente Norme internationale spécifie une méthode de détermination rapide de la teneur en huile et en eau dans les graines entières du commerce, par spectrométrie par résonance magnétique nucléaire (RMN) pulsée. Elle est applicable aux graines de colza, de soja, de lin et de tournesol dont la teneur en eau est inférieure à 10 %. Pour des graines ayant des teneurs en eau plus élevées, il est nécessaire de les sécher avant de déterminer leur teneur en huile par RMN pulsée. NOTE 1 Cette méthode a été expérimentée sur les graines de colza, de soja, de lin et de tournesol. Cela n'exclut toutefois pas qu'elle puisse s'appliquer également à d'autres graines oléagineuses du commerce dont l'huile est liquide à la température de mesurage. NOTE 2 Les valeurs de reproductibilité obtenues sont généralement plus élevées que celles obtenues par la méthode par dessiccation (ISO 665).

Oljna semena - Simultano določanje olja in vode - Spektrometrija jedrske magnetne resonance s pulznim delovanjem (ISO/DIS 10565:2025)

General Information

Status
Not Published
Publication Date
20-Dec-2026
Current Stage
4060 - Closure of enquiry - Enquiry
Start Date
19-Aug-2025
Completion Date
19-Aug-2025

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Draft
prEN ISO 10565:2025
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SLOVENSKI STANDARD
01-julij-2025
Oljna semena - Simultano določevanje olja in vode - Spektrometrijska metoda z
uporabo pulzne jedrske magnetne resonance (ISO/DIS 10565:2025)
Oilseeds - Simultaneous determination of oil and water contents - Method using pulsed
nuclear magnetic resonance spectrometry (ISO/DIS 10565:2025)
Ölsaaten - Gleichzeitige Bestimmung des Öl- und Wassergehalts - Verfahren mit
gepulster Kernspinresonanzspektrometrie (ISO/DIS 10565:2025)
Graines oléagineuses - Détermination simultanée de la teneur en huile et en eau -
Méthode par spectrométrie par résonance magnétique nucléaire pulsée (ISO/DIS
10565:2025)
Ta slovenski standard je istoveten z: prEN ISO 10565
ICS:
67.200.20 Oljnice Oilseeds
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

DRAFT
International
Standard
ISO/DIS 10565
ISO/TC 34/SC 2
Oilseeds — Simultaneous
Secretariat: AFNOR
determination of oil and water
Voting begins on:
contents — Method using pulsed
2025-05-27
nuclear magnetic resonance
Voting terminates on:
spectrometry
2025-08-19
Graines oléagineuses — Détermination simultanée de la teneur
en huile et en eau — Méthode par spectrométrie par résonance
magnétique nucléaire pulsée
ICS: 67.200.20
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENTS AND APPROVAL. IT
IS THEREFORE SUBJECT TO CHANGE
AND MAY NOT BE REFERRED TO AS AN
INTERNATIONAL STANDARD UNTIL
PUBLISHED AS SUCH.
This document is circulated as received from the committee secretariat.
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STANDARDS MAY ON OCCASION HAVE TO
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NOTIFICATION OF ANY RELEVANT PATENT
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PROVIDE SUPPORTING DOCUMENTATION.
Reference number
ISO/DIS 10565:2025(en)
DRAFT
ISO/DIS 10565:2025(en)
International
Standard
ISO/DIS 10565
ISO/TC 34/SC 2
Oilseeds — Simultaneous
Secretariat: AFNOR
determination of oil and water
Voting begins on:
contents — Method using pulsed
nuclear magnetic resonance
Voting terminates on:
spectrometry
Graines oléagineuses — Détermination simultanée de la teneur
en huile et en eau — Méthode par spectrométrie par résonance
magnétique nucléaire pulsée
ICS: 67.200.20
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENTS AND APPROVAL. IT
IS THEREFORE SUBJECT TO CHANGE
AND MAY NOT BE REFERRED TO AS AN
INTERNATIONAL STANDARD UNTIL
PUBLISHED AS SUCH.
This document is circulated as received from the committee secretariat.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
© ISO 2025
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
STANDARDS MAY ON OCCASION HAVE TO
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BE CONSIDERED IN THE LIGHT OF THEIR
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POTENTIAL TO BECOME STANDARDS TO
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or ISO’s member body in the country of the requester.
NATIONAL REGULATIONS.
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TO SUBMIT, WITH THEIR COMMENTS,
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NOTIFICATION OF ANY RELEVANT PATENT
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Website: www.iso.org
Published in Switzerland Reference number
ISO/DIS 10565:2025(en)
ii
ISO/DIS 10565:2025(en)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Samples . 2
5.1 General .2
5.2 Calibration samples .2
5.2.1 Samples for moisture-content calibration .2
5.2.2 Samples for oil-content calibration .2
6 Apparatus . 2
7 Sampling . 3
8 Preparation of test sample . 3
9 Calibration procedure . 3
9.1 General .3
9.2 Calibration procedure for the determination of water content .4
9.2.1 Procedure A: Three calibration samples with known water contents .4
9.2.2 Procedure B: One calibration sample with known water content .4
9.3 Calibration procedure for the determination of oil content .5
9.3.1 Procedure A: Three calibration samples with known oil contents .5
9.3.2 Procedure B: One calibration sample with known oil content.6
10 Procedure . 7
10.1 Requirements for the test room and conditioning of the test sample.7
10.2 Test portion .7
10.3 Determination .7
10.3.1 General case .7
10.3.2 Rapeseeds, linseeds and sunflower seeds having a water content greater than
10 % (m/m) and soya beans having a water content greater than 14 % (m/m) .8
11 Expression of the results . 8
12 Precision . 9
12.1 Interlaboratory tests .9
12.2 Repeatability .9
12.3 Reproducibility .9
13 Test report . 9
Annex A (informative) Results of interlaboratory tests . 10
Annex B (informative) Results of test to compare different equipment .12
Bibliography . 14

iii
ISO/DIS 10565:2025(en)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee
has been established has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely
with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are described
in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types
of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the
ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent
rights identified during the development of the document will be in the Introduction and/or on the ISO list of
patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions
related to conformity assessment, as well as information about ISO's adherence to the World Trade
Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.
This document was prepared by Technical ISO/TC 34, Food products, Subcommittee SC 2, Oleaginous seeds and
fruits and oilseed meals.
This third edition cancels and replaces the second edition (ISO 10565:1998), which has been technically
revised.
The main changes compared to the previous edition are as follows:
— Clarification of the scope;
— Addition of additional information in the protocol.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.

iv
DRAFT International Standard ISO/DIS 10565:2025(en)
Oilseeds — Simultaneous determination of oil and water
contents — Method using pulsed nuclear magnetic resonance
spectrometry
1 Scope
This International Standard specifies a rapid method for the determination of the oil and water contents of
commercial oilseeds using pulsed Nuclear Magnetic Resonance (NMR).
It is applicable to rapeseeds, soya beans, linseeds and sunflower seeds with a water content less than 10 %. For
seeds with higher water contents, drying is necessary before the oil co
...

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