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ASTM D6227-04a

(Specification)

Standard Specification for Grade 82 Unleaded Aviation Gasoline

Standard Specification for Grade 82 Unleaded Aviation Gasoline

ABSTRACT
This specification covers Grade 82 unleaded aviation gasoline for use only in engines and associated aircraft that are specifically approved by the engine and aircraft manufacturers, and certified by the National Certifying Agencies to use this fuel. Aviation gasoline shall consist of blends of refined hydrocarbons derived from crude petroleum, natural gasoline or blends thereof, with specific aliphatic ethers, synthetic hydrocarbons, or aromatic hydrocarbons, and when applicable, methyl tertiarybutyl ether (MTBE). They may also contain antioxidants (oxidation inhibitors), metal deactivators, corrosion inhibitors, and fuel system icing inhibitors. The gasoline shall be tested and conform accordingly to the following property requirements: lean mixture knock value and motor method octane number; color; blue and red dye content; distillation temperature at % evaporated, end point, and residue content; distillation recovery; distillation loss; net heat of combustion; freezing point; vapor pressure; lead content; copper strip corrosion; sulfur content; potential gum; and alcohols and ether content (aliphatic ethers, methanol, and ethanol).
SCOPE
1.1 Grade 82 unleaded aviation gasoline defined by this specification is for use only in engines and associated aircraft that are specifically approved by the engine and aircraft manufacturers, and certified by the National Certifying Agencies to use this fuel. This fuel is not considered suitable for use in other engines and associated aircraft that are certified to use aviation gasolines meeting Specification D910.  
1.2 A fuel may be certified to meet this specification by a producer as Grade 82 UL aviation gasoline, only if blended from component(s) approved for use in Grade 82 UL aviation gasoline by the refiner(s) of such components because only the refiner(s) can attest to the component source and processing, absence of contamination, and the additives used and their concentrations. Consequently, re-classifying and any other product to Grade 82 UL aviation gasoline does not meet this specification.  
1.3 Appendix XI contains an explanation for the rationale of the specification. Appendix X2 details the reasons for the individual specification requirements.  
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.

General Information

Status
Historical
Publication Date
31-Oct-2004
ICS
75.160.20 - Liquid fuels
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.J0.02 - Aviation Piston Engine Fuels
Current Stage
Ref Project

Relations

Replaces
ASTM D6227-04 - Standard Specification for Grade 82 Unleaded Aviation Gasoline
Effective Date
01-Nov-2004
Replaced By
ASTM D6227-10 - Standard Specification for Grades UL82 and UL87 Unleaded Aviation Gasoline
Effective Date
01-Oct-2010
Referred By
ASTM F2507-15 - Standard Specification for Recreational Airpark Design
Effective Date
01-Nov-2004
Referred By
ASTM D4529-17 - Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
Effective Date
01-Nov-2004
Referred By
ASTM E1259-23 - Standard Practice for Evaluation of Antimicrobials in Liquid Fuels Boiling Below 390 °C
Effective Date
01-Nov-2004
Referred By
ASTM D7960-21 - Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Non-hydrocarbon Components
Effective Date
01-Nov-2004
Referred By
ASTM D7464-20 - Standard Practice for Manual Sampling of Liquid Fuels, Associated Materials and Fuel System Components for Microbiological Testing
Effective Date
01-Nov-2004
Referred By
ASTM D7826-23a - Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives
Effective Date
01-Nov-2004
Referred By
ASTM D6469-20 - Standard Guide for Microbial Contamination in Fuels and Fuel Systems
Effective Date
01-Nov-2004

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ASTM D6227-04a - Standard Specification for Grade 82 Unleaded Aviation GasolineASTM D6227-04a - Standard Specification for Grade 82 Unleaded Aviation Gasoline
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ASTM D6227-04a - Standard Specification for Grade 82 Unleaded Aviation Gasoline
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D6227 – 04a
Standard Specification for
1
Grade 82 Unleaded Aviation Gasoline
This standard is issued under the fixed designation D6227; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D381 Test Method for Gum Content in Fuels by Jet Evapo-
ration
1.1 This specification covers Grade 82 unleaded aviation
D873 Test Method for Oxidation Stability ofAviation Fuels
gasoline, which is defined by this specification as for use only
(Potential Residue Method)
inenginesandassociatedaircraftthatarespecificallyapproved
D909 Test Method for Supercharge Rating of Spark-
by the engine and aircraft manufacturers, and certified by the
Ignition Aviation Gasoline
National Certifying Agencies to use this fuel. This fuel is not
D910 Specification for Aviation Gasolines
considered suitable for use in other engines and associated
D1266 Test Method for Sulfur in Petroleum Products
aircraft that are certified to use aviation gasolines meeting
(Lamp Method)
Specification D910.
D2386 Test Method for Freezing Point of Aviation Fuels
1.2 A fuel may be certified to meet this specification by a
D2392 Test Method for Color of Dyed Aviation Gasolines
producer as Grade 82 UL aviation gasoline only if blended
D2622 Test Method for Sulfur in Petroleum Products by
from component(s) approved for use in Grade 82 UL aviation
Wavelength Dispersive X-ray Fluorescence Spectrometry
gasolinebytherefiner(s)ofsuchcomponents,becauseonlythe
D2700 Test Method for Motor Octane Number of Spark-
refiner(s) can attest to the component source and processing,
Ignition Engine Fuel
absence of contamination, and the additives used and their
D3120 Test Method for Trace Quantities of Sulfur in Light
concentrations. Consequently, re-classifying of any other prod-
Liquid Petroleum Hydrocarbons by Oxidative Microcou-
uct to Grade 82 UL aviation gasoline does not meet this
lometry
specification.
D3231 Test Method for Phosphorus in Gasoline
1.3 Appendix X1 contains an explanation for the rationale
D3237 Test Method for Lead in Gasoline by Atomic Ab-
of the specification. Appendix X2 details the reasons for the
sorption Spectroscopy
individual specification requirements.
D3338 Test Method for Estimation of Net Heat of Combus-
1.4 The values stated in SI units are to be regarded as the
tion of Aviation Fuels
standard. The values given in parentheses are provided for
D4057 Practice for Manual Sampling of Petroleum and
information only.
Petroleum Products
2. Referenced Documents
D4171 Specification for Fuel System Icing Inhibitors
2
D4294 Test Method for Sulfur in Petroleum and Petroleum
2.1 ASTM Standards:
Products by Energy Dispersive X-ray Fluorescence Spec-
D86 Test Method for Distillation of Petroleum Products at
trometry
Atmospheric Pressure
D4529 Test Method for Estimation of Net Heat of Combus-
D130 Test Method for Corrosiveness to Copper from Pe-
tion of Aviation Fuels
troleum Products by Copper Strip Test
D4809 Test Method for Heat of Combustion of Liquid
D357 Method of Test for Knock Characteristics of Motor
3
Hydrocarbon Fuels by Bomb Calorimeter (Precision
Fuels Below 100 Octane Number by the Motor Method
Method)
D4815 Test Method for Determination of MTBE, ETBE,
1
This test method is under the jurisdiction of ASTM Committee D02 on
TAME, DIPE, tertiary-Amyl Alcohol and C to C Alco-
1 4
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
hols in Gasoline by Gas Chromatography
D02.J0 on Aviation Fuels.
D4953 Test Method for Vapor Pressure of Gasoline and
Current edition approved Nov. 1, 2004. Published November 2004. Originally
approved in 1998. Last previous edition approved in 2004 as D6227–04. DOI:
Gasoline-Oxygenate Blends (Dry Method)
10.1520/D6227-04A.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3
Withdrawn. The last approved version of this historical standard is referenced
on www.astm.org.
*ASummary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6227 – 04a
D5059 Test Methods for Lead in Gasoline by X-Ray Spec- thereof, with specific aliphatic ethers, synthetic hydrocarbons,
troscopy or aromatic hydrocarbons. When applicable, methyl tertiary-
D5190 Test Method for Vapor Pressure of Petroleum Prod- butyl
...

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5.1 The combustion quality of aviation turbine fuel has traditionally been controlled in specifications by such tests as smoke point (see Test Method D1322), smoke volatility index, aromatic content of luminometer number (see Test Method D1740). Evidence is accumulating that a better control of the quality may be obtained by limiting the minimum hydrogen content of the fuel.  
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1.1 This test method covers the determination of the hydrogen content of aviation turbine fuels.  
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SIGNIFICANCE AND USE
5.1 This guide is intended for the developers or sponsors of new aviation gasolines or additives to describe the data requirements necessary to support the development of specifications for these new products by ASTM members. The ultimate goal of the data generated in accordance with this guide is to provide an understanding of the performance of the new fuel or additive within the property constraints and compositional bounds of the proposed specification criteria.  
5.2 This guide is not an approval process. It is intended to describe test and analysis requirements necessary to generate data to support specification development. This guide does not address the approval process for ASTM International standards.  
5.3 This guide will reduce the uncertainty and risk to developers or sponsors of new aviation gasolines or additives by describing the test and analysis requirements necessary to proceed with the development of an ASTM International specification for aviation gasoline or specification revision for an aviation gasoline additive. There are certain sections within this guide that do not specify an exact number of data points required. For example, 6.2.4.3 requires viscosity to be measured from freezing point to room temperature; 6.2.4.4, 6.2.4.5, and 6.3.2.3 require measurements over the operating temperature range; 6.3.2.4 and 6.3.2.5 require measurements versus temperature. In these cases, the developers or sponsors of new aviation gasolines or additives should attempt to generate data close to the upper and lower boundaries indicated. If no boundary is specified (for example, generate data versus temperature), then data at the widest practical test limits should be generated. A minimum of three data points is required in all cases (for example, upper, middle, lower), while five or more data points are preferred.  
5.4 This guide does not purport to specify an all-inclusive listing of test and analysis requirements to achieve ASTM International approval ...
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1.1 This guide provides procedures to develop data for use in research reports for new aviation gasolines or new aviation gasoline additives.  
1.2 This data is intended to be used by the ASTM subcommittee to make a determination of the suitability of the fuel for use as an aviation fuel in either a fleet-wide or limited capacity, and to make a determination that the proposed properties and criteria in the associated standard specification provide the necessary controls to ensure this fuel maintains this suitability during high-volume production.  
1.3 These research reports are intended to support the development and issuance of new specifications or specification revisions for these products. Guidance to develop ASTM International standard specifications for aviation gasoline is provided in Subcommittee J on Aviation Fuels Operating Procedures, Annex A6, “Guidelines for the Development and Acceptance of a New Aviation Fuel Specification for Spark-Ignition Reciprocating Engines.”  
1.4 The procedures, tests, selection of materials, engines, and aircraft detailed in this guide are based on industry expertise to give appropriate data for review. Because of the diversity of aviation hardware and potential variation in fuel/additive formulations, not every aspect may be encompassed and further work may be required. Therefore, additional data beyond that described in this guide may be requested by the ASTM task force, Subcommittee J, or Committee D02 upon review of the specific composition, performance, or other characteristics of the candidate fuel or additive.  
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SIGNIFICANCE AND USE
5.1 Some acids can be present in aviation turbine fuels due either to the acid treatment during the refining process or to naturally occurring organic acids. Significant acid contamination is not likely to be present because of the many check tests made during the various stages of refining. However, trace amounts of acid can be present and are undesirable because of the consequent tendencies of the fuel to corrode metals that it contacts or to impair the water separation characteristics of the aviation turbine fuel.  
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1.1 This test method covers the determination of the acidity in aviation turbine fuel in the range from 0.000 mg/g to 0.100 mg/g KOH.  
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5.1 This test method provides a rapid and precise elemental measurement with simple sample preparation. Typical analysis times are approximately 4 min to 5 min per sample with a preparation time of approximately 1 min to 3 min per sample.  
5.2 The quality of crude oil is related to the amount of sulfur present. Knowledge of the vanadium and nickel concentration is necessary for processing purposes as well as contractual agreements.  
5.3 The presence of vanadium and nickel presents significant risks for contamination of the cracking catalysts in the refining process.  
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1.3 This test method is limited to the use of X-ray fluorescence (XRF) spectrometers employing an X-ray tube for excitation in conjunction with wavelength dispersive detection system or energy dispersive high resolution semiconductor detector with the ability to separate signals of adjacent and near-adjacent elements.  
1.4 This test method uses inter-element correction factors calculated from XRF theory, the fundamental parameters (FP) approach, or best fit regression.  
1.5 Samples containing higher concentrations than shown in Table 1 must be diluted to bring the elemental concentration of the diluted material within the scope of this test method.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6.1 The preferred concentrations units are mg/kg for vanadium and nickel.  
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5.1 The analysis of trace oxygenates in automotive spark-ignition engine fuel has become routine in certain areas to ensure compliance whenever oxygenated fuels are used. In addition, test methods to measure trace levels of oxygenates in automotive spark-ignition fuel are necessary to assess product quality.
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1.1 This test method covers the determination of trace oxygenates in automotive spark-ignition engine fuel. The method used is a multidimensional gas chromatographic method using 1,2-dimethoxy ethane as the internal standard. The oxygenates that are analyzed are: methyl-tertiary butyl ether (MTBE), ethyl-tertiary butyl ether (ETBE), diisopropyl ether (DIPE), methanol, tertiary-amyl methyl ether (TAME), n-propanol, i-propanol, n-butanol, i-butanol, tert-butyl alcohol, sec-butyl alcohol, and tert-pentanol. Ethanol is usually not measured as a trace oxygenate since ethanol can be used as the main oxygenate compound in finished automotive spark-ignition fuels such as reformulated automotive spark-ignition fuels. The concentration range of the oxygenates covered in the ILS study was from 10 mg/kg to 2000 mg/kg. In addition this method is also suitable for the measurement of the C5 isomeric alcohols (2-methyl-1-butanol, 2-methyl-2-butanol) present from the fermentation of ethanol.  
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Standard Test Methods for Hydrogen Content of Light Distillates, Middle Distillates, Gas Oils, and Residua by Low-Resolution Nuclear Magnetic Resonance Spectroscopy

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5.1 The hydrogen content represents a fundamental quality of a petroleum product that has been correlated with many of the performance characteristics of that product.  
5.2 This test method provides a simple and more precise alternative to existing test methods, specifically combustion techniques (Test Methods D5291) for determining the hydrogen content on a range of petroleum products.
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1.1 These test methods cover the determination of the hydrogen content of petroleum products ranging from atmospheric distillates to vacuum residua using a continuous wave, low-resolution nuclear magnetic resonance spectrometer. (Test Method D3701 is the preferred method for determining the hydrogen content of aviation turbine fuels using nuclear magnetic resonance spectroscopy.)  
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Gas Oils  
370–510 (700–950)  
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5.1 The tendency of a fuel to vaporize in automotive engine fuel systems is indicated by the vapor-liquid ratio of the fuel.  
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1.1 This test method covers the determination of the temperature at which the vapor formed from a selected volume of volatile petroleum product saturated with air at 0 °C to 1 °C (32 °F to 34 °F) produces a pressure of 101.3 kPa (one atmosphere) against vacuum. This test method is applicable to samples for which the determined temperature is between 36 °C and 80 °C (97 °F and 176 °F) and the vapor-liquid ratio is between 8 to 1 and 75 to 1.
Note 1: When the vapor-liquid ratio is 20:1, the result is intended to be comparable to the results determined by Test Method D2533.
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1.2 This test method is applicable to both gasoline and gasoline-oxygenate blends.  
1.2.1 Some gasoline-oxygenate blends may show a haze when cooled to 0 °C to 1 °C. If a haze is observed in 12.5, it shall be indicated in the reporting of results. The precision and bias statements for hazy samples have not been determined (see Note 12).  
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1.3.1 Exception—The values given in parentheses are provided for information only.  
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SIGNIFICANCE AND USE
5.1 Wear due to excessive friction resulting in shortened life of engine components such as fuel pumps and fuel controls has sometimes been ascribed to lack of lubricity in an aviation fuel.  
5.2 The relationship of test results to aviation fuel system component distress due to wear has been demonstrated for some fuel/hardware combinations where boundary lubrication is a factor in the operation of the component.  
5.3 The wear scar generated in the ball-on-cylinder lubricity evaluator (BOCLE) test is sensitive to contamination of the fluids and test materials, the presence of oxygen and water in the atmosphere, and the temperature of the test. Lubricity measurements are also sensitive to trace materials acquired during sampling and storage. Containers specified in Practice D4306 shall be used.  
5.4 The BOCLE test method may not directly reflect operating conditions of engine hardware. For example, some fuels that contain a high content of certain sulfur compounds can give anomalous test results.
SCOPE
1.1 This test method covers assessment of the wear aspects of the boundary lubrication properties of aviation turbine fuels on rubbing steel surfaces.  
1.1.1 This test method incorporates two procedures, one using a semi-automated instrument and the second a fully automated instrument. Either of the two instruments may be used to carry out the test.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7398-23(Test Method)
Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of FAMES provides an insight into the composition of product related to the transesterification process. This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for product specification testing with the mutual agreement of interested parties.  
5.2 Biodiesel (FAMES) exhibits a boiling point rather than a distillation curve. The fatty acid chains in the raw oils and fats from which biodiesel is produced are mainly comprised of straight chain hydrocarbons with 16 to 18 carbons that have similar boiling temperatures. The atmospheric boiling point of biodiesel generally ranges from 330 °C to 357 °C. The Specification D6751 value of 360 °C max at 90 % off by Test Method D1160 was incorporated as a precaution to ensure the fuel has not been adulterated with high boiling contaminants.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of fatty acid methyl esters (FAME). This test method is applicable to FAMES (biodiesel, B100) having an initial boiling point greater than 100 °C and a final boiling point less than 615 °C at atmospheric pressure as measured by this test method.  
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1.6 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method was developed to assess the performance of a heavy-duty engine oil in controlling engine wear under operating conditions selected to accelerate soot production and valve-train wear in a turbocharged and aftercooled four-cycle diesel engine with sliding tappet followers equipped with exhaust gas recirculation hardware.  
5.2 The design of the engine used in this test method is representative of many, but not all, modern diesel engines. This factor, along with the accelerated operating conditions, shall be considered when extrapolating test results.
SCOPE
1.1 This test method, commonly referred to as the Cummins ISB Test, covers the utilization of a modern, 5.9 L, diesel engine equipped with exhaust gas recirculation and is used to evaluate oil performance with regard to valve-train wear.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exceptions—SI units are provided for all parameters except where there is no direct equivalent such as the units for screw threads, National Pipe Threads/diameters, tubing size, or where there is a sole source of supply equipment specification.  
1.2.2 See also A7.1 for clarification; it does not supersede 1.2 and 1.2.1.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions.  
1.4 Table of Contents:    
Section  
Scope  
1  
Referenced Documents  
2  
Terminology  
3  
Summary of Test Method  
4  
Significance and Use  
5  
Apparatus  
6  
Engine Fluids and Cleaning Solvents  
7  
Preparation of Apparatus  
8  
Engine/Stand Calibration and Non-Reference Oil Tests  
9  
Test Procedure  
10  
Calculations, Ratings, and Test Validity  
11  
Report  
12  
Precision and Bias  
13  
Annexes  
Safety Precautions  
Annex A1  
Intake Air Aftercooler  
Annex A2  
The Cummins ISB Engine Build Parts Kit  
Annex A3  
Sensor Locations and Special Hardware  
Annex A4  
External Oil System  
Annex A5  
Cummins Service Publications  
Annex A6  
Specified Units and Formats  
Annex A7  
Oil Analyses  
Annex A8  
Alternate Fuel Approval Process  
Annex A9  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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