SIST ISO 18400-203:2019
Soil quality - Sampling - Part 203: Investigation of potentially contaminated sites
Soil quality - Sampling - Part 203: Investigation of potentially contaminated sites
This document gives guidance on the:
— investigation of sites, where either it is known that soil contamination is present, or the presence of soil contamination is suspected;
— investigation of sites where no soil contamination is expected, but the soil quality is to be determined (e.g. to make sure that there is no contamination present);
— investigation in anticipation of a need to manage re-use or disposal of excavated soil which might be contaminated;
— collection of information that is necessary for risk assessment and/or the development of remedial action plans (e.g. whether remediation is required and suggestions as to how this might be best achieved).
Although the information on soil quality for the risk assessment and/or the development of remedial action plans is gathered by applying this document, it does not give guidance on the decisions and actions that follow from a site investigation, for example, risk assessment and decisions about the requirements for remediation (if any).
Qualité du sol - Échantillonnage - Partie 203: Investigation des sites potentiellement contaminés
Le présent document fournit des recommandations concernant:
— l'investigation de sites au niveau desquels la présence d'une contamination du sol est connue ou suspectée;
— l'investigation de sites au niveau desquels aucune contamination du sol n'est attendue, mais dont la qualité du sol doit être déterminée (par exemple pour s'assurer qu'aucune contamination n'est présente);
— l'investigation en prévision de la nécessité de gérer la réutilisation ou l'extraction de terre excavée susceptible d'être contaminée;
— la collecte des informations nécessaires à l'appréciation du risque et/ou à l'élaboration de plans d'assainissement (par exemple, pour déterminer si une remédiation est nécessaire et proposer le meilleur moyen d'y parvenir).
Bien que les informations sur la qualité du sol en vue de l'appréciation du risque et/ou de l'élaboration de plans d'assainissement soient collectées en appliquant le présent document, il ne fournit pas de recommandations concernant les décisions et les actions qui suivent l'investigation d'un site, par exemple l'appréciation du risque et les décisions concernant les exigences de remédiation (le cas échéant).
Kakovost tal - Vzorčenje - 203. del: Preiskava domnevno onesnaženih območij
Ta dokument podaja smernice glede:
– preiskav območij, za katera se ve, da so tla onesnažena ali
obstaja sum, da so tla onesnažena;
– preiskav območij, kjer onesnaženost tal ni pričakovana, vendar je treba določiti kakovost tal (npr. da se potrdi, da tla niso onesnažena);
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Čeprav se informacije o kakovosti tal za oceno tveganja in/ali načrte sanacijskih ukrepov zbirajo z uporabo tega dokumenta, ta ne podaja smernic glede odločitev in ukrepov, ki izhajajo iz preiskav območja, na primer ocene tveganja in odločitve o zahtevah za sanacijo (če obstajajo).
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-marec-2019
1DGRPHãþD
SIST ISO 10381-5:2006
.DNRYRVWWDO9]RUþHQMHGHO3UHLVNDYDGRPQHYQRRQHVQDåHQLKREPRþLM
Soil quality - Sampling - Part 203: Investigation of potentially contaminated sites
Qualité du sol - Échantillonnage - Partie 203: Investigation des sites potentiellement
contaminés
Ta slovenski standard je istoveten z: ISO 18400-203:2018
ICS:
13.080.05 Preiskava tal na splošno Examination of soils in
general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
INTERNATIONAL ISO
STANDARD 18400-203
First edition
2018-10
Soil quality — Sampling —
Part 203:
Investigation of potentially
contaminated sites
Qualité du sol — Échantillonnage —
Partie 203: Investigation des sites potentiellement contaminés
Reference number
©
ISO 2018
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
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ii © ISO 2018 – All rights reserved
Contents Page
Foreword .v
Introduction .vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Objectives . 2
4.1 General . 2
4.2 Definitions of objectives . 2
5 General strategy of site investigation . 3
5.1 General . 3
5.2 Scope of preliminary investigation . 6
5.3 Scope of exploratory investigation . 6
5.4 Scope of detailed site investigation . 7
6 Preliminary investigation . 7
6.1 General . 7
6.2 Development of the conceptual site model . 8
6.2.1 Overall conceptual site model . 8
6.2.2 Formulation of contamination-related hypotheses . 8
6.3 Reporting the preliminary investigation and the conceptual site model . 8
7 Design of intrusive investigations . 8
7.1 Overview . 8
7.2 General aspects of field work . 9
7.3 Overall design aspects . 9
7.3.1 General. 9
7.3.2 Design of site works .10
7.4 Sampling patterns and spacing for sampling soils .11
7.4.1 General.11
7.4.2 Judgemental sampling . .12
7.4.3 Systematic sampling .12
7.4.4 Detection of hotspots .13
7.4.5 Depth of sampling and the strata to be sampled . .13
7.4.6 Sample sizes .13
7.4.7 Sample types .13
7.4.8 Number of samples .13
7.5 Analytical and testing strategies .13
7.5.1 General.13
7.5.2 Analysis of soil samples .14
7.6 Quality assurance and quality control .15
8 Exploratory investigation .15
8.1 General .15
8.1.1 Basis of the exploratory investigation .15
8.1.2 Steps to be incorporated .15
8.1.3 Aspects to be considered when drawing up a strategy .15
8.2 Sampling strategy .16
8.2.1 General.16
8.2.2 Sampling locations .16
8.2.3 Depth of sampling .17
8.2.4 Selection of soil samples for analysis .17
8.2.5 Selecting parameters for testing and analysis .17
8.3 Evaluation of the exploratory investigation .18
8.3.1 Testing the hypotheses formulated during the preliminary investigation .18
8.3.2 Risk assessment . .18
8.3.3 Considering hypotheses by zone .18
8.3.4 Obtaining information on soil quality .18
8.3.5 Checking if investigation strategy is adequate .19
8.3.6 Re-examining the hypotheses .19
8.3.7 Examples indicating if the hypothesis should be revised or rejected .19
8.3.8 Possible actions if a hypothesis is not valid .20
8.4 Reporting the exploratory investigation .20
8.5 Determination of the need for a detailed site investigation.21
9 Detailed site investigation .21
9.1 General .21
9.2 Objectives and scope .22
9.2.1 Objectives .22
9.2.2 Major aspects to be considered in setting the scope and determining the
objectives .22
9.3 Investigation design.22
9.4 Sampling strategy .23
9.4.1 General.23
9.4.2 Sampling locations .23
9.4.3 Depth of sampling .23
9.4.4 Selecting parameters for testing and analysis .23
9.5 Evaluation of the detailed site investigation .24
9.6 Reporting .25
Annex A (informative) Contamination hypotheses .27
Annex B (informative) Methods of non-intrusive investigation .30
Bibliography .32
iv © ISO 2018 – All rights reserved
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see
www .iso .org/iso/foreword .html.
This document was prepared by Technical Committee ISO/TC 190, Soil quality, Subcommittee SC 2,
Sampling.
This first edition of ISO 18400-203, together with ISO 18400-104 and ISO 18400-202, cancels and
replaces ISO 10381-5:2005, which has been technically and structurally revised.
The new ISO 18400 series is based on a modular structure and cannot be compared to ISO 10381-5
clause by clause.
A list of all parts in the ISO 18400 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/members .html.
Introduction
This document is one of a series of standards dealing with various aspects of site investigation and
sampling. It is intended to be used in conjunction with the other parts of the ISO 18400 series. The role/
position of the individual standards within the total investigation programme is shown in Figure 1.
While serious cases of soil contamination mostly occur on urban and industrial sites, serious
contamination of agricultural land can also occur (for example, due to pesticides usage, long-term
irrigation and application of organic wastes). In addition, it is important to recognize that agricultural,
near-natural and wooded sites, etc. are sometimes developed on deposited wastes or suffer severe
aerial deposition when close to industrial sites. In such cases, a combination of the methodologies
described in ISO 18400-205 and in this document would be appropriate.
An understanding of the surface water, groundwater and soil gas regimes is essential to the assessment
of the potential risks to human health and safety and to other potential receptors including, for
example, groundwater resources. However, the provision of detailed guidance on the investigation of
groundwater, surface water and soil gas falls outside the scope of this document. For more information
on groundwater and surface water sampling, see ISO 5667. Guidance on the sampling of soil gas is
provided in ISO 18400-204.
vi © ISO 2018 – All rights reserved
NOTE 1 The numbers in circles in this figure define the key elements (1 to 7) of the investigation programme.
NOTE 2 This figure displays a generic process which can be amended when necessary.
Figure 1 — Links between the essential elements of an investigation programme
INTERNATIONAL STANDARD ISO 18400-203:2018(E)
Soil quality — Sampling —
Part 203:
Investigation of potentially contaminated sites
1 Scope
This document gives guidance on the:
— investigation of sites, where either it is known that soil contamination is present, or the presence of
soil contamination is suspected;
— investigation of sites where no soil contamination is expected, but the soil quality is to be determined
(e.g. to make sure that there is no contamination present);
— investigation in anticipation of a need to manage re-use or disposal of excavated soil which might be
contaminated;
— collection of information that is necessary for risk assessment and/or the development of remedial
action plans (e.g. whether remediation is required and suggestions as to how this might be best
achieved).
Although the information on soil quality for the risk assessment and/or the development of remedial
action plans is gathered by applying this document, it does not give guidance on the decisions and
actions that follow from a site investigation, for example, risk assessment and decisions about the
requirements for remediation (if any).
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 11074, Soil quality — Vocabulary
ISO 18400-104, Soil quality — Sampling — Part 104: Strategies
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 11074 and ISO 18400-104 apply.
NOTE When the definitions in these two standards differ, those in ISO 18400-104 take precedence.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https: //www .iso .org/obp
— IEC Electropedia: available at http: //www .electropedia .org/
4 Objectives
4.1 General
This document provides a framework for the various phases and stages in the investigation of
potentially contaminated sites. The resulting determination of the contamination status can then
lead to risk assessment and, where necessary, facilitate the selection and application of appropriate
remedial actions. Guidance on data and information requirements for particular purposes is provided
in a number of International Standards including ISO 11504, ISO 15175, ISO 15176, ISO 15799 and
ISO 15800.
Investigations for contamination could be required:
— when the purpose is to identify and deal with contamination (e.g. site where it is known or believed
there might be unacceptable risks to humans or other receptors – sometimes called “problem” sites);
— incidental to plans for the redevelopment of sites (e.g. of an industrial site for housing); or
— especially in urban areas, because it is known that possibly contaminated soils will have to be
excavated and removed from the site (e.g. because basements are to be formed, utilities installed or
underground infrastructure built).
The guidance provided in this document should be adapted as appropriate for these and any other
circumstances where potential contamination is an issue.
NOTE 1 Contamination is defined in ISO 11074 as a result of human influences; however, the methods
described for investigation are also applicable where there are naturally high concentrations of potentially
harmful substances.
NOTE 2 With respect to remediation, this document only provides guidance on the information required in
general. Specific remediation methods could need additional information.
NOTE 3 This document deals only with the investigation of the ground. On old urban and industrial sites,
there could be derelict buildings and/or industrial plants awaiting demolition, dismantling or refurbishment.
Failure to investigate these buildings before demolition could put the safety of workers at risk or lead to the
spread of contamination on and around the site. The investigation of derelict buildings or remnant foundations
falls outside the scope of this document.
NOTE 4 In many situations, there is a close relation between the contamination of the soil, groundwater, soil
gas and, to a lesser extent, surface water. Consequently, an understanding of the surface water, groundwater
and soil gas regimes is essential to the assessment of the potential risks to human health and safety and to other
potential receptors including, for example, groundwater resources. However, the provision of detailed guidance
on the investigation of groundwater, surface water and soil gas falls outside the scope of this document. For more
information on groundwater and surface water sampling, see ISO 5667. Guidance on the sampling of soil gas is
provided in ISO 18400-204.
4.2 Definitions of objectives
The reasons for an investigation and hence the objectives can vary widely but are generally to:
— identify and assess the risks to those using the site, and in the event of redevelopment, to subsequent
users and occupiers of the site;
— identify and assess the risks presented to the environment including adjacent land, surface and
groundwater, ecosystems and public health;
— identify and assess the risks which could be presented to workers who are involved in investigation,
remediation, redevelopment or maintenance of the site;
— enable proper management of excavated materials especially on urban sites;
— identify and assess the potential for adverse effects on building materials;
2 © ISO 2018 – All rights reserved
so that decisions can be made about the importance of the risks and whether it is necessary to take any
form of action to deal with them.
From the principal objectives of the investigation, a number of subsidiary objectives can be derived.
These might include the following:
a) determine if any immediate action is required to protect exposed receptors;
b) identify compounds that are, or might be, present that might represent a risk to one or more actual
or potential receptors;
c) identify receptors (e.g. human, ecosystems, groundwater) that are or might in the future be at risk;
d) identify pathways by which particular receptors might be exposed to the contaminants;
e) provide the data and other information to use in a risk assessment;
f) provide information to aid the design of protective or remedial measures;
g) provide information to aid the management of excavated soil and other materials;
h) enable characterization of contaminated soil and other materials to ensure safe and suitable
handling and disposal;
i) provide reference data against which the achievement of remediation performance can be judged;
j) enable judgements to be made about the likely impact of continued use of the site on the environment
including soil quality;
k) provide information to assess the risk of (legal) environmental liabilities and the effect on the value
of the property.
These generalized objectives will be formulated into specific requirements depending upon the purpose
of the investigation.
EXAMPLE A site investigation prior to the purchase of a site for redevelopment could have one or more of
the following objectives:
— establish the history of the site and the potential for the presence of contamination;
— establish the nature, extent and distribution of contamination within the site boundaries;
— identify the potential for migration of contamination beyond the site boundaries including surface and
groundwater (this could indicate there are potential legal environmental liabilities);
— identify any immediate dangers to public health, safety, and the environment;
— identify contamination-related constraints in relation to a proposed development (e.g. human and
environmental risks) and any remedial works necessary and provide data from which to develop cost
estimates;
— provide information to facilitate the formulation of a full interpretative report with conclusions,
recommendations and budget costing for remedial actions, if required;
— provide information to facilitate the advice to the client about how to address the issues raised by any off-site
migration of contamination.
5 General strategy of site investigation
5.1 General
Determination of the extent of a contaminated area and, particularly, the assessment of human and
environmental risks caused by contamination can be complex. Because of this complexity, the process
of identifying, quantifying and evaluating the risks associated with contaminated land should be an
iterative process with several phases of investigation (each with specific objectives to be achieved),
in order to obtain sufficient relevant data to characterize the potential risks, pathways and receptors
of concern. The objectives should be reconsidered at each stage, and the requirements for further
investigation reviewed as the investigatory and assessment processes are developed.
NOTE 1 General guidance on the development of site investigation strategies and sampling strategies is
provided in ISO 18400-104. Guidance on the preparation of a sampling plan is provided in ISO 18400-101.
The principal phases are
— preliminary investigation (see 5.2 and Clause 6),
— exploratory investigation (see 5.3, Clause 7 and Clause 8), and
— detailed (main) site investigation (see 5.4, Clause 7 and Clause 9).
The relationship between these phases is illustrated in Figure 2.
Supplementary investigations could be required subsequent to the detailed site investigation in order
to provide information relevant to the selection of remedial methods, or design of remediation or
construction works.
On completion of the on-site work during any phase or stage of investigation, a sampling report should
be prepared in accordance with ISO 18400-107.
Following completion of any phase or stage of investigations, a report giving its results should be
prepared (see 8.4 and 9.6).
4 © ISO 2018 – All rights reserved
Clause 6
No
No
No
Figure 2 — Process of site investigation
Before embarking on any phase or stage of investigation, it is important to set data quality objectives
in terms of the type, quantity and quality (e.g. analytical quality) of the data and other information that
is to be collected. These data quality objectives will depend in part on the nature of the decisions to be
made on the basis of the investigation, and the confidence required in those decisions. The strategy for
the investigation (whether preliminary, exploratory or detailed) will be determined by the objectives.
For example, the different requirements of site investigations for the purpose of selling, determining
whether contamination is present as suspected, or redevelopment will influence the spacing of sample
locations and the number of samples analysed, and hence the cost of the investigation.
Failure to set data quality objectives at the outset can lead to considerable waste of money, if, for
example, the data collected are not suitable or sufficient for a reliable risk assessment, or leave too
many uncertainties about the “conceptual site model” developed for the site (see 6.2 for the description
of the conceptual site model).
When deciding on the strategy, consideration should be given to the applicability and use of on-site
analysis and/or in situ measurement techniques.
NOTE 2 Guidance on the selection and application of on-site methods is provided in ISO 12404.
5.2 Scope of preliminary investigation
The preliminary investigation comprises a desk study and site reconnaissance (walk-over survey,
site inspection). It is carried out using historical records and other sources to obtain information on
the past and present usage of the site together with information about local soil properties, geology,
geomorphology, pedology, surface hydrology, hydrogeology and environmental setting. It should be
carried out in accordance with ISO 18400-202 and the guidance in Clause 6.
From this preliminary investigation, the possibility of contamination can be deduced, and hypotheses
can be formulated on the nature, location and distribution of the contamination, such as those listed in
Annex A.
These hypotheses form part of the overall conceptual site model of the site that should be developed,
encompassing not only the contamination aspects but also the geology, geomorphology, pedology,
hydrogeology, surface hydrology, geotechnical properties and the environmental setting. The current
and planned site uses are also important aspects of the conceptual site model.
NOTE Guidance on the development of conceptual site models is provided in ISO 18400-202.
The preliminary investigation should provide sufficient information:
— for initial conclusions about potential risks to actual or potential human and other receptors;
— to determine whether there is a need for further action (e.g. intrusive investigation).
The amount and type of information required will depend on the objectives of the investigation. The
amount of work required will vary with the age of the site, the complexity of its historic usage, and the
complexity of the underlying geology, etc.
It should be remembered that the contamination on a site could be more complex than initially indicated
(for example, by current usage) and adequate information on the history of the site should always be
obtained in the preliminary investigation.
5.3 Scope of exploratory investigation
The exploratory investigation involves a limited on-site investigation, including collecting samples of
soil or fill, surface water, groundwater, and soil gas, where appropriate, and the subsequent analysis or
testing of the collected samples. The data and information produced are then assessed to determine if
the hypotheses from the preliminary investigation are correct, and, where appropriate, to test other
aspects of the conceptual site model. An exploratory investigation can identify areas of contamination
(essentially a qualitative process) but would not be sufficient to identify its extent or the variation of
contamination within it (i.e. quantify the contamination), which is the function of the detailed site
investigation.
In some cases, where the information required according to the objectives has been achieved
sufficiently, no further investigation might be needed. However, it could become apparent as a result
6 © ISO 2018 – All rights reserved
of the exploratory site investigation, for example, that the contamination pattern is more complex,
or concentrations of contamination are higher than anticipated, and already present, or in the future
might present, a hazard(s) and hence a risk to one or more potential receptor. In this situation, the
information obtained might be insufficient to make decisions with a satisfactory degree of confidence,
and it will be necessary to either
— carry out a further stage of exploratory investigation before proceeding to the design and execution
of a detailed investigation, or
— carry out a detailed site investigation to produce sufficient information to enable a full risk
assessment to be carried out, the need for protective or remedial measures to be determined, and
in due course and possibly following further stages of investigation, to select, design and apply
protective or remedial measures.
5.4 Scope of detailed site investigation
The detailed site investigation provides the basis for the quantitative determination of the amount
and spatial distribution of contaminants, their mobile and mobilizable fractions and possibilities of
them spreading in the environment. This includes possible future development of the contamination
situation.
It could require, depending on the objectives, the collection and analysis of soil or fill, surface water,
groundwater, and soil gas samples in order to obtain the information necessary to enable a full
assessment of the risks presented by the contamination to humans and other potential receptors, and
also to enable appropriate containment or remediation actions to be identified, together when required
with an initial estimate of costs. The intrusive investigation can be supported by model calculations and
investigation techniques that do not require samples to be taken such as those described in Annex B.
Detailed design of protective or remedial works could require further supplementary investigation.
NOTE It could be appropriate to investigate ambient air, vegetation, potable water supplies and a variety of
other media depending on the findings of the preliminary investigation.
The amount and nature of the information required from the detailed site investigation (or any particular
stage of it) will vary depending on the nature of the site, and the objectives of the investigation. The
implications for the decisions on what actions should be implemented on a site will vary from site to
site. Additionally, the amount and quality of the information required will also vary according to the
requirements of the decision making processes (e.g. the risk assessment, decisions regarding the need
for and type of remedial actions). All parties involved in the decision making process should be kept
fully informed as information is produced to ensure that the information is sufficient for the purpose
intended.
After completion of the interpretation of the information generated, including any risk assessment, it
should be possible to determine whether protective or remedial measures are required and to make
generalizations about the type of measures that might be appropriate.
6 Preliminary investigation
6.1 General
A preliminary investigation in accordance with ISO 18400-202 should be carried out before any
intrusive or other field investigation.
The results of the preliminary investigation should be used to prepare an initial conceptual site model,
including the development of contamination-related hypotheses, as described in 6.2.2 and Annex A.
6.2 Development of the conceptual site model
6.2.1 Overall conceptual site model
The conceptual site model is a representation and/or description of the site incorporating all that is
known and anticipated about the site (e.g. contamination, geology, pedology, environmental setting).
It should identify pathways by which current and future receptors could be affected by contamination
currently or in the future. An important aspect of the conceptual site model is the formulation of
contamination-related hypotheses. Note that its preparation requires some interpretation of the
available information and explicit recognition of the uncertainties in that information.
The development of a conceptual site model can aid greatly understanding of the site and the risks it
might present to human and other receptors as well as the design of future phases of investigation. It
also aids decisions on how remediation (if required) might be achieved and other works carried out.
The conceptual site model is also an aid to communication between the different parties involved and
with the public.
6.2.2 Formulation of contamination-related hypotheses
Based on the results of the preliminary investigation, hypotheses should be formulated in relation to the
probable nature, variation and spatial distribution of contaminating substances that are anticipated on
the site (see Annex A). In arriving at appropriate hypotheses, it will be frequently necessary to identify
different zones of a site to which different hypotheses are applicable. This will normally be essential for
a large site but is also frequently appropriate for small sites.
Before deciding on the sampling strategy, it is essential to determine for each zone (and for the site
as a whole) from the information available, whether it is reasonable to expect the zone or site to be
contaminated or not, i.e. whether the zone (or site) should be considered as “probably uncontaminated”
or as “probably contaminated”.
Hypotheses relating to individual substances should be developed, it can then be incorporated into a
conceptual site model, taking into account all the information available, and translating the information
into the most likely overall scenario with respect to the contamination status of a zone. The conceptual
site models for individual zones can be combined into a conceptual site model for the site as a whole.
This site-wide conceptual site model is used to design the sampling strategy to be employed in the next
phase or stage of investigation.
6.3 Reporting the preliminary investigation and the conceptual site model
The preliminary investigation should be reported in such a way that the initial formulation of the
conceptual site model and individual hypotheses will stand out as a clearly recognizable, identifiable,
section of the report as described in ISO 18400-202:2018, Clause 9.
7 Design of intrusive investigations
7.1 Overview
This clause, which should be applied in conjunction with ISO 18400-104, provides guidance applicable
to the design of all types of intrusive investigations of potentially contaminated sites (e.g. exploratory
and detailed investigations). Subsequent sections provide guidance relating to specific types of
investigation. Guidance is provided on overall design, sampling soils, preparation of laboratory
composite samples, and analytical and testing strategies.
8 © ISO 2018 – All rights reserved
7.2 General aspects of field work
It is important to understand that field work on contaminated sites can present a significant risk to the
health of the investigators. ISO 18400-103 should be consulted for further information on the possible
risks and precautions to control those risks.
ISO 18400-102, ISO 18400-104 and ISO 18400-105 should be consulted for information on specific
aspects of sampling including sampling patterns, methods of collecting samples including boreholes,
probe holes and trial pits, sample preservation, and the potential risks to investigators and the
environment which could result from a site investigation. It should be noted that other, non-intrusive,
investigation techniques can contribute significantly to the understanding of the spatial distribution of
contamination (see Annex B).
Instead of taking samples for laboratory analysis, it might be advantageous to use on-site and/or in situ
methods for testing and analysis (see ISO 12404 and ISO 13196).
Once the investigation has been designed and planned (7.3.2.1) a sampling plan should be prepared in
accordance with ISO 18400-101.
It is advisable to ensure from the start of the field work that sufficient samples will be collected. It
will sometimes not be necessary to analyse all the samples that have been taken, but that it could be
(very) expensive to have to return to the location to obtain additional samples. This will particularly
be the case if samples are taken at a considerable depth in the soil profile. However, analysis for volatile
and semi-volatile components should be carried out as quickly as possible after sampling, and for these
c
...
INTERNATIONAL ISO
STANDARD 18400-203
First edition
2018-10
Soil quality — Sampling —
Part 203:
Investigation of potentially
contaminated sites
Qualité du sol — Échantillonnage —
Partie 203: Investigation des sites potentiellement contaminés
Reference number
©
ISO 2018
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
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ii © ISO 2018 – All rights reserved
Contents Page
Foreword .v
Introduction .vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Objectives . 2
4.1 General . 2
4.2 Definitions of objectives . 2
5 General strategy of site investigation . 3
5.1 General . 3
5.2 Scope of preliminary investigation . 6
5.3 Scope of exploratory investigation . 6
5.4 Scope of detailed site investigation . 7
6 Preliminary investigation . 7
6.1 General . 7
6.2 Development of the conceptual site model . 8
6.2.1 Overall conceptual site model . 8
6.2.2 Formulation of contamination-related hypotheses . 8
6.3 Reporting the preliminary investigation and the conceptual site model . 8
7 Design of intrusive investigations . 8
7.1 Overview . 8
7.2 General aspects of field work . 9
7.3 Overall design aspects . 9
7.3.1 General. 9
7.3.2 Design of site works .10
7.4 Sampling patterns and spacing for sampling soils .11
7.4.1 General.11
7.4.2 Judgemental sampling . .12
7.4.3 Systematic sampling .12
7.4.4 Detection of hotspots .13
7.4.5 Depth of sampling and the strata to be sampled . .13
7.4.6 Sample sizes .13
7.4.7 Sample types .13
7.4.8 Number of samples .13
7.5 Analytical and testing strategies .13
7.5.1 General.13
7.5.2 Analysis of soil samples .14
7.6 Quality assurance and quality control .15
8 Exploratory investigation .15
8.1 General .15
8.1.1 Basis of the exploratory investigation .15
8.1.2 Steps to be incorporated .15
8.1.3 Aspects to be considered when drawing up a strategy .15
8.2 Sampling strategy .16
8.2.1 General.16
8.2.2 Sampling locations .16
8.2.3 Depth of sampling .17
8.2.4 Selection of soil samples for analysis .17
8.2.5 Selecting parameters for testing and analysis .17
8.3 Evaluation of the exploratory investigation .18
8.3.1 Testing the hypotheses formulated during the preliminary investigation .18
8.3.2 Risk assessment . .18
8.3.3 Considering hypotheses by zone .18
8.3.4 Obtaining information on soil quality .18
8.3.5 Checking if investigation strategy is adequate .19
8.3.6 Re-examining the hypotheses .19
8.3.7 Examples indicating if the hypothesis should be revised or rejected .19
8.3.8 Possible actions if a hypothesis is not valid .20
8.4 Reporting the exploratory investigation .20
8.5 Determination of the need for a detailed site investigation.21
9 Detailed site investigation .21
9.1 General .21
9.2 Objectives and scope .22
9.2.1 Objectives .22
9.2.2 Major aspects to be considered in setting the scope and determining the
objectives .22
9.3 Investigation design.22
9.4 Sampling strategy .23
9.4.1 General.23
9.4.2 Sampling locations .23
9.4.3 Depth of sampling .23
9.4.4 Selecting parameters for testing and analysis .23
9.5 Evaluation of the detailed site investigation .24
9.6 Reporting .25
Annex A (informative) Contamination hypotheses .27
Annex B (informative) Methods of non-intrusive investigation .30
Bibliography .32
iv © ISO 2018 – All rights reserved
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see
www .iso .org/iso/foreword .html.
This document was prepared by Technical Committee ISO/TC 190, Soil quality, Subcommittee SC 2,
Sampling.
This first edition of ISO 18400-203, together with ISO 18400-104 and ISO 18400-202, cancels and
replaces ISO 10381-5:2005, which has been technically and structurally revised.
The new ISO 18400 series is based on a modular structure and cannot be compared to ISO 10381-5
clause by clause.
A list of all parts in the ISO 18400 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/members .html.
Introduction
This document is one of a series of standards dealing with various aspects of site investigation and
sampling. It is intended to be used in conjunction with the other parts of the ISO 18400 series. The role/
position of the individual standards within the total investigation programme is shown in Figure 1.
While serious cases of soil contamination mostly occur on urban and industrial sites, serious
contamination of agricultural land can also occur (for example, due to pesticides usage, long-term
irrigation and application of organic wastes). In addition, it is important to recognize that agricultural,
near-natural and wooded sites, etc. are sometimes developed on deposited wastes or suffer severe
aerial deposition when close to industrial sites. In such cases, a combination of the methodologies
described in ISO 18400-205 and in this document would be appropriate.
An understanding of the surface water, groundwater and soil gas regimes is essential to the assessment
of the potential risks to human health and safety and to other potential receptors including, for
example, groundwater resources. However, the provision of detailed guidance on the investigation of
groundwater, surface water and soil gas falls outside the scope of this document. For more information
on groundwater and surface water sampling, see ISO 5667. Guidance on the sampling of soil gas is
provided in ISO 18400-204.
vi © ISO 2018 – All rights reserved
NOTE 1 The numbers in circles in this figure define the key elements (1 to 7) of the investigation programme.
NOTE 2 This figure displays a generic process which can be amended when necessary.
Figure 1 — Links between the essential elements of an investigation programme
INTERNATIONAL STANDARD ISO 18400-203:2018(E)
Soil quality — Sampling —
Part 203:
Investigation of potentially contaminated sites
1 Scope
This document gives guidance on the:
— investigation of sites, where either it is known that soil contamination is present, or the presence of
soil contamination is suspected;
— investigation of sites where no soil contamination is expected, but the soil quality is to be determined
(e.g. to make sure that there is no contamination present);
— investigation in anticipation of a need to manage re-use or disposal of excavated soil which might be
contaminated;
— collection of information that is necessary for risk assessment and/or the development of remedial
action plans (e.g. whether remediation is required and suggestions as to how this might be best
achieved).
Although the information on soil quality for the risk assessment and/or the development of remedial
action plans is gathered by applying this document, it does not give guidance on the decisions and
actions that follow from a site investigation, for example, risk assessment and decisions about the
requirements for remediation (if any).
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 11074, Soil quality — Vocabulary
ISO 18400-104, Soil quality — Sampling — Part 104: Strategies
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 11074 and ISO 18400-104 apply.
NOTE When the definitions in these two standards differ, those in ISO 18400-104 take precedence.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https: //www .iso .org/obp
— IEC Electropedia: available at http: //www .electropedia .org/
4 Objectives
4.1 General
This document provides a framework for the various phases and stages in the investigation of
potentially contaminated sites. The resulting determination of the contamination status can then
lead to risk assessment and, where necessary, facilitate the selection and application of appropriate
remedial actions. Guidance on data and information requirements for particular purposes is provided
in a number of International Standards including ISO 11504, ISO 15175, ISO 15176, ISO 15799 and
ISO 15800.
Investigations for contamination could be required:
— when the purpose is to identify and deal with contamination (e.g. site where it is known or believed
there might be unacceptable risks to humans or other receptors – sometimes called “problem” sites);
— incidental to plans for the redevelopment of sites (e.g. of an industrial site for housing); or
— especially in urban areas, because it is known that possibly contaminated soils will have to be
excavated and removed from the site (e.g. because basements are to be formed, utilities installed or
underground infrastructure built).
The guidance provided in this document should be adapted as appropriate for these and any other
circumstances where potential contamination is an issue.
NOTE 1 Contamination is defined in ISO 11074 as a result of human influences; however, the methods
described for investigation are also applicable where there are naturally high concentrations of potentially
harmful substances.
NOTE 2 With respect to remediation, this document only provides guidance on the information required in
general. Specific remediation methods could need additional information.
NOTE 3 This document deals only with the investigation of the ground. On old urban and industrial sites,
there could be derelict buildings and/or industrial plants awaiting demolition, dismantling or refurbishment.
Failure to investigate these buildings before demolition could put the safety of workers at risk or lead to the
spread of contamination on and around the site. The investigation of derelict buildings or remnant foundations
falls outside the scope of this document.
NOTE 4 In many situations, there is a close relation between the contamination of the soil, groundwater, soil
gas and, to a lesser extent, surface water. Consequently, an understanding of the surface water, groundwater
and soil gas regimes is essential to the assessment of the potential risks to human health and safety and to other
potential receptors including, for example, groundwater resources. However, the provision of detailed guidance
on the investigation of groundwater, surface water and soil gas falls outside the scope of this document. For more
information on groundwater and surface water sampling, see ISO 5667. Guidance on the sampling of soil gas is
provided in ISO 18400-204.
4.2 Definitions of objectives
The reasons for an investigation and hence the objectives can vary widely but are generally to:
— identify and assess the risks to those using the site, and in the event of redevelopment, to subsequent
users and occupiers of the site;
— identify and assess the risks presented to the environment including adjacent land, surface and
groundwater, ecosystems and public health;
— identify and assess the risks which could be presented to workers who are involved in investigation,
remediation, redevelopment or maintenance of the site;
— enable proper management of excavated materials especially on urban sites;
— identify and assess the potential for adverse effects on building materials;
2 © ISO 2018 – All rights reserved
so that decisions can be made about the importance of the risks and whether it is necessary to take any
form of action to deal with them.
From the principal objectives of the investigation, a number of subsidiary objectives can be derived.
These might include the following:
a) determine if any immediate action is required to protect exposed receptors;
b) identify compounds that are, or might be, present that might represent a risk to one or more actual
or potential receptors;
c) identify receptors (e.g. human, ecosystems, groundwater) that are or might in the future be at risk;
d) identify pathways by which particular receptors might be exposed to the contaminants;
e) provide the data and other information to use in a risk assessment;
f) provide information to aid the design of protective or remedial measures;
g) provide information to aid the management of excavated soil and other materials;
h) enable characterization of contaminated soil and other materials to ensure safe and suitable
handling and disposal;
i) provide reference data against which the achievement of remediation performance can be judged;
j) enable judgements to be made about the likely impact of continued use of the site on the environment
including soil quality;
k) provide information to assess the risk of (legal) environmental liabilities and the effect on the value
of the property.
These generalized objectives will be formulated into specific requirements depending upon the purpose
of the investigation.
EXAMPLE A site investigation prior to the purchase of a site for redevelopment could have one or more of
the following objectives:
— establish the history of the site and the potential for the presence of contamination;
— establish the nature, extent and distribution of contamination within the site boundaries;
— identify the potential for migration of contamination beyond the site boundaries including surface and
groundwater (this could indicate there are potential legal environmental liabilities);
— identify any immediate dangers to public health, safety, and the environment;
— identify contamination-related constraints in relation to a proposed development (e.g. human and
environmental risks) and any remedial works necessary and provide data from which to develop cost
estimates;
— provide information to facilitate the formulation of a full interpretative report with conclusions,
recommendations and budget costing for remedial actions, if required;
— provide information to facilitate the advice to the client about how to address the issues raised by any off-site
migration of contamination.
5 General strategy of site investigation
5.1 General
Determination of the extent of a contaminated area and, particularly, the assessment of human and
environmental risks caused by contamination can be complex. Because of this complexity, the process
of identifying, quantifying and evaluating the risks associated with contaminated land should be an
iterative process with several phases of investigation (each with specific objectives to be achieved),
in order to obtain sufficient relevant data to characterize the potential risks, pathways and receptors
of concern. The objectives should be reconsidered at each stage, and the requirements for further
investigation reviewed as the investigatory and assessment processes are developed.
NOTE 1 General guidance on the development of site investigation strategies and sampling strategies is
provided in ISO 18400-104. Guidance on the preparation of a sampling plan is provided in ISO 18400-101.
The principal phases are
— preliminary investigation (see 5.2 and Clause 6),
— exploratory investigation (see 5.3, Clause 7 and Clause 8), and
— detailed (main) site investigation (see 5.4, Clause 7 and Clause 9).
The relationship between these phases is illustrated in Figure 2.
Supplementary investigations could be required subsequent to the detailed site investigation in order
to provide information relevant to the selection of remedial methods, or design of remediation or
construction works.
On completion of the on-site work during any phase or stage of investigation, a sampling report should
be prepared in accordance with ISO 18400-107.
Following completion of any phase or stage of investigations, a report giving its results should be
prepared (see 8.4 and 9.6).
4 © ISO 2018 – All rights reserved
Clause 6
No
No
No
Figure 2 — Process of site investigation
Before embarking on any phase or stage of investigation, it is important to set data quality objectives
in terms of the type, quantity and quality (e.g. analytical quality) of the data and other information that
is to be collected. These data quality objectives will depend in part on the nature of the decisions to be
made on the basis of the investigation, and the confidence required in those decisions. The strategy for
the investigation (whether preliminary, exploratory or detailed) will be determined by the objectives.
For example, the different requirements of site investigations for the purpose of selling, determining
whether contamination is present as suspected, or redevelopment will influence the spacing of sample
locations and the number of samples analysed, and hence the cost of the investigation.
Failure to set data quality objectives at the outset can lead to considerable waste of money, if, for
example, the data collected are not suitable or sufficient for a reliable risk assessment, or leave too
many uncertainties about the “conceptual site model” developed for the site (see 6.2 for the description
of the conceptual site model).
When deciding on the strategy, consideration should be given to the applicability and use of on-site
analysis and/or in situ measurement techniques.
NOTE 2 Guidance on the selection and application of on-site methods is provided in ISO 12404.
5.2 Scope of preliminary investigation
The preliminary investigation comprises a desk study and site reconnaissance (walk-over survey,
site inspection). It is carried out using historical records and other sources to obtain information on
the past and present usage of the site together with information about local soil properties, geology,
geomorphology, pedology, surface hydrology, hydrogeology and environmental setting. It should be
carried out in accordance with ISO 18400-202 and the guidance in Clause 6.
From this preliminary investigation, the possibility of contamination can be deduced, and hypotheses
can be formulated on the nature, location and distribution of the contamination, such as those listed in
Annex A.
These hypotheses form part of the overall conceptual site model of the site that should be developed,
encompassing not only the contamination aspects but also the geology, geomorphology, pedology,
hydrogeology, surface hydrology, geotechnical properties and the environmental setting. The current
and planned site uses are also important aspects of the conceptual site model.
NOTE Guidance on the development of conceptual site models is provided in ISO 18400-202.
The preliminary investigation should provide sufficient information:
— for initial conclusions about potential risks to actual or potential human and other receptors;
— to determine whether there is a need for further action (e.g. intrusive investigation).
The amount and type of information required will depend on the objectives of the investigation. The
amount of work required will vary with the age of the site, the complexity of its historic usage, and the
complexity of the underlying geology, etc.
It should be remembered that the contamination on a site could be more complex than initially indicated
(for example, by current usage) and adequate information on the history of the site should always be
obtained in the preliminary investigation.
5.3 Scope of exploratory investigation
The exploratory investigation involves a limited on-site investigation, including collecting samples of
soil or fill, surface water, groundwater, and soil gas, where appropriate, and the subsequent analysis or
testing of the collected samples. The data and information produced are then assessed to determine if
the hypotheses from the preliminary investigation are correct, and, where appropriate, to test other
aspects of the conceptual site model. An exploratory investigation can identify areas of contamination
(essentially a qualitative process) but would not be sufficient to identify its extent or the variation of
contamination within it (i.e. quantify the contamination), which is the function of the detailed site
investigation.
In some cases, where the information required according to the objectives has been achieved
sufficiently, no further investigation might be needed. However, it could become apparent as a result
6 © ISO 2018 – All rights reserved
of the exploratory site investigation, for example, that the contamination pattern is more complex,
or concentrations of contamination are higher than anticipated, and already present, or in the future
might present, a hazard(s) and hence a risk to one or more potential receptor. In this situation, the
information obtained might be insufficient to make decisions with a satisfactory degree of confidence,
and it will be necessary to either
— carry out a further stage of exploratory investigation before proceeding to the design and execution
of a detailed investigation, or
— carry out a detailed site investigation to produce sufficient information to enable a full risk
assessment to be carried out, the need for protective or remedial measures to be determined, and
in due course and possibly following further stages of investigation, to select, design and apply
protective or remedial measures.
5.4 Scope of detailed site investigation
The detailed site investigation provides the basis for the quantitative determination of the amount
and spatial distribution of contaminants, their mobile and mobilizable fractions and possibilities of
them spreading in the environment. This includes possible future development of the contamination
situation.
It could require, depending on the objectives, the collection and analysis of soil or fill, surface water,
groundwater, and soil gas samples in order to obtain the information necessary to enable a full
assessment of the risks presented by the contamination to humans and other potential receptors, and
also to enable appropriate containment or remediation actions to be identified, together when required
with an initial estimate of costs. The intrusive investigation can be supported by model calculations and
investigation techniques that do not require samples to be taken such as those described in Annex B.
Detailed design of protective or remedial works could require further supplementary investigation.
NOTE It could be appropriate to investigate ambient air, vegetation, potable water supplies and a variety of
other media depending on the findings of the preliminary investigation.
The amount and nature of the information required from the detailed site investigation (or any particular
stage of it) will vary depending on the nature of the site, and the objectives of the investigation. The
implications for the decisions on what actions should be implemented on a site will vary from site to
site. Additionally, the amount and quality of the information required will also vary according to the
requirements of the decision making processes (e.g. the risk assessment, decisions regarding the need
for and type of remedial actions). All parties involved in the decision making process should be kept
fully informed as information is produced to ensure that the information is sufficient for the purpose
intended.
After completion of the interpretation of the information generated, including any risk assessment, it
should be possible to determine whether protective or remedial measures are required and to make
generalizations about the type of measures that might be appropriate.
6 Preliminary investigation
6.1 General
A preliminary investigation in accordance with ISO 18400-202 should be carried out before any
intrusive or other field investigation.
The results of the preliminary investigation should be used to prepare an initial conceptual site model,
including the development of contamination-related hypotheses, as described in 6.2.2 and Annex A.
6.2 Development of the conceptual site model
6.2.1 Overall conceptual site model
The conceptual site model is a representation and/or description of the site incorporating all that is
known and anticipated about the site (e.g. contamination, geology, pedology, environmental setting).
It should identify pathways by which current and future receptors could be affected by contamination
currently or in the future. An important aspect of the conceptual site model is the formulation of
contamination-related hypotheses. Note that its preparation requires some interpretation of the
available information and explicit recognition of the uncertainties in that information.
The development of a conceptual site model can aid greatly understanding of the site and the risks it
might present to human and other receptors as well as the design of future phases of investigation. It
also aids decisions on how remediation (if required) might be achieved and other works carried out.
The conceptual site model is also an aid to communication between the different parties involved and
with the public.
6.2.2 Formulation of contamination-related hypotheses
Based on the results of the preliminary investigation, hypotheses should be formulated in relation to the
probable nature, variation and spatial distribution of contaminating substances that are anticipated on
the site (see Annex A). In arriving at appropriate hypotheses, it will be frequently necessary to identify
different zones of a site to which different hypotheses are applicable. This will normally be essential for
a large site but is also frequently appropriate for small sites.
Before deciding on the sampling strategy, it is essential to determine for each zone (and for the site
as a whole) from the information available, whether it is reasonable to expect the zone or site to be
contaminated or not, i.e. whether the zone (or site) should be considered as “probably uncontaminated”
or as “probably contaminated”.
Hypotheses relating to individual substances should be developed, it can then be incorporated into a
conceptual site model, taking into account all the information available, and translating the information
into the most likely overall scenario with respect to the contamination status of a zone. The conceptual
site models for individual zones can be combined into a conceptual site model for the site as a whole.
This site-wide conceptual site model is used to design the sampling strategy to be employed in the next
phase or stage of investigation.
6.3 Reporting the preliminary investigation and the conceptual site model
The preliminary investigation should be reported in such a way that the initial formulation of the
conceptual site model and individual hypotheses will stand out as a clearly recognizable, identifiable,
section of the report as described in ISO 18400-202:2018, Clause 9.
7 Design of intrusive investigations
7.1 Overview
This clause, which should be applied in conjunction with ISO 18400-104, provides guidance applicable
to the design of all types of intrusive investigations of potentially contaminated sites (e.g. exploratory
and detailed investigations). Subsequent sections provide guidance relating to specific types of
investigation. Guidance is provided on overall design, sampling soils, preparation of laboratory
composite samples, and analytical and testing strategies.
8 © ISO 2018 – All rights reserved
7.2 General aspects of field work
It is important to understand that field work on contaminated sites can present a significant risk to the
health of the investigators. ISO 18400-103 should be consulted for further information on the possible
risks and precautions to control those risks.
ISO 18400-102, ISO 18400-104 and ISO 18400-105 should be consulted for information on specific
aspects of sampling including sampling patterns, methods of collecting samples including boreholes,
probe holes and trial pits, sample preservation, and the potential risks to investigators and the
environment which could result from a site investigation. It should be noted that other, non-intrusive,
investigation techniques can contribute significantly to the understanding of the spatial distribution of
contamination (see Annex B).
Instead of taking samples for laboratory analysis, it might be advantageous to use on-site and/or in situ
methods for testing and analysis (see ISO 12404 and ISO 13196).
Once the investigation has been designed and planned (7.3.2.1) a sampling plan should be prepared in
accordance with ISO 18400-101.
It is advisable to ensure from the start of the field work that sufficient samples will be collected. It
will sometimes not be necessary to analyse all the samples that have been taken, but that it could be
(very) expensive to have to return to the location to obtain additional samples. This will particularly
be the case if samples are taken at a considerable depth in the soil profile. However, analysis for volatile
and semi-volatile components should be carried out as quickly as possible after sampling, and for these
components it might not be possible to preserve the samples for later analysis.
If at any time during the investigation it becomes evident that the implemented strategy has not been
optimal (e.g. on the basis of site observations), the strategy should be altered immediately. In some
cases, it might be necessary to take additional samples on the basis of the adjusted strategy or to take
into account the unforeseen conditions. However, where this situation is not clearly evident, the original
strategy should be followed.
Whenever changes are required to the predetermined sampling plan, the project leader should be
informed or consulted as required by ISO 18400-101.
Descriptions of ground strata should be drawn up in the field immediately after work at a sampling
location has been completed if this has not been done during formation of the exploratory hole. Taking
photographs with boards showing the sampling location designation, colour charts and scale markers
is often a useful aid to ground strata descriptions.
7.3 Overall design aspects
7.3.1 General
The design of on-site (intrusive) investigations involving the collection of samples and on-site testing
(if any) should be based on the results of the preliminary investigation and th
...
NORME ISO
INTERNATIONALE 18400-203
Première édition
2018-10
Qualité du sol — Échantillonnage —
Partie 203:
Investigation des sites potentiellement
contaminés
Soil quality — Sampling —
Part 203: Investigation of potentially contaminated sites
Numéro de référence
©
ISO 2018
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Sommaire Page
Avant-propos .v
Introduction .vi
1 Domaine d’application . 1
2 Références normatives . 1
3 Termes et définitions . 1
4 Objectifs . 2
4.1 Généralités . 2
4.2 Définitions des objectifs . 2
5 Stratégie générale d’investigation d’un site . 4
5.1 Généralités . 4
5.2 Périmètre de l’investigation préliminaire . 6
5.3 Périmètre de l’investigation exploratoire . 6
5.4 Périmètre de l’investigation détaillée du site . 7
6 Investigation préliminaire . 7
6.1 Généralités . 7
6.2 Élaboration du schéma conceptuel du site . 8
6.2.1 Schéma conceptuel global du site . 8
6.2.2 Formulation d’hypothèses liées à la contamination . 8
6.3 Rapport sur l’investigation préliminaire et le schéma conceptuel du site . 8
7 Conception des investigations intrusives . 8
7.1 Vue d’ensemble . 8
7.2 Aspects généraux du travail sur le terrain . 9
7.3 Aspects relatifs à la conception globale . 9
7.3.1 Généralités . 9
7.3.2 Conception des travaux sur site .10
7.4 Schémas d’échantillonnage et espacement pour l’échantillonnage des sols .11
7.4.1 Généralités .11
7.4.2 Échantillonnage sur avis d’expert .12
7.4.3 Échantillonnage systématique .13
7.4.4 Détection des zones concentrées . .13
7.4.5 Profondeur d’échantillonnage et strates à échantillonner .13
7.4.6 Taille des échantillons .14
7.4.7 Types d’échantillons .14
7.4.8 Nombre d’échantillons.14
7.5 Stratégies d’analyse et d’essais .14
7.5.1 Généralités .14
7.5.2 Analyse des échantillons de sol .14
7.6 Assurance et contrôle de la qualité .15
8 Investigation exploratoire .15
8.1 Généralités .15
8.1.1 Base de l’inventaire exploratoire .15
8.1.2 Étapes à intégrer .16
8.1.3 Aspects à prendre en compte lors de l’élaboration d’une stratégie .16
8.2 Stratégie d’échantillonnage .17
8.2.1 Généralités .17
8.2.2 Emplacements d’échantillonnage .17
8.2.3 Profondeur d’échantillonnage .18
8.2.4 Sélection des échantillons de sol en vue de l’analyse.18
8.2.5 Sélection des paramètres pour les essais et l’analyse .18
8.3 Évaluation de l’investigation exploratoire.19
8.3.1 Vérification des hypothèses formulées lors de l’investigation préliminaire .19
8.3.2 Appréciation du risque .19
8.3.3 Étude des hypothèses par zone . .19
8.3.4 Obtention d’informations sur la qualité du sol .19
8.3.5 Vérification de l’adéquation de la stratégie d’investigation .19
8.3.6 Réexamen des hypothèses .20
8.3.7 Exemples indiquant s’il convient de réviser ou rejeter l’hypothèse .20
8.3.8 Actions possibles si une hypothèse n’est pas valable .21
8.4 Rapport de l’investigation exploratoire .21
8.5 Détermination de la nécessité d’une investigation détaillée du site .22
9 Investigation détaillée du site.22
9.1 Généralités .22
9.2 Objectifs et périmètre d’investigation .23
9.2.1 Objectifs .23
9.2.2 Principaux aspects à prendre en compte lors de la détermination du
périmètre et des objectifs.23
9.3 Conception de l’investigation .23
9.4 Stratégie d’échantillonnage .24
9.4.1 Généralités .24
9.4.2 Emplacements d’échantillonnage .24
9.4.3 Profondeur d’échantillonnage .25
9.4.4 Sélection des paramètres pour les essais et l’analyse .25
9.5 Évaluation de l’investigation détaillée du site.25
9.6 Rapport .26
Annexe A (informative) Hypothèses relatives à la contamination .28
Annexe B (informative) Méthodes d’investigation non intrusive .31
Bibliographie .34
iv © ISO 2018 – Tous droits réservés
Avant-propos
L’ISO (Organisation internationale de normalisation) est une fédération mondiale d’organismes
nationaux de normalisation (comités membres de l’ISO). L’élaboration des Normes internationales est
en général confiée aux comités techniques de l’ISO. Chaque comité membre intéressé par une étude
a le droit de faire partie du comité technique créé à cet effet. Les organisations internationales,
gouvernementales et non gouvernementales, en liaison avec l’ISO participent également aux travaux.
L’ISO collabore étroitement avec la Commission électrotechnique internationale (IEC) en ce qui
concerne la normalisation électrotechnique.
Les procédures utilisées pour élaborer le présent document et celles destinées à sa mise à jour sont
décrites dans les Directives ISO/IEC, Partie 1. Il convient, en particulier de prendre note des différents
critères d’approbation requis pour les différents types de documents ISO. Le présent document a été
rédigé conformément aux règles de rédaction données dans les Directives ISO/IEC, Partie 2 (voir www
.iso .org/directives).
L’attention est attirée sur le fait que certains des éléments du présent document peuvent faire l’objet de
droits de propriété intellectuelle ou de droits analogues. L’ISO ne saurait être tenue pour responsable
de ne pas avoir identifié de tels droits de propriété et averti de leur existence. Les détails concernant
les références aux droits de propriété intellectuelle ou autres droits analogues identifiés lors de
l’élaboration du document sont indiqués dans l’Introduction et/ou dans la liste des déclarations de
brevets reçues par l’ISO (voir www .iso .org/brevets).
Les appellations commerciales éventuellement mentionnées dans le présent document sont données
pour information, par souci de commodité, à l’intention des utilisateurs et ne sauraient constituer un
engagement.
Pour une explication de la nature volontaire des normes, la signification des termes et expressions
spécifiques de l’ISO liés à l’évaluation de la conformité, ou pour toute information au sujet de l’adhésion
de l’ISO aux principes de l’Organisation mondiale du commerce (OMC) concernant les obstacles
techniques au commerce (OTC), voir le lien suivant: www .iso .org/iso/fr/avant -propos.
Le présent document a été élaboré par le comité technique ISO/TC 190, Qualité du sol, sous-comité SC 2,
Échantillonnage.
Cette première édition de l’ISO 18400-203, associée à l’ISO 18400-104 et à l’ISO 18400-202, annule et
remplace l’ISO 10381-5:2005, qui a fait l’objet d’une révision technique et structurelle.
La nouvelle série ISO 18400 est fondée sur une structure modulaire et ne peut être comparée, article
par article, à l’ISO 10381-5.
Une liste de toutes les parties de la série ISO 18400 se trouve sur le site web de l’ISO.
Il convient que l’utilisateur adresse tout retour d’information ou toute question concernant le présent
document à l’organisme national de normalisation de son pays. Une liste exhaustive desdits organismes
se trouve à l’adresse www .iso .org/fr/members .html.
Introduction
Le présent document est l’une des normes d’une série traitant de divers aspects de l’investigation et de
l’échantillonnage de sites. Il est destiné à être utilisé conjointement avec les autres parties de la série
ISO 18400. Le rôle/la fonction de chaque norme au sein de l’ensemble du programme d’investigation est
illustré(e) à la Figure 1.
Bien que les cas graves de contamination des sols se produisent essentiellement au niveau de sites
urbains et industriels, une contamination importante des terrains agricoles peut également se produire
(par exemple en raison de l’usage de pesticides, d’une irrigation à long terme et de l’épandage de déchets
organiques). En outre, il est important de reconnaître que des sites agricoles, quasi naturels et boisés,
etc. sont parfois aménagés sur des décharges ou subissent d’importantes retombées atmosphériques
lorsqu’ils se situent à proximité de sites industriels. Dans ce cas, une combinaison des méthodologies
décrites dans l’ISO 18400-205 et dans le présent document serait appropriée.
Il est essentiel de comprendre le fonctionnement des eaux de surface, des eaux souterraines et des
gaz du sol pour évaluer les risques potentiels pour la santé et la sécurité humaines ainsi que pour
d’autres récepteurs potentiels tels que, par exemple, les ressources en eaux souterraines. Cependant, la
fourniture de recommandations détaillées concernant l’investigation des eaux souterraines, des eaux
de surface et des gaz du sol ne relève pas du domaine d’application du présent document. Pour de plus
amples informations sur l’échantillonnage des eaux souterraines et des eaux de surface, voir l’ISO 5667.
Des recommandations sur l’échantillonnage des gaz du sol sont fournies dans l’ISO 18400-204.
vi © ISO 2018 – Tous droits réservés
NOTE 1 Les chiffres encerclés de cette figure définissent les éléments clés (1 à 7) du programme d’investigation.
NOTE 2 Cette figure présente un processus générique qui peut être modifié si nécessaire.
Figure 1 — Liens entre les éléments essentiels d’un programme d’investigation
NORME INTERNATIONALE ISO 18400-203:2018(F)
Qualité du sol — Échantillonnage —
Partie 203:
Investigation des sites potentiellement contaminés
1 Domaine d’application
Le présent document fournit des recommandations concernant:
— l’investigation de sites au niveau desquels la présence d’une contamination du sol est connue ou
suspectée;
— l’investigation de sites au niveau desquels aucune contamination du sol n’est attendue, mais dont
la qualité du sol doit être déterminée (par exemple pour s’assurer qu’aucune contamination n’est
présente);
— l’investigation en prévision de la nécessité de gérer la réutilisation ou l’extraction de terre excavée
susceptible d’être contaminée;
— la collecte des informations nécessaires à l’appréciation du risque et/ou à l’élaboration de plans
d’assainissement (par exemple, pour déterminer si une remédiation est nécessaire et proposer le
meilleur moyen d’y parvenir).
Bien que les informations sur la qualité du sol en vue de l’appréciation du risque et/ou de l’élaboration
de plans d’assainissement soient collectées en appliquant le présent document, il ne fournit pas de
recommandations concernant les décisions et les actions qui suivent l’investigation d’un site, par
exemple l’appréciation du risque et les décisions concernant les exigences de remédiation (le cas
échéant).
2 Références normatives
Les documents suivants cités dans le texte constituent, pour tout ou partie de leur contenu, des
exigences du présent document. Pour les références datées, seule l’édition citée s’applique. Pour les
références non datées, la dernière édition du document de référence s’applique (y compris les éventuels
amendements).
ISO 11074, Qualité du sol — Vocabulaire
ISO 18400-104, Qualité du sol — Échantillonnage — Partie 104: Stratégies
3 Termes et définitions
Pour les besoins du présent document, les termes et définitions donnés dans l’ISO 11074 et
l’ISO 18400-104 s’appliquent.
NOTE Lorsque les définitions de ces deux normes diffèrent, celles de l’ISO 18400-104 prévalent.
L’ISO et l’IEC tiennent à jour des bases de données terminologiques destinées à être utilisées en
normalisation, consultables aux adresses suivantes:
— ISO Online browsing platform: disponible à l’adresse http: //www .iso .org/obp;
— IEC Electropedia: disponible à l’adresse http: //www .electropedia .org/.
4 Objectifs
4.1 Généralités
Le présent document fournit un cadre pour les différentes phases et étapes de l’investigation de sites
potentiellement contaminés. La détermination de l’état de contamination qui en résulte peut ensuite
conduire à une appréciation du risque et, si nécessaire, faciliter la sélection et la mise en œuvre des
mesures de remédiation appropriées. Des recommandations sur les données et informations exigées
à des fins particulières sont données dans de nombreuses Normes internationales, notamment
l’ISO 11504, l’ISO 15175, l’ISO 15176, l’ISO 15799 et l’ISO 15800.
Des investigations en matière de contamination peuvent être exigées:
— lorsque le but est d’identifier et de traiter une contamination (par exemple sur un site connu ou
suspecté de présenter des risques inacceptables pour l’homme ou d’autres récepteurs – parfois
appelés sites «problématiques»);
— en raison de plans de réaménagement de sites (par exemple d’un site industriel en logements); ou
— en particulier dans les zones urbaines, car il est connu que des sols potentiellement contaminés
doivent être excavés et éliminés du site (par exemple pour réaliser des fondations, installer des
réseaux ou construire des infrastructures souterraines).
Il convient d’adapter les recommandations données dans le présent document en fonction de ces
situations, ainsi que lorsque la contamination potentielle pose problème.
NOTE 1 Bien que la contamination soit définie dans l’ISO 11074 comme le résultat de l’activité humaine, les
méthodes d’investigation décrites sont également applicables en présence de concentrations naturellement
élevées de substances potentiellement dangereuses.
NOTE 2 En ce qui concerne la remédiation, le présent document ne fournit que des recommandations
concernant les informations exigées en général. Des méthodes de remédiation spécifiques peuvent nécessiter des
informations supplémentaires.
NOTE 3 Le présent document traite uniquement de l’investigation du sol. D’anciens sites urbains et industriels
peuvent contenir des bâtiments et/ou des installations industrielles abandonnés en attente de démolition, de
démantèlement ou de remise en état. L’absence d’investigation de ces bâtiments avant leur démolition peut
menacer la sécurité des travailleurs ou conduire à une dispersion de la contamination sur et autour du site.
L’investigation des bâtiments dégradés ou des vestiges de fondations n’entre pas dans le domaine d’application
du présent document.
NOTE 4 Dans de nombreuses situations, il existe une relation étroite entre la contamination du sol, des eaux
souterraines, des gaz du sol et, dans une moindre mesure, des eaux de surface. Par conséquent, il est essentiel
de comprendre le fonctionnement des eaux de surface, des eaux souterraines et des gaz du sol pour évaluer
les risques potentiels pour la santé et la sécurité humaines ainsi que pour d’autres récepteurs potentiels tels
que, par exemple, les ressources en eaux souterraines. Cependant, la fourniture de recommandations détaillées
concernant l’investigation des eaux souterraines, des eaux de surface et des gaz du sol ne relève pas du domaine
d’application du présent document. Pour de plus amples informations sur l’échantillonnage des eaux souterraines
et des eaux de surface, voir l’ISO 5667. Des recommandations sur l’échantillonnage des gaz du sol sont fournies
dans l’ISO 18400-204.
4.2 Définitions des objectifs
Bien que les raisons d’une investigation et, par conséquent, les objectifs, puissent considérablement
varier, ils visent généralement à:
— identifier et évaluer les risques pour les personnes utilisant le site et, en cas de réaménagement,
pour les futurs utilisateurs et occupants du site;
— identifier et évaluer les risques pour l’environnement, y compris les terrains adjacents, les eaux de
surface, les eaux souterraines, les écosystèmes et la santé publique;
2 © ISO 2018 – Tous droits réservés
— identifier et évaluer les risques potentiels pour les travailleurs impliqués dans les investigations, la
remédiation, le réaménagement ou l’entretien du site;
— permettre une gestion appropriée des matériaux excavés, notamment sur les sites urbains;
— identifier et évaluer la possibilité d’effets préjudiciables sur les matériaux de construction;
de manière à pouvoir déterminer l’importance des risques et décider s’il est nécessaire de prendre toute
forme de mesure pour les traiter.
À partir des principaux objectifs de l’investigation, il est possible de déduire de nombreux objectifs
secondaires. qui peuvent notamment comprendre de:
a) déterminer si une action immédiate est exigée pour protéger les récepteurs exposés;
b) identifier des composés qui sont, ou peuvent être, présents et qui sont susceptibles de représenter
un risque pour un ou plusieurs récepteurs réels ou potentiels;
c) identifier les récepteurs (par exemple humains, écosystèmes, eaux souterraines) qui sont en danger
ou peuvent l’être dans le futur;
d) identifier les voies par lesquelles des récepteurs particuliers peuvent être exposés aux
contaminants;
e) fournir des données et d’autres informations à utiliser lors de l’appréciation du risque;
f) fournir des informations aidant à concevoir des mesures de protection ou de remédiation;
g) fournir des informations facilitant la gestion des terres excavées et autres matériaux;
h) permettre la caractérisation du sol contaminé et d’autres matériaux pour assurer leur manipulation
et leur élimination de façon sûre et appropriée;
i) fournir des données de référence permettant d’évaluer les résultats de la remédiation entreprise;
j) permettre d’évaluer l’impact probable de la poursuite de l’utilisation du site sur l’environnement, y
compris la qualité du sol;
k) fournir des informations permettant d’évaluer le risque de la responsabilité environnementale
(légale) et l’effet sur la valeur du bien.
Ces objectifs généralisés seront formulés en exigences spécifiques selon l’objectif de l’investigation.
EXEMPLE L’investigation d’un site avant l’achat du site en vue de son réaménagement peut avoir un ou
plusieurs des objectifs suivants:
— établir l’historique du site et l’éventuelle présence d’une contamination;
— établir la nature, l’étendue et la répartition de la contamination dans les limites du site;
— identifier la possibilité de migration de la contamination au-delà des limites du site, y compris dans les eaux
de surface et les eaux souterraines (ce qui pourrait indiquer qu’il existe des passifs environnementaux légaux
potentiels);
— identifier tout danger immédiat pour la santé publique, la sécurité et l’environnement;
— identifier les contraintes liées à la contamination en rapport avec l’aménagement proposé (par exemple
risques pour l’homme et l’environnement) et tous les travaux de remédiation nécessaires, et fournir des
données permettant d’estimer les coûts;
— fournir des informations facilitant la formulation d’un rapport d’interprétation complet avec des conclusions,
des recommandations et un chiffrage budgétaire des mesures de remédiation, si nécessaire;
— fournir des informations permettant de conseiller le commanditaire sur la manière de traiter les problèmes
soulevés par toute migration de la contamination hors du site.
5 Stratégie générale d’investigation d’un site
5.1 Généralités
La détermination de l’étendue d’une zone contaminée, et notamment l’appréciation des risques pour
l’homme et l’environnement dus à la contamination, peuvent être complexes. En raison de cette
complexité, il convient que le processus d’identification, de quantification et d’évaluation des risques
associés à un terrain contaminé soit un processus itératif comportant plusieurs étapes d’investigation
(chacune devant atteindre des objectifs spécifiques), afin d’obtenir suffisamment de données
pertinentes pour caractériser les risques potentiels, les voies d’exposition et les récepteurs étudiés. Il
convient de réexaminer les objectifs à chaque étape et revoir les exigences relatives à une investigation
plus approfondie au fur et à mesure de l’évolution des processus d’investigation et d’évaluation.
NOTE 1 Des recommandations générales concernant l’élaboration des stratégies d’investigation de site et des
stratégies d’échantillonnage sont données dans l’ISO 18400-104. Des recommandations sur la préparation du
plan d’échantillonnage sont fournies dans l’ISO 18400-101.
Les phases principales sont:
— investigation préliminaire (voir 5.2 et Article 6);
— investigation exploratoire (voir 5.3, Articles 7 et 8); et
— investigation détaillée (approfondie) du site (voir 5.4, Articles 7 et 9).
La relation entre ces phases est illustrée à la Figure 2.
Des investigations complémentaires peuvent être exigées après l’investigation détaillée du site afin
d’obtenir des informations pertinentes pour la sélection des méthodes de remédiation ou la conception
des travaux de remédiation ou de construction.
À l’issue des travaux réalisés sur le site pendant toute la phase ou l’étape d’investigation, il convient de
rédiger un rapport d’échantillonnage conformément à l’ISO 18400-107.
Après toute phase ou étape d’investigation, il y a lieu d’établir un rapport indiquant les résultats obtenus
(voir 8.4 et 9.6).
4 © ISO 2018 – Tous droits réservés
Figure 2 — Processus d’investigation d’un site
Avant de s’engager dans une phase ou étape d’investigation, il est important d’établir des objectifs de
qualité des données en termes de type, de quantité et de qualité (par exemple qualité analytique) des
données et autres informations à collecter. Ces objectifs de qualité des données dépendront en partie
de la nature des décisions à prendre sur la base de l’investigation, ainsi que de la confiance nécessaire
dans ces décisions. La stratégie d’investigation (qu’elle soit préliminaire, exploratoire ou détaillée) sera
déterminée par les objectifs. Par exemple, les différentes exigences d’investigations de site en vue d’une
vente, de la confirmation d’une contamination suspectée ou d’un réaménagement, auront une incidence
sur l’espacement des points d’échantillonnage et le nombre d’échantillons analysés, et donc sur le coût
de l’investigation.
L’absence d’objectifs initiaux en termes de qualité des données peut entraîner des pertes économiques
considérables lorsque, par exemple, les données collectées ne sont pas adaptées ou suffisantes pour une
appréciation fiable des risques, ou lorsqu’elles laissent subsister de trop nombreuses incertitudes sur
le «schéma conceptuel du site» élaboré pour le site (voir 6.2 pour la description du schéma conceptuel
du site).
Pour décider de la stratégie, il convient de prendre en compte l’applicabilité et l’utilisation des
techniques d’analyse et/ou de mesure sur site.
NOTE 2 Des recommandations pour la sélection et l’application de méthodes sur site sont données dans
l’ISO 12404.
5.2 Périmètre de l’investigation préliminaire
L’investigation préliminaire comprend une étude sur documents et une reconnaissance du site (levé
de surface, inspection du site). Elle est réalisée à l’aide d’historiques et d’autres sources permettant
d’obtenir des informations sur l’usage passé et présent du site ainsi que des informations sur les
propriétés locales du sol, la géologie, la géomorphologie, la pédologie, l’hydrologie de surface,
l’hydrogéologie et les paramètres environnementaux. Il convient qu’elle soit réalisée conformément à
l’ISO 18400-202 et aux recommandations de l’Article 6.
À partir de cette investigation préliminaire, la possibilité d’une contamination peut être déduite et des
hypothèses formulées à propos de la nature, la localisation et la répartition de la contamination, telles
que celles énumérées à l’Annexe A.
Ces hypothèses font partie intégrante du schéma conceptuel du site qu’il convient de développer, en
englobant non seulement les aspects de la contamination, mais aussi la géologie, la géomorphologie, la
pédologie, l’hydrogéologie, l’hydrologie de surface, les caractéristiques géotechniques et les paramètres
environnementaux. Les utilisations actuelles et planifiées du site représentent également des aspects
importants du schéma conceptuel du site.
NOTE Des recommandations concernant l’élaboration de schémas conceptuels de site sont données dans
l’ISO 18400-202.
Il convient que l’investigation préliminaire fournisse suffisamment d’informations:
— pour tirer des conclusions initiales sur les risques potentiels pour l’homme et les autres récepteurs,
réels ou potentiels;
— pour déterminer si une action supplémentaire est nécessaire (par exemple une investigation
intrusive).
La quantité et le type d’informations exigées dépendront des objectifs de l’investigation. La quantité
de travail exigée variera en fonction de l’âge du site, de la complexité de son usage antérieur et de la
complexité de la géologie sous-jacente, etc.
Il convient de garder à l’esprit que la contamination d’un site peut être plus complexe qu’initialement
indiqué (par exemple par l’usage actuel) et de toujours obtenir des informations appropriées sur
l’historique du site lors de l’investigation préliminaire.
5.3 Périmètre de l’investigation exploratoire
L’investigation exploratoire implique une investigation sur site limitée, y compris le prélèvement
d’échantillons de sol ou de remblai, d’eaux de surface, d’eaux souterraines et de gaz du sol, le cas
échéant, et l’analyse ou des essais ultérieurs des échantillons prélevés. Les données et les informations
obtenues sont ensuite évaluées afin de déterminer si les hypothèses de l’investigation préliminaire sont
correctes et, le cas échéant, évaluer d’autres aspects du schéma conceptuel du site. Une investigation
exploratoire peut identifier des zones de contamination (processus essentiellement qualitatif), mais ne
6 © ISO 2018 – Tous droits réservés
suffit pas à déterminer son étendue ou la variation de la contamination dans ces zones (c’est-à-dire la
quantification de la contamination) qui relève de l’investigation détaillée du site.
Dans certains cas, lorsque les informations exigées d’après les objectifs définis et obtenues à l’issue
de l’investigation exploratoire sont suffisantes, aucune investigation supplémentaire n’est nécessaire.
Toutefois, l’investigation exploratoire du site peut mettre en évidence, par exemple, que le schéma de
contamination est plus complexe, ou que les concentrations de contaminants sont plus élevées que
prévu, et représentent déjà, ou peuvent représenter dans le futur, un (des) danger(s) et donc un risque
pour un ou plusieurs récepteurs potentiels. Dans cette situation, les informations obtenues peuvent
s’avérer insuffisantes pour prendre des décisions avec un niveau de confiance satisfaisant et il sera
nécessaire:
— soit de réaliser une étape supplémentaire d’investigation exploratoire avant de passer à la conception
et à l’exécution d’une investigation détaillée;
— soit de procéder à une investigation détaillée du site afin d’obtenir suffisamment d’informations
pour pouvoir réaliser une appréciation du risque complète, déterminer la nécessité de mesures de
protection ou de remédiation, en temps utile et éventuellement après des étapes supplémentaires
d’investigation, sélectionner, concevoir et mettre en œuvre des mesures de protection ou de
remédiation.
5.4 Périmètre de l’investigation détaillée du site
L’investigation détaillée du site fournit les informations de base permettant de déterminer la quantité
et la répartition spatiale des contaminants, leurs fractions mobile et mobilisable et les possibilités
de dispersion dans l’environnement. Elle inclut une future évolution possible de l’ampleur de la
contamination.
Selon les objectifs, elle peut nécessiter le prélèvement et l’analyse d’échantillons de sol ou de remblai,
d’eaux de surface, d’eaux souterraines et de gaz du sol afin d’obtenir les informations nécessaires à une
évaluation complète des risques dus à la contamination pour l’homme et d’autres récepteurs potentiels,
et de pouvoir également déterminer des mesures appropriées de confinement ou de remédiation avec,
si nécessaire, une estimation initiale des coûts. L’investigation intrusive peut être étayée par des calculs
de modélisation et des techniques d’investigation ne nécessitant pas le prélèvement d’échantillons,
telles que celles décrites dans l’Annexe B. La conception détaillée des travaux de protection ou de
remédiation peut nécessiter d’autres étapes d’investigation complémentaires.
NOTE Il peut être approprié d’étudier l’air ambiant, la végétation, les sources d’eau potable et divers autres
milieux, en fonction des résultats de l’investigation préliminaire.
La quantité et la nature des informations devant être obtenues à l’issue de l’investigation détaillée du
site (ou de toute étape particulière de celui-ci) varieront en fonction de la nature du site et des objectifs
de l’investigation. Les conséquences des décisions relatives aux mesures qu’il convient de mettre en
œuvre sur un site varieront d’un site à l’autre. De plus, la quantité et la qualité des informations exigées
varieront également en fonction des exigences des processus décisionnels (par exemple l’appréciation
du risque, les décisions concernant la nécessité et le type de mesures de remédiation). Il convient
que toutes les parties impliquées dans le processus décisionnel soient tenues informées dès qu’une
information est disponible afin de s’assurer que l’information est suffisante pour l’usage prévu.
Au terme de l’interprétation des informations générées, y compris toute appréciation du risque, il
convient de pouvoir déterminer si des mesures de protection ou de remédiation sont nécessaires, et de
généraliser le type de mesures susceptibles d’être appropriées.
6 Investigation préliminaire
6.1 Généralités
Il convient de réaliser une investigation préliminaire conformément à l’ISO 18400-202 avant toute
investigation intrusive ou autre investigation de terrain.
Il y a lieu d’utiliser les résultats de l’investigation préliminaire pour préparer un schéma conceptuel
initial du site, y compris la formulation d’hypothèses relatives à la contamination, tel que décrit au 6.2.2
et à l’Annexe A.
6.2 Élaboration du schéma conceptuel du site
6.2.1 Schéma conceptuel global du site
Le schéma conceptuel du site est une représentation et/ou une description du site incorporant tous
les éléments connus et attendus concernant le site (par exemple contamination, géologie, pédologie,
paramètres environnementaux). Il convient d’identifier les voies par lesquelles les récepteurs actuels
et futurs pourraient être affectés par la contamination, dans le présent ou dans le futur. Un aspect
important du schéma conceptuel du site est la formulation d’hypothèses relatives à la contamination.
Il faut noter que sa préparation nécessaire une certaine interprétation des informations disponibles et
une reconnaissance explicite des incertitudes sur ces informations.
L’élaboration d’un schéma conceptuel du site peut largement contribuer à comprendre le site et les
risques qu’il peut présenter pour l’homme et d’autres récepteurs, et à concevoir les futures étapes
d’investigation. Il aide également à déterminer comment procéder à la remédiation (si elle est
nécessaire) et réaliser d’autres travaux.
Le schéma conceptuel du site facilite également la communication entre les différentes parties
concernées et avec le public.
6.2.2 Formulation d’hypothèses liées à la contamination
Sur la base des résultats de l’investigation préliminaire, il convient de formuler des hypothèses relatives
à la nature probable, à la variation et à la répartition spatiale des substances contaminantes prévues
sur le site (voir l’Annexe A). Pour parvenir à des hypothèses pertinentes, il sera souvent nécessaire
d’identifier différentes zones d’un site pour lesquelles différentes hypothèses sont applicables. Si cette
condition est généralement essentielle pour un site aux dimensions importantes, elle est également
souvent applicable à des sites de petites dimensions.
Avant de décider de la stratégie d’échantillonnage à adopter, il est primordial de déterminer pour chaque
zone (et pour le site dans son ensemble), à partir des informations disponibles, s’il est raisonnable de
s’attendre - ou non - à une contamination de la zone ou du site, autrement dit s’il convient de classer la
zone (ou le site) comme étant «probablement non contaminé(e)» ou «probablement contaminé(e)».
Il convient de formuler les hypothèses relatives à chaque substance de manière à pouvoir les intégrer
dans un schéma conceptuel du site, en tenant compte de toutes les informations disponibles et en
traduisant ces informations en un scénario le plus probable en ce qui concerne l’état de contamination
d’une zone. Les schémas conceptuels relatifs aux zones individuelles du site peuvent être combinés en
un schéma conceptuel global du site. Ce schéma conceptuel portant sur l’ensemble du site est utilisé pour
concevoir la stratégie d’échantillonnage à appliquer dans la prochaine phase ou étape d’investigation.
6.3 Rapport sur l’investigation préliminaire et le schéma conceptuel du site
Il convient de rédiger un rapport sur l’investigation préliminaire de manière à considérer la formulation
initiale du schéma conceptuel du site et les hypothèses spécifiques comme une partie du rapport
clairement reconnaissable et identifiable, tel que décrit dans l’ISO 18400-202:2018, Article 9.
7 Conception des investigations intrusives
7.1 Vue d’ensemble
Le présent article, qu’il convient d’appliquer conjointement avec l’ISO 18400-104, fournit des
recommandations applicables à la conception de tous les types d’investigations intrusives de
8 © ISO 2018 – Tous droits réservés
sites potentielleme
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