SIST EN 14063-1:2005

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Thermal insulation products for buildings - In-situ formed expanded clay lightweight aggregate products - Part 1: Specification for the loose-fill products before installationToplotnoizolacijski materiali in proizvodi - Proizvodi iz ekspandiranega glinenega agregatnega proizvoda (LWA), oblikovani na mestu vgradnje - 1. del: Specifikacija za vezane in razsute proizvode pred vgradnjoProduits isolants thermiques pour le bâtiment - Isolation thermique formée en place a base de granulats légers d'argile expansée - Partie 1: Spécification des produits en vrac avant la mise en placeWärmedämmstoffe für Gebäude - An der Verwendungsstelle hergestellte Wärmedämmung aus Blähton-Leichtzuschlagsstoffen - Teil 1: Spezifikation für die Schüttdämmstoffe vor dem EinbauTa slovenski standard je istoveten z:EN 14063-1:2004SIST EN 14063-1:2005en91.100.60ICS:SLOVENSKI
STANDARDSIST EN 14063-1:200501-februar-2005







EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14063-1August 2004ICS 91.100.60 English versionThermal insulation materials and products - In-situ formedexpanded clay lightweight aggregate products (LWA) - Part 1:Specification for the loose-fill products before installationProduits isolants thermiques pour le bâtiment - Isolationthermique formée en place à base de granulats légersd'argile expansée (LWA) - Partie 1: Spécification desproduits en vrac avant la mise en oeuvreWärmedämmstoffe für Gebäude - An derVerwendungsstelle hergestellte Wärmedämmung ausBlähton-Leichtzuschlagsstoffen (LWA) - Teil 1:Spezifikation für die Schüttdämmstoffe vor dem EinbauThis European Standard was approved by CEN on 10 June 2004.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2004 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14063-1:2004: E



EN 14063-1:2004 (E) 2 Contents page Foreword.3 1 Scope.4 2 Normative references.4 3 Terms, definitions, symbols, units and abbreviated terms.5 4 Requirements.6 5 Test methods.8 6 Designation code.10 7 Evaluation of conformity.10 8 Marking and labelling.10 Annex A (normative)
Determination of the declared value of thermal conductivity.12 A.1 Introduction.12 A.2 Input data.12 A.3 Declared values.12 A.4 Indirect test results of thermal conductivity.13 Annex B (normative)
Preparation of test specimen for λλλλ-measurement.15 B.1 Sampling.15 B.2 Dividing of samples.15 B.3 Conditioning of samples.15 B.4 Test specimens.15 B.5 λλλλ-measurement.16 B.6 Actions after the λλλλ-measurement.16 B.7 Conversion of λλλλ.16 Annex C (normative)
Factory production control.17 Annex D (informative)
Example of the determination of the declared value of thermal conductivity for a product or a product group.18 Annex ZA (informative)
Clauses of this European Standard addressing the provisions of the EU Construction Products Directive.20 ZA.1 Scope and relevant characteristics.20 ZA.2 Procedures for attestation of conformity of loose fill expanded clay lightweight aggregate products.21 ZA.3 CE Marking and labelling.25 Bibliography.29



EN 14063-1:2004 (E) 3 Foreword This document (EN 14063-1:2004) has been prepared by Technical Committee CEN/TC 88 “Thermal insulating materials and products”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2005, and conflicting national standards shall be withdrawn at the latest by May 2006. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EU Directive(s). For relationship with EU Directive(s), see informative Annex ZA, which is an integral part of this document. This standard consists of two parts. The first part, which is the harmonised part satisfying the mandate, the CPD and is the basis for the CE marking, covers the products which are placed on the market. The second part, which is the non-harmonised part, covers the specification for the installed products. This European Standard is one of a series for mineral wool, expanded clay, expanded perlite, exfoliated vermiculite, polyurethane/polyisocyanurate, cellulose and urea formaldehyde in-situ formed insulation products used in buildings, but this standard may be used in other areas where appropriate. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.



EN 14063-1:2004 (E) 4 1 Scope This document specifies the requirements for loose-fill expanded clay lightweight aggregate products for in-situ installation in roofs, ceilings, floors and ground floors. This document is a specification for the insulation products before installation. This document also describes the product characteristics and includes procedures for testing, marking and labelling. This document does not specify the required level of a given property to be achieved by a product to demonstrate fitness for purpose in a particular application. The levels required for a given application are to be found in regulations or non-conflicting standards. This document does not specify performance requirements for airborne sound insulation and for acoustic absorption applications. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 932-1:1996, Tests for general properties of aggregates — Part 1: Methods for sampling. EN 932-2, Tests for general properties of aggregates — Part 2: Methods for reducing laboratory samples. EN 933-1, Tests for geometrical properties of aggregates — Part 1: Determination of particle size distribution — Sieving method. EN 1097-3, Tests for mechanical and physical properties of aggregates — Part 3: Determination of loose bulk density and voids. EN 1097-5, Tests for mechanical and physical properties of aggregates — Part 5: Determination of the water content by drying in a ventilated oven. EN 1097-10, Tests for mechanical and physical properties of aggregates — Part 10: Determination of water suction height. EN 12667:2001, Thermal performance of building materials and products — Determination of thermal resistance by means of guarded hot plate and heat flow meter methods — Products of high and medium thermal resistance. EN 13055-1:2002, Lightweight aggregates — Part 1: Lightweight aggregates for concrete, mortar and grout. EN 13055-2, Lightweight aggregates — Part 2: Lightweight aggregates for bituminous mixtures and surface treatments and for unbound and bound applications. EN 13172:2001, Thermal insulation products — Evaluation of conformity. EN 13501-1, Fire classification of construction products and building elements — Part 1: Classification using test data from reaction to fire tests. EN 13820, Thermal insulating materials for building applications — Determination of organic content.



EN 14063-1:2004 (E) 5 EN ISO 10456, Building materials and products — Procedures for determining declared and design thermal values (ISO 10456:1999). ISO 12491, Statistical methods for quality control of building materials and components. 3 Terms, definitions, symbols, units and abbreviated terms 3.1 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1.1 expanded clay lightweight aggregate insulation material or product composed of lightweight granular material having a cellular structure formed by expanding clay minerals by heat [prEN ISO 9229:1997] 3.1.2 settlement decrease of installed insulation thickness with time, expressed as a percentage of the initial installed thickness (after compaction if prescribed) 3.1.3 compaction mechanical compression (e.g. by vibrator) of the installed insulation layer, expressed as a percentage of the initial untreated layer thickness 3.1.4 level given value, which is the upper or lower limit of a requirement. The level is given by the declared value of the characteristic concerned 3.1.5 class combination of two levels of the same property, between which the performance shall fall, where the levels are given by the declared value of the characteristic concerned 3.2 Symbols, units and abbreviated terms Symbols and units used in this document: H is the water suction height mm k is a factor related to the number of test results available – λ10, dry is the thermal conductivity at 10 °C mean temperature after drying at (110 ± 5) °C
W/(m⋅K) λ90/90 is the 90 % fractile with a confidence level of 90 % for the thermal conductivity W/(m⋅K) λD is the declared thermal conductivity W/(m⋅K) λi
is one test result of thermal conductivity W/(m⋅K) λmean
is the mean thermal conductivity W/(m⋅K) n is the number of test results
– sλ
is the estimate of the standard deviation of the thermal conductivity W/(m⋅K) LD is the symbol of the declared level for loose bulk density PS is the symbol of the declared level for aggregate size CR is the symbol of the declared level for crushing resistance WH is the symbol of the declared level for water suction height



EN 14063-1:2004 (E) 6 Abbreviated terms used in this document: LWA is Lightweight Aggregate ITT is Initial Type Test FPC is Factory Production Control 4 Requirements 4.1 General Product properties shall be assessed in accordance with Clause 5. To conform with this document, products shall meet the requirements of 4.2, and the requirements of 4.3 as appropriate. This document gives requirements for two different groups of applications:  roof, ceiling and floor insulation;  insulation in ground floors. NOTE 1 The difference between the two applications lies in the requirement for water suction height in ground floors, whereas there should be no requirement for water suction height when the products are used for roof, ceiling and floor insulation. One test result on a product property is the average of the measured values on the number of test specimens given in Table 1. 4.2 For all applications 4.2.1 Thermal resistance and thermal conductivity Thermal resistance and thermal conductivity shall be based upon measurements carried out in accordance with EN 12667. The thermal values shall be determined in accordance with Annex A and declared by the manufacturer, according to the following:  the reference mean temperature shall be 10 °C;  the measured values shall be expressed with three significant figures;  the declared thermal values, shall be given as limit values representing at least 90 % of the production determined with a confidence level of 90 %;  the declared thermal resistance, RD, shall be calculated from the insulation thickness and the declared thermal conductivity, λD (see NOTE 1);  the value of thermal conductivity λ90/90 shall be rounded upwards to the nearest 0,001 W/(m·K) and declared as λD in levels with steps of 0,001 W/(m·K);  the value of thermal resistance, RD, shall be rounded downwards to the nearest 0,05 m²·K/W and declared in levels with steps of 0,05 m²·K/W. NOTE 1 The declaration of the installed thermal resistance for loose fill expanded clay LWA is described in prEN 14063-2.



EN 14063-1:2004 (E) 7 NOTE 2 A correlation between thermal conductivity and loose bulk density / particle size distribution, specific to manufacturer and each product can be used for indirect testing (see A.4). 4.2.2 Loose bulk density Loose bulk density shall be measured in accordance with EN 1097-3 and declared by the manufacturer in classes with steps of 5 kg/m3 up to a density of 400 kg/m3 and thereafter with steps of 10 kg/m3 and shall be in the range of ±15 % of the manufacturers declared value. The value shall be expressed in kg/m3. NOTE The dry loose bulk density for expanded clay LWA products will normally be in the range
150 kg/m3 to 800 kg/m3. 4.2.3 Particle size distribution 4.2.3.1 General Particle size distribution shall be measured in accordance with EN 933-1 and shall be declared in % by mass. 4.2.3.2 Aggregate size The pair of sieve sizes between which the main proportion of the particles lies shall designate the size and any undersize or oversize shall comply with 4.2.3.3 and 4.2.3.4. The sieve sizes in mm shall be selected from the specifications in EN 13055-2. NOTE Normally the aggregate size for expanded clay LWA products will be in the range 0 mm to 32 mm. 4.2.3.3 Undersize The content of undersize material shall not exceed 15 % by mass. 4.2.3.4 Oversize The content of oversize material shall not exceed 10 % by mass. 4.2.4 Reaction to fire Reaction to fire classification (Euroclasses) shall be determined in accordance with EN 13501-1. NOTE Expanded clay LWA as described in 3.1.1.1 of this document is classified without testing as a class A1 product in accordance with Commission Decision 96/603/EC as amended by decision 2000/605/EC. 4.2.5 Durability characteristics 4.2.5.1 General The appropriate durability characteristics have been considered and are covered in 4.2.5.2, 4.2.5.3 and 4.2.5.4. 4.2.5.2 Durability of reaction to fire against ageing/degradation The reaction to fire performance of expanded clay does not change with time. The product is classified without testing as a class A1 product in accordance with EN 13501-1.



EN 14063-1:2004 (E) 8 4.2.5.3 Durability of thermal resistance against ageing/degradation The thermal conductivity (4.2.1) of the product does not change with time and neither does the insulation thickness since any settlement (4.3.3) is negligible. 4.2.5.4 Durability of compression strength against ageing/degradation The compression strength of expanded clay does not change with time. The product is a clay mineral product burnt to clinkers in a stable structure. 4.3 For specific applications 4.3.1 General If there is no requirement for a property, described in 4.3, for a product in use, then the property need not be determined and declared by the manufacturer. 4.3.2 Crushing resistance Crushing resistance shall be measured in accordance with EN 13055-1:2002, Annex A, shall be expressed in N/mm2 and if declaration is required, declared by the manufacturer in levels with steps of 0,05 N/mm2 up to 1,0 N/mm2 and thereafter with steps of 0,1 N/mm2. 4.3.3 Settlement Settlement for expanded clay LWA's is negligible and need no measurement. 4.3.4 Water vapour transmission This property is not measured because the open structure of the final product itself offers no substantial resistance to the free movement of water vapour. See EN 12524. 4.3.5 Water suction height Water suction height shall be measured in accordance with EN 1097-10, expressed in mm. Declaration of water suction height is only required for application in contact with the ground. 4.3.6 Release of dangerous substances NOTE See Annex ZA. 5 Test methods 5.1 Sampling Sampling shall be carried out according to the procedures given in EN 932-1. 5.2 Conditioning The test specimens shall be dried to constant mass at (110 ± 5) °C according to EN 1097-5. NOTE Conditioning for measurements of thermal conductivity, see Annex B.



EN 14063-1:2004 (E) 9 5.3 Testing 5.3.1 General Table 1 gives the dimensions of the test specimens, the minimum number of measurements required to get one test result and any specific conditions, which are necessary. 5.3.2 Thermal conductivity Thermal conductivity shall be determined in accordance with EN 12667 under the following conditions:  at a mean temperature of (10 ± 0,3) °C;  the test specimen shall be prepared according to Annex B and to EN 12667. The thermal conductivity shall be declared by the manufacturer in accordance with Annex A. NOTE 1 Thermal conductivity may also be measured at mean temperatures other than 10 °C, providing that the accuracy of the relationship between temperature and thermal conductivity is sufficiently well documented. NOTE 2 The measured thermal conductivity, λ10, dry, may be converted to a value at the moisture content at 23 °C and 50% relative humidity provided that the accuracy of the relationship is sufficiently documented. Annex C gives the formula for the conversion to other conditions than λ10, dry. Table 1 — Test methods, test specimens and conditions Dimensions in millimetres Clause No. Title Test method Dimensions of test specimen Minimum number of measure-ments to get one test result Specific conditions 4.2.1 Thermal conductivity EN 12667 a ≥ 600 × 600 × 100 1 Measuring area ≥ 250 × 250 Thickness ≥ 100 4.2.2 Loose bulk density EN 1097-3 see EN 1097-3 3 - 4.2.3 Particle size distribution EN 933-1 see EN 933-1 3 - 4.2.4 Reaction to fire, organic content
EN 13820
see Annex ZA, Reaction to fire class A1 without testing 4.3.2 Crushing resistance EN 13055-1 see EN 13055-1 3 - 4.3.5 Water suction height EN 1097-10 see EN 1097-10 1 - a See Annex B for conditioning.



EN 14063-1:2004 (E) 10 6 Designation code A designation code for the product shall be given by the manufacturer. The following shall be included except when there is no requirement for a property described in 4.3:
Abbreviated term
– Expanded clay LWA Exp. clay LWA
– This EN standard number EN 14063-1
– Loose bulk density LD
– Particle size PS
– Crushing resistance CR –
Water suction height WH The designation code according to this document for an expanded clay lightweight aggregate product is illustrated by the following example: Exp. clay LWA EN 14063-1 – LD250 – PS(8-16) 7 Evaluation of conformity The manufacturer or his authorised representative shall be responsible for the conformity of his product with the requirements of this document. The evaluation of conformity shall be carried out in accordance with EN 13172 and shall be based on initial type testing (ITT), factory production control (FPC) by the manufacturer, including product assessment and tests on samples taken at the factory. ITT shall be carried out in accordance with EN 13172 for all characteristics declared. FPC testing shall be made for the characteristics listed in Annex C. If a manufacturer decides to group his products it shall be done in accordance with EN 13172. The minimum frequencies of tests in the factory production control shall be in accordance with Annex C of this document. When indirect testing is used, the correlation to direct testing shall be established in accordance with EN 13172. The manufacturer or his authorised representative shall make available, in response to a request, a certificate or declaration of conformity as appropriate. NOTE For the EC certificate and declaration of conformity, as appropriate, see ZA.2.2. 8 Marking and labelling Products conforming with this document shall be clearly marked, either on the label on the packaging or on the delivery note, with the following information:  product name or other identifying characteristic;  name or identifying mark and address of the manufacturer or his authorised representative;



EN 14063-1:2004 (E) 11  year of manufacture (the last two digits);  date of delivery, manufacturing plant and/or traceability code;  reaction to fire class;  declared thermal conductivity;  designation code as given in Clause 6;  quantity of material, in m3. NOTE For CE marking and labelling, see ZA.3.



EN 14063-1:2004 (E) 12 Annex A
(normative)
Determination of the declared value of thermal conductivity A.1 Introduction It is the responsibility of the manufacturer to determine the declared value of thermal conductivity. He will have to demonstrate conformity of the product to its declared value. The declared value of thermal conductivity of a product are the expected value of the property during an economically reasonable working life under normal conditions, assessed through measured data at reference conditions. A.2 Input data A.2.1 The manufacturer shall have at least ten test results for thermal conductivity, obtained from internal or external measurements in order to calculate the declared value. A.2.2
Out of the ten test results the manufacturer shall have at least three test results for thermal conductivity, obtained from internal or external direct measurements. The direct thermal conductivity measurements shall be carried out at regular intervals spread over a time period of the last twelve month. If less than three results are available, the time period may be extended, until three test results are reached, but with a maximum of three years within which the product and the production conditions have not changed significantly. A.2.3
If the manufacturer has established a correlation according to A.4 and the direct test results mentioned above comply with the correlation the following procedure can be used to supplement the direct tests under A.2.2. A weighting factor giving the direct test results ten times the weight of the indirect test results shall be used as shown in Annex D. The measurements shall be carried out at regular intervals spread over a time period of the last twelve month. A.2.4
For new products minimum three direct thermal conductivity test results shall be carried out spread over a minimum period of ten days. If these test results comply with an already established correlation, the direct test results may be supplemented by indirect test results from the same period. The declared values shall be calculated according to the method given in A.3 and shall be recalculated at intervals not exceeding three months of production. A.3 Declared values The derivation of the declared value, λD, from the calculated value, λ90/90, shall use the rules given in 4.2.1, which include the rounding conditions.



EN 14063-1:2004 (E) 13 Case where thermal conductivity are declared The declared value, λD, shall be derived from the calculated value, λ90/90, which are determined using the equations A.1 and A.2. λλλsk⋅+=mean90/90 (A.1) 1)(12−−=∑=nsnimeaniλλλ (A.2) Table A.1 — Values for k for one-sided 90 % tolerance interval with a confidence level of 90 % Number of test results k 3 4,26 5 2,74 7 2,33 10 2,07 11 2,01 12 1,97 13 1,93 14 1,90 15 1,87 16 1,84 17 1,82 18 1,80 19 1,78 20 1,77 22 1,74 24 1,71 25 1,70 30 1,66 35 1,62 40 1,60 45 1,58 50 1,56 100 1,47 300 1,39 500 1,36 2 000 1,32 For other numbers of test results use ISO 12491 or linear interpolation. A.4 Indirect test results of thermal conductivity Indirect test results can only be accepted if the manufacturer can demonstrate a correlation between the direct measured thermal conductivity [λ] in the one hand, and loose bulk density [ρ] and particle size [d] in the other hand on the following conditions, which shall all be fulfilled. The correlation may for instance be presented as: λ = A + B·ρ + C·d, where A, B and C is plant dependant constants. 1) The correlation shall be based on test results from a period within which the product and the production conditions have not changed significantly.



EN 14063-1:2004 (E) 14 2) The correlation shall be based on testing of minimum ten samples. 3) The correlation shall be established by regression analysis with a regression coefficient better than 0,9. 4) The correlation shall be updated at least once a year by adding at least one test result in the regression for thermal conductivity, density and particle size. No result shall be used more than once and no result shall be excluded. 5) The correlation can only be used within the measured density range. No extrapolation is allowed. 6) In case the product or production conditions change significantly a new correlation shall be established.



EN 14063-1:2004 (E) 15 Annex B
(normative)
Preparation of test specimen for λλλλ-measurement B.1 Sampling Sampling is carried out according to the procedures given in EN 932-1. Sample at least three times the amount of the test specimens. For LWA one of the following ways is normally used:  Sampling of packed aggregates, min. 100 L.  Sampling from stationary conveyor belts using a sampling frame. Repeat until min. 100 L is sampled in a bag.  Sampling at belt and chute discharge points using a sampling box. Repeat until min. 100 L is sampled in a bag.  Sampling from stockpiles, see EN 932-1:1996, Annex C. Min. 100 L should be sampled in a bag. B.2 Dividing of samples Divide the samples according to EN 932-2. Divide the bulk sample (samples in the bags) into a test sample that is 5 % to 25 % larger than required for the test specimen. If 2 specimens are required for the λ-measurement 2 test samples of the same size is made. Divide the samples using a riffle box or a rotary sample divider. The rotary sample divider is preferred. B.3 Conditioning of samples Dry the sample at (110 ± 5) °C to constant mass. Protect the sample from moisture pick-up and let it cool down in the laboratory one or two days before measuring of loose bulk density and preparation of test specimens for λ-measurement. In case of dispute, the test specimen shall be stored to constant mass at (23 ± 2) °C and (50 ± 5) % relative humidity after drying at (110 ± 5) °C to constant mass. B.4 Test specimens The dried sample is manually filled in the measuring frame, levelled b
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