Bitumens and bituminous binders - Determination of complex shear modulus and phase angle - Dynamic Shear Rheometer (DSR)

This document specifies a general method of using a dynamic shear rheometer (DSR) for measuring the rheological properties of bituminous binders. The procedure involves determining the complex shear modulus and phase angle of binders over a range of test frequencies and test temperatures when tested in oscillatory shear.
From the test, the complex shear modulus, |G*|, and its phase angle, δ, at a given temperature and frequency are calculated, as well as the components G' and G" of the complex shear modulus.
This method is applicable to un-aged, aged, stabilized and recovered bituminous binders. The test procedure in accordance with this document is not applicable for bituminous binders with particles larger than 250 μm (e.g. filler material, granulated rubber).
WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des komplexen Schermoduls und des Phasenwinkels - Dynamisches Scherrheometer (DSR)

Die allgemeine Warnung muss durch Folgendes ersetzt werden:
„WARNUNG — Die Anwendung dieses Dokuments kann den Einsatz gefährlicher Stoffe, Arbeitsgänge und Geräte bedingen. Dieses Dokument erhebt nicht den Anspruch, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme anzusprechen. Es liegt in der Verantwortung des Anwenders dieses Dokuments, geeignete Sicherheits-, Gesundheits- und Arbeitsschutzmaßnahmen umzusetzen und im Vorfeld die Anwendbarkeit der gesetzlichen Beschränkungen zu bestimmen. Die Anwendung dieses Dokuments schließt den Umgang mit Geräten und Bindemitteln bei sehr hohen Temperaturen ein.“.

Bitumes et liants bitumineux - Détermination du module complexe en cisaillement et de l'angle de phase à l'aide d'un rhéomètre à cisaillement dynamique (DSR)

Remplacer le texte général d’avertissement par :
« AVERTISSEMENT — L'utilisation de ce document peut impliquer l'utilisation de produits, d'opérations et d'équipements à caractère dangereux. Le présent document n'a pas vocation à aborder tous les problèmes de sécurité concernés par son usage. Il incombe à son utilisateur d'établir des règles d'hygiène et de sécurité appropriées, de définir les équipements de protection des intervenants et de déterminer l'applicabilité des restrictions réglementaires avant utilisation. L'utilisation de ce document implique la manipulation d'appareillages et d'échantillons de liants à très haute température. ».

Bitumen in bitumenska veziva - Določanje kompleksnega strižnega modula in faznega kota - Dinamični strižni reometer (DSR)

Ta dokument določa splošno metodo uporabe dinamičnega strižnega reometra (DSR) za merjenje reoloških lastnosti bitumenskih veziv. Postopek vključuje določanje kompleksnega strižnega modula in faznega kota veziv v razponu preskusnih frekvenc in preskusnih temperatur pri testiranju v oscilacijskem strigu.
Iz preskusa se izračunata kompleksni strižni modul, |G*|, in njegov fazni kot, δ, pri dani temperaturi in frekvenci, kot tudi komponenti G' in G" kompleksnega strižnega modula.
Ta metoda je uporabna za nepostarana, postarana, stabilizirana in regenerirana bitumenska veziva. Preskusni postopek v skladu s tem dokumentom ni primeren za bitumenska veziva z delci, večjimi od 250 μm (npr. polnilni material, granulirana guma).
OPOZORILO - Uporaba tega dokumenta lahko vključuje nevarne materiale, postopke in opremo. Ta dokument ne obravnava vseh varnostnih težav, povezanih z njegovo uporabo. Odgovornost uporabnika tega dokumenta je, da vzpostavi ustrezne varnostne in zdravstvene prakse ter določi uporabnost regulativnih omejitev pred uporabo.

General Information

Status
Not Published
Public Enquiry End Date
25-Jun-2026
Technical Committee
VLA - Water proofing
Current Stage
4020 - Public enquire (PE) (Adopted Project)
Start Date
06-May-2026
Due Date
23-Sep-2026

Relations

Effective Date
17-Sep-2025

Overview

SIST EN 14770:2023/oprA1:2026, Bitumens and bituminous binders - Determination of complex shear modulus and phase angle - Dynamic Shear Rheometer (DSR), is a draft European amendment developed by CEN/TC 336. This standard specifies a general method for measuring the rheological properties of bituminous binders using a Dynamic Shear Rheometer (DSR). The procedure involves determining the complex shear modulus (|G|)* and phase angle (δ) of bituminous binders across various test frequencies and temperatures using oscillatory shear. Additionally, the standard outlines the calculation of the components of the complex shear modulus, namely G' (storage modulus) and G" (loss modulus).

The method is suitable for a wide variety of binders, including un-aged, aged, stabilized, and recovered bituminous binders, provided that the sample does not contain particles larger than 250 μm, such as filler material or granulated rubber.

Key Topics

  • Dynamic Shear Rheometer (DSR): The standard defines the detailed use of DSR apparatus for precise rheological analysis of bituminous binders.
  • Complex Shear Modulus and Phase Angle: Guidelines for measuring |G*| and δ, which represent the viscoelastic behavior of the binder, are elaborated for comprehensive material characterization.
  • Sample Preparation: Step-by-step instructions are provided for homogenizing, molding, and storing specimens to ensure reliable and repeatable test results, including storage conditions and minimum/maximum recommended storage times.
  • Applicability and Limitations: The methodology does not apply to binders with large particles (over 250 μm), ensuring the test's reliability for bounded homogeneous samples.
  • Safety Considerations: The standard emphasizes safe handling practices due to the potential hazards associated with high-temperature operations and the handling of hot bituminous binders.
  • Quality Assurance: Recommendations are included for preparing extra test specimens and for steps to avoid contamination and ensure the integrity of results.

Applications

The EN 14770 standard is essential for:

  • Asphalt and Pavement Design: Determining the viscoelastic properties of binders informs the performance grading of asphalt and contributes to more durable road surfaces.
  • Binder Specification and Quality Control: Manufacturers and laboratories use the DSR method to verify that bituminous binders meet regulatory or customer requirements.
  • R&D and Material Development: Researchers rely on this standard when developing new polymer-modified bitumen or evaluating the effects of ageing, additives, and recycling processes.
  • Forensics and Failure Analysis: Identifying the root causes of pavement distress by measuring changes in binder rheology due to traffic, environment, or production issues.
  • Compliance with European Standards: Industry professionals and compliance officers use this test to ensure their materials align with harmonized CEN standards for construction and infrastructure projects.

Related Standards

For comprehensive binder analysis and quality assurance, consider referencing these related standards:

  • EN 12594: Bitumen and bituminous binders - Preparation of test samples
  • EN 13302: Bitumen and bituminous binders - Determination of dynamic viscosity
  • EN 1426 / EN 1427: Determination of needle penetration and softening point for bituminous binders
  • ASTM D7175: Standard test method for determining the rheological properties of asphalt binder using a DSR
  • EN 14771: Bituminous binders - Determination of flexural creep stiffness (Bending Beam Rheometer Method)

By aligning with SIST EN 14770:2023/oprA1:2026, laboratories and manufacturers can ensure high-quality, consistent binder characterization essential for robust and long-lasting pavements and infrastructure.

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Frequently Asked Questions

SIST EN 14770:2023/oprA1:2026 is a draft published by the Slovenian Institute for Standardization (SIST). Its full title is "Bitumens and bituminous binders - Determination of complex shear modulus and phase angle - Dynamic Shear Rheometer (DSR)". This standard covers: This document specifies a general method of using a dynamic shear rheometer (DSR) for measuring the rheological properties of bituminous binders. The procedure involves determining the complex shear modulus and phase angle of binders over a range of test frequencies and test temperatures when tested in oscillatory shear. From the test, the complex shear modulus, |G*|, and its phase angle, δ, at a given temperature and frequency are calculated, as well as the components G' and G" of the complex shear modulus. This method is applicable to un-aged, aged, stabilized and recovered bituminous binders. The test procedure in accordance with this document is not applicable for bituminous binders with particles larger than 250 μm (e.g. filler material, granulated rubber). WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

This document specifies a general method of using a dynamic shear rheometer (DSR) for measuring the rheological properties of bituminous binders. The procedure involves determining the complex shear modulus and phase angle of binders over a range of test frequencies and test temperatures when tested in oscillatory shear. From the test, the complex shear modulus, |G*|, and its phase angle, δ, at a given temperature and frequency are calculated, as well as the components G' and G" of the complex shear modulus. This method is applicable to un-aged, aged, stabilized and recovered bituminous binders. The test procedure in accordance with this document is not applicable for bituminous binders with particles larger than 250 μm (e.g. filler material, granulated rubber). WARNING - The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

SIST EN 14770:2023/oprA1:2026 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.

SIST EN 14770:2023/oprA1:2026 has the following relationships with other standards: It is inter standard links to SIST EN 14770:2023. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

SIST EN 14770:2023/oprA1:2026 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


SLOVENSKI STANDARD
01-junij-2026
Bitumen in bitumenska veziva - Določanje kompleksnega strižnega modula in
faznega kota - Dinamični strižni reometer (DSR)
Bitumens and bituminous binders - Determination of complex shear modulus and phase
angle - Dynamic Shear Rheometer (DSR)
Bitumen und bitumenhaltige Bindemittel - Bestimmung des komplexen Schermoduls und
des Phasenwinkels - Dynamisches Scherrheometer (DSR)
Bitumes et liants bitumineux - Détermination du module complexe en cisaillement et de
l'angle de phase à l'aide d'un rhéomètre à cisaillement dynamique (DSR)
Ta slovenski standard je istoveten z: EN 14770:2023/prA1
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

DRAFT
EUROPEAN STANDARD
EN 14770:2023
NORME EUROPÉENNE
EUROPÄISCHE NORM
prA1
April 2026
ICS 75.140; 91.100.50
English Version
Bitumens and bituminous binders - Determination of
complex shear modulus and phase angle - Dynamic Shear
Rheometer (DSR)
Bitumes et liants bitumineux - Détermination du Bitumen und bitumenhaltige Bindemittel -
module complexe en cisaillement et de l'angle de phase Bestimmung des komplexen Schermoduls und des
à l'aide d'un rhéomètre à cisaillement dynamique Phasenwinkels - Dynamisches Scherrheometer (DSR)
(DSR)
This draft amendment is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee CEN/TC 336.

This draft amendment A1, if approved, will modify the European Standard EN 14770:2023. If this draft becomes an amendment,
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for inclusion of
this amendment into the relevant national standard without any alteration.

This draft amendment was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.

EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2026 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 14770:2023/prA1:2026 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
1 Modification to the English title of the standard . 4
2 Modification to Clause 1, Scope . 4
3 Modification to Clause 4, Principle . 4
4 Modification to Clause 5, Apparatus . 4
5 Modification to 5.1, Dynamic shear rheometer (DSR) . 4
6 Modification to 5.2, Moulds or sheet materials . 5
7 Modification to 6.3, Set up . 5
8 Modification to 7.1, General . 5
9 Modification to 7.3, Specimen manufacturing and storage conditions . 5
10 Modification to 8.2, Specimen placing into the rheometer . 6

European foreword
This document (EN 14770:2023/prA1:2026) has been prepared by Technical Committee CEN/TC 336
“Bitumens and bituminous binders”, the secretariat of which is held by AFNOR.
This document is currently submitted to the CEN Enquiry.
This document will amend EN 14770:2023.

1 Modification to the English title of the standard
Replace the word "Bitumen" with "Bitumens".
2 Modification to Clause 1, Scope
Replace the general warning with the following:
"WARNING — The use of this document can involve hazardous materials, operations and equipment.
This document does not purport to address all of the safety problems associated wi
...