ASTM D1110-21
(Test Method)Standard Test Methods for Water Solubility of Wood
Standard Test Methods for Water Solubility of Wood
SIGNIFICANCE AND USE
2.1 Cold water removes a part of such extraneous materials as tannins, gums, sugars, and coloring matters. Hot water removes these plus the starches.
SCOPE
1.1 These test methods3 cover the determination of the water solubility of wood. Two methods are given, as follows:
1.1.1 Method A—Cold-Water Solubility—This method provides a measure of the tannins, gums, sugars, and coloring matter in the wood.
1.1.2 Method B—Hot-Water Solubility—This method provides a measure of the tannins, gums, sugars, coloring matter, and starches in the wood.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
- Status
- Published
- Publication Date
- 31-Mar-2021
- Technical Committee
- D07 - Wood
- Drafting Committee
- D07.01 - Fundamental Test Methods and Properties
Overview
ASTM D1110-21: Standard Test Methods for Water Solubility of Wood establishes procedures to determine the water solubility of wood using both cold and hot water extraction methods. These methods enable accurate measurement of the content of extraneous materials in wood such as tannins, gums, sugars, coloring matters, and starches. Developed by ASTM, this internationally recognized standard is essential for quality control and research in industries where understanding wood’s soluble content is critical, such as pulp and paper manufacturing, wood processing, and related sectors.
Key Topics
Cold-Water Solubility (Method A):
- Measures the portion of tannins, gums, sugars, and coloring matter that are soluble in cold water.
- Useful for assessing wood purity and the presence of non-structural materials.
Hot-Water Solubility (Method B):
- Determines the fraction of tannins, gums, sugars, coloring matter, and starches dissolved by hot water.
- Provides deeper insight into the total water-soluble content of the wood sample.
Test Procedures:
- Standardized sample sizes and controlled conditions ensure repeatability and comparability.
- Includes clear reporting requirements for results, typically as a percentage of soluble matter on a moisture-free basis.
Precision and Repeatability:
- Detailed repeatability data supports consistent implementation within laboratories.
Safety and Compliance:
- Emphasizes the need for users to establish appropriate safety, health, and environmental practices.
Applications
The ASTM D1110-21 standard is widely used in:
Pulp and Paper Industry:
Determining the content of water-soluble extractives is essential for assessing wood suitability for pulp production and ensuring product consistency.Wood Processing and Manufacturing:
Understanding water solubility helps in choosing suitable wood species and treatments for specific end uses, especially where extractives could interfere with adhesives, finishes, or coatings.Research and Development:
Provides a consistent methodology for analyzing the chemical composition of wood in academic and industrial research settings.Quality Control and Compliance:
Enables manufacturers to verify that wood products meet required specifications for water-soluble content, supporting regulatory compliance and product performance.
Related Standards
Professionals referencing ASTM D1110-21 should also consider the following related standards and resources:
- TAPPI T 207: Water Solubility of Wood and Pulp (similar methodology, recognized in the pulp and paper industry).
- ISO Standards for Wood Analysis: International methods for assessing wood composition and extractives.
- Other ASTM Wood Standards: For assessing additional wood properties such as density, moisture content, and mechanical characteristics.
By adhering to ASTM D1110-21, laboratories and manufacturers can assure consistent, reliable results in the determination of water solubility in wood, enhancing both product quality and process efficiency. This standard is an integral part of wood characterization, underpinning the production of high-quality wood and paper products and supporting research into wood chemistry.
Keywords: ASTM D1110-21, water solubility of wood, cold-water solubility, hot-water solubility, wood testing methods, pulp and paper, wood extractives, quality control in wood industry.
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Frequently Asked Questions
ASTM D1110-21 is a standard published by ASTM International. Its full title is "Standard Test Methods for Water Solubility of Wood". This standard covers: SIGNIFICANCE AND USE 2.1 Cold water removes a part of such extraneous materials as tannins, gums, sugars, and coloring matters. Hot water removes these plus the starches. SCOPE 1.1 These test methods3 cover the determination of the water solubility of wood. Two methods are given, as follows: 1.1.1 Method A—Cold-Water Solubility—This method provides a measure of the tannins, gums, sugars, and coloring matter in the wood. 1.1.2 Method B—Hot-Water Solubility—This method provides a measure of the tannins, gums, sugars, coloring matter, and starches in the wood. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
SIGNIFICANCE AND USE 2.1 Cold water removes a part of such extraneous materials as tannins, gums, sugars, and coloring matters. Hot water removes these plus the starches. SCOPE 1.1 These test methods3 cover the determination of the water solubility of wood. Two methods are given, as follows: 1.1.1 Method A—Cold-Water Solubility—This method provides a measure of the tannins, gums, sugars, and coloring matter in the wood. 1.1.2 Method B—Hot-Water Solubility—This method provides a measure of the tannins, gums, sugars, coloring matter, and starches in the wood. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D1110-21 is classified under the following ICS (International Classification for Standards) categories: 79.040 - Wood, sawlogs and sawn timber. The ICS classification helps identify the subject area and facilitates finding related standards.
ASTM D1110-21 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1110 − 21
Standard Test Methods for
1,2
Water Solubility of Wood
This standard is issued under the fixed designation D1110; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2 Filtering Flask—Asuction filtering flask, equipped with
a rubber flange for the crucible and funnel, shall be provided.
1.1 These test methods cover the determination of the
water solubility of wood. Two methods are given, as follows:
4. Test Specimen
1.1.1 Method A—Cold-Water Solubility—This method pro-
vides a measure of the tannins, gums, sugars, and coloring 4.1 The test specimen shall consist of2gofair-dried
matter in the wood. sawdust or milled wood that has been ground to pass through
1.1.2 Method B—Hot-Water Solubility—This method pro- a 425-µm (approx. 40 mesh) sieve and be retained on a 250-µm
vides a measure of the tannins, gums, sugars, coloring matter, (approx. 60 mesh) sieve.
and starches in the wood.
5. Procedure
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 5.1 Place a 2-g test specimen, the moisture content of which
responsibility of the user of this standard to establish appro-
hasbeenpreviouslydetermined,ina400-mLbeaker,andcover
priate safety, health, and environmental practices and deter- with 300 mL of distilled water. Let this mixture solvate at a
mine the applicability of regulatory limitations prior to use.
temperature of 23 6 2 °C, with frequent stirring, for 48 h.
1.3 This international standard was developed in accor-
5.2 Filter the material on an Alundum or fritted-glass
dance with internationally recognized principles on standard-
crucible, using suction, wash with cold distilled water, and dry
ization established in the Decision on Principles for the
to constant weight at 100 to 105°C. Drying usually requires
Development of International Standards, Guides and Recom-
approximately 4 h. Place the crucible in a loosely stoppered
mendations issued by the World Trade Organization Technical
weighing bottle, cool in a desiccator, and weigh.
Barriers to Trade (TBT) Committee.
6. Report
2. Significance and Use
6.1 Reporttheresultsaspercentageofmattersolubleincold
2.1 Cold water removes a part of such extraneous materials
water, on the moisture-free basis, calculated as follows:
as tannins, gums, sugars, and coloring matters. Hot water
Cold water solubility,% 5 @ W 2 W /W # 3100 (1)
removes these plus the starches. ~ !
1 2 1
where:
METHOD A—COLD-WATER SOLUBILITY
W = weight of moisture-free specimen used in 5.1, and
3. Apparatus W = weight of dried specimen after extraction with cold
water (5.2).
3.1 Filtering Crucibles—Alundum or fritted-glass crucibles
of coarse porosity will be required.
METHOD B—HOT-WATER SOLUBILITY
1 7. Apparatus
These test methods are under the jurisdiction of ASTM Committee D07 on
Wood and are the direct responsibility of D07.01 on Fundamental Test Methods and
7.1 Solvation Apparatus—a 200-mL Erlenmeyer flask pro-
Properties.
vided with a reflux condenser shall be used.
Current edition approved April 1, 2021. Published April 2021. Originally
approved in 1950. Last previous edition approved in 2013 as D1110 – 84 (2013).
7.2
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1110 − 84 (Reapproved 2013) D1110 − 21 Technical Association of Pulp and Paper Industry
Standard Method T 207 om-81
Standard Test Methods for
1,2
Water Solubility of Wood
This standard is issued under the fixed designation D1110; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 These test methods cover the determination of the water solubility of wood. Two methods are given, as follows:
1.1.1 Method A—Cold-Water Solubility—This method provides a measure of the tannins, gums, sugars, and coloring matter in the
wood.
1.1.2 Method B—Hot-Water Solubility—This method provides a measure of the tannins, gums, sugars, coloring matter, and
starches in the wood.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Significance and Use
2.1 Cold water removes a part of such extraneous materials as tannins, gums, sugars, and coloring matters. Hot water removes
these plus the starches.
METHOD A—COLD-WATER SOLUBILITY
3. Apparatus
3.1 Filtering Crucibles—Alundum or fritted-glass crucibles of coarse porosity will be required.
3.2 Filtering Flask—A suction filtering flask, equipped with a rubber flange for the crucible and funnel, shall be provided.
These test methods are under the jurisdiction of ASTM Committee D07 on Wood and are the direct responsibility of D07.01 on Fundamental Test Methods and Properties.
Current edition approved Aug. 1, 2013April 1, 2021. Published September 2013April 2021. Originally approved in 1950. Last previous edition approved in 20072013 as
D1110 – 84 (2007).(2013). DOI: 10.1520/D1110-84R13.10.1520/D1110-21.
Based upon Technical Association of the Pulp and Paper Industry Standard Method T 207 om-08 Water Solubility of Wood and Pulp.
For further information on these test methods, the following references may be consulted:
Schorger, A. W., “Chemistry of Cellulose and Woods,” 1926, p. 506, McGraw-Hill, NY.
Hawley and Wise, “Chemistry of Wood,” 1926, p. 134, Chemical Catalog Co., NY.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D1110 − 21
4. Test Specimen
4.1 The test specimen shall consist of 2 g of air-dried sawdust or milled wood that has been ground to pass through a 425-μm
(approx. 40 mesh) sieve and be retained on a 250-μm (approx. 60 mesh) sieve.
5. Procedure
5.1 Place a 2-g test specimen, the moisture content of which has been previously determined, in a 400-mL beaker, and cover with
300 mL of distilled water. Let this mixture digestsolvate at a temperature of 23 6 2°C, 2 °C, with frequent stirring, for 48 h.
5.2 Filter the material on an Alundum or fritted-glass
...








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