ISO 22863-11:2022

INTERNATIONAL ISO
STANDARD 22863-11
First edition
2022-07
Fireworks — Test methods for
determination of specific chemical
substances —
Part 11:
Phosphorus content by inductively
coupled plasma optical emission
spectrometry (ICP-OES)
Partie 11: Titre manque
Reference number
© ISO 2022
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Published in Switzerland
ii
Contents Page
Foreword .iv
1 S c op e . 1
2 Nor m at i ve r ef er enc e s . 1
3 T erms and definitions . 1
4 P rinciple . 1
5 R e a g ent s . 1
6 A pp a r at u s . 2
7 P rep a r at ion s . 3
8 P r o c e du re .3
8 .1 S a mple s i z e . 3
8.2 N itrification process . 3
8. 3 Bl ank t e st . 3
8 .4 C a l ibr at ion c u r ve . 3
8 . 5 S a mple de t er m i n at ion. 3
8 . 6 P a r a l lel t e s t . 4
9 Re sults calculation. 4
10 P r e c i s ion . 4
11 Detection limit . 4
12 Te s t r ep or t . 4
Bibliography . 6
iii
Foreword
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electrotechnical standardization.
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This document was prepared by Technical Committee ISO/TC 264, Fireworks.
A list of all the parts in the ISO 22863 series can be found on the ISO website.
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iv
INTERNATIONAL STANDARD ISO 22863-11:2022(E)
Fireworks — Test methods for determination of specific
chemical substances —
Part 11:
Phosphorus content by inductively coupled plasma optical
emission spectrometry (ICP-OES)
1 S cope
This document specifies the test method for the determination of phosphorus content in firework
compositions by inductively coupled plasma optical emission spectrometry (ICP-AES).
Such test is applied to fireworks excluding Christmas crackers, party poppers, or snaps according to
ISO 25947-5. The use of white phosphorus can lead to fireworks of hazardous chemical stability that can
be detected by possible self-ignition during the thermal conditioning test according to ISO 25947-4:2017,
6.16 (75,0 ± 2,5 °C for 48 h).
2 Normat ive references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 22863-1:2020, Fireworks — Test methods for determination of specific chemical substances — Part 1:
General
3 T erms and definitions
No terms and defini
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