Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method

SIGNIFICANCE AND USE
5.1 The ICN value determined by this test method provides a measure of the ignition characteristics of diesel fuel oil used in compression ignition engines.  
5.2 This test can be used by engine manufacturers, petroleum refiners, fuel producers and in commerce as a specification aid to relate or match fuels and engines.  
5.3 The relationship of diesel fuel ICN determinations to the full scale, variable speed, variable load diesel engine is not completely understood.  
5.4 This test can be applied to non-conventional diesel fuels.  
5.5 This test determines ICN; it requires a sample of approximately 40 mL and a test time of approximately 25 min.  
5.6 This test method is based on the Energy Institute Test Method IP 617.
SCOPE
1.1 This test method covers the quantitative determination of the indicated cetane number (ICN) of conventional diesel fuel oils, and diesel fuel oils containing cetane number improver additives; it is applicable to products typical of Specification D975, Grades No.1-D and 2-D diesel fuel oils, European standard EN 590, and Canadian standards CAN/CGSB-3.517 and CAN/CGSB-3.520. The test method is also applicable to biodiesel, blends of diesel fuel oils containing biodiesel material (for example, materials as specified in Specifications D975, D6751, D7467 and European standards EN 14214, EN 16734, and EN 16709), diesel fuels from non-petroleum origin, hydrocarbon oils, diesel fuel oil blending components, aviation turbine fuels, and polyoxymethylene dimethyl ether (OME).  
1.2 This test method utilizes a constant volume combustion chamber (CVCC) with direct fuel injection into heated compressed air. The apparatus is calibrated using blends of reference fuels. ICN is determined directly from ignition delay using an instrument specific reference fuel calibration curve.  
1.3 This test method and its precision cover the calibrated range of 35 ICN to 85 ICN, inclusive. The analyzer can measure ICN outside the calibrated range, but the precision has not been determined.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in Section 7 on Hazards.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D8183-22 - Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8183 − 22
Standard Test Method for
Determination of Indicated Cetane Number (ICN) of Diesel
Fuel Oils using a Constant Volume Combustion Chamber—
1
Reference Fuels Calibration Method
This standard is issued under the fixed designation D8183; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 This test method covers the quantitative determination
ization established in the Decision on Principles for the
of the indicated cetane number (ICN) of conventional diesel
Development of International Standards, Guides and Recom-
fuel oils, and diesel fuel oils containing cetane number im-
mendations issued by the World Trade Organization Technical
prover additives; it is applicable to products typical of Speci-
Barriers to Trade (TBT) Committee.
fication D975, Grades No.1-D and 2-D diesel fuel oils,
European standard EN 590, and Canadian standards CAN/
2. Referenced Documents
CGSB-3.517 and CAN/CGSB-3.520. The test method is also
2
2.1 ASTM Standards:
applicable to biodiesel, blends of diesel fuel oils containing
D613 Test Method for Cetane Number of Diesel Fuel Oil
biodiesel material (for example, materials as specified in
D975 Specification for Diesel Fuel
Specifications D975, D6751, D7467 and European standards
D1193 Specification for Reagent Water
EN 14214, EN 16734, and EN 16709), diesel fuels from
D3703 Test Method for Hydroperoxide Number of Aviation
non-petroleum origin, hydrocarbon oils, diesel fuel oil blend-
Turbine Fuels, Gasoline and Diesel Fuels
ing components, aviation turbine fuels, and polyoxymethylene
D4052 Test Method for Density, Relative Density, and API
dimethyl ether (OME).
Gravity of Liquids by Digital Density Meter
1.2 This test method utilizes a constant volume combustion
D4057 Practice for Manual Sampling of Petroleum and
chamber (CVCC) with direct fuel injection into heated com-
Petroleum Products
pressed air. The apparatus is calibrated using blends of refer-
D4175 Terminology Relating to Petroleum Products, Liquid
ence fuels. ICN is determined directly from ignition delay
Fuels, and Lubricants
using an instrument specific reference fuel calibration curve.
D4177 Practice for Automatic Sampling of Petroleum and
1.3 This test method and its precision cover the calibrated Petroleum Products
D5854 Practice for Mixing and Handling of Liquid Samples
range of 35 ICN to 85 ICN, inclusive. The analyzer can
measureICNoutsidethecalibratedrange,buttheprecisionhas of Petroleum and Petroleum Products
D6299 Practice for Applying Statistical Quality Assurance
not been determined.
and Control Charting Techniques to Evaluate Analytical
1.4 The values stated in SI units are to be regarded as
Measurement System Performance
standard. No other units of measurement are included in this
D6300 Practice for Determination of Precision and Bias
standard.
Data for Use in Test Methods for Petroleum Products,
1.5 This standard does not purport to address all of the
Liquid Fuels, and Lubricants
safety concerns, if any, associated with its use. It is the
D6708 Practice for StatisticalAssessment and Improvement
responsibility of the user of this standard to establish appro-
of Expected Agreement Between Two Test Methods that
priate safety, health, and environmental practices and deter-
Purport to Measure the Same Property of a Material
mine the applicability of regulatory limitations prior to use.
D6751 Specification for Biodiesel Fuel Blend Stock (B100)
Some specific hazards statements are given in Section 7 on
for Middle Distillate Fuels
Hazards.
D7467 Specification for Diesel Fuel Oil, Biodiesel Blend
(B6 to B20)
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of
2
Subcommittee D02.01 on Combustion Characteristics. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved July 1, 2022. Published August 2022. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2018. Last previous edition approved in 2018 as D8183 – 18. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D8183-22. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D8183 − 18 D8183 − 22
Standard Test Method for
Determination of Indicated Cetane Number (ICN) of Diesel
Fuel Oils using a Constant Volume Combustion Chamber—
1
Reference Fuels Calibration Method
This standard is issued under the fixed designation D8183; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This test method covers the quantitative determination of the indicated cetane number (ICN) of conventional diesel fuel oils,
and diesel fuel oils containing cetane number improver additives; it is applicable to products typical of Specification D975, Grades
No.1-D and 2-D diesel fuel oils, European standard EN 590, and Canadian standards CAN/CGSB-3.517 and CAN/CGSB-3.520.
The test method is also applicable to biodiesel, blends of diesel fuel oils containing biodiesel material (for example, materials as
specified in Specifications D975, D6751, D7467 and European standards EN 14214, EN 16734, and EN 16709), diesel fuels from
non-petroleum origin, hydrocarbon oils, diesel fuel oil blending components, aviation turbine fuels, and polyoxymethylene
dimethyl ether (OME).
1.2 This test method utilizes a constant volume combustion chamber (CVCC) with direct fuel injection into heated compressed
air. The apparatus is calibrated using blends of reference fuels. ICN is determined directly from ignition delay using an instrument
specific reference fuel calibration curve.
1.3 This test method and its precision cover the calibrated range of 35 ICN to 85 ICN, inclusive. The analyzer can measure ICN
outside the calibrated range, but the precision has not been determined.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use. Some specific hazards statements are given in Section 7 on Hazards.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D613 Test Method for Cetane Number of Diesel Fuel Oil
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.01 on Combustion Characteristics.
Current edition approved April 1, 2018July 1, 2022. Published May 2018August 2022. Originally approved in 2018. Last previous edition approved in 2018 as D8183 – 18.
DOI: 10.1520/D8183-18.10.1520/D8183-22.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8183 − 22
D975 Specification for Diesel Fuel
D1193 Specification for Reagent Water
D3703 Test Method for Hydroperoxide Number of Aviation Turbine Fuels, Gasoline and Diesel Fuels
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4175 Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D5854 Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measure-
ment System Performance
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and
Lubricants
...

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