Water quality - Gross beta activity in non-saline water - Test method using thick source (ISO 9697:2015)

ISO 9697:2015 specifies a test method for the determination of gross beta activity concentration in non-saline waters. The method covers non-volatile radionuclides with maximum beta energies of approximately 0,3 MeV or higher. Measurement of low energy beta emitters (e.g. 3H, 228Ra, 210Pb, 14C, 35S, and 241Pu) and some gaseous or volatile radionuclides (e.g. radon and radioiodine) might not be included in the gross beta quantification using the test method described in ISO 9697:2015.
This test method is applicable to the analysis of raw and drinking waters. The range of application depends on the amount of total soluble salts in the water and on the performance characteristics (background count rate and counting efficiency) of the counter used. It is the laboratory's responsibility to ensure the suitability of this method for the water samples tested.

Wasserbeschaffenheit - Bestimmung der Gesamt-Beta-Aktivität in nicht-salzhaltigem Wasser - Dickschichtverfahren (ISO 9697:2015)

Qualité de l'eau - Activité bêta globale des eaux non salines - Méthode d'essai par source concentrée (ISO 9697:2015)

L'ISO 9697:2015 spécifie une méthode d'essai permettant de déterminer l'activité volumique bêta globale des eaux non salines. La méthode couvre les radionucléides non volatils émetteurs bêta avec des énergies maximales d'environ 0,3 MeV ou plus élevées. Les mesurages des émetteurs bêta à faible énergie (par exemple, 3H, 228Ra, 210Pb, 14C, 35S et 241Pu) et de certains radionucléides gazeux ou volatils (par exemple, radon et iode radioactif) peuvent ne pas être inclus dans la quantification bêta globale en utilisant la méthode d'essai décrite dans l'ISO 9697:2015.
Cette méthode d'essai est applicable à l'analyse des eaux brutes et potables. La gamme d'application dépend de la quantité de sels solubles totaux dans l'eau et des caractéristiques de performance (taux de comptage du bruit de fond et efficacité de comptage) du compteur utilisé. Il incombe au laboratoire de s'assurer de l'adéquation de cette méthode pour les échantillons d'eau soumis à essai.

Kakovost vode - Skupna beta aktivnost v neslanih vodah - Preskusna metoda robustnega vira (ISO 9697:2015)

Ta mednarodni standard opisuje metodo za določevanje skupne beta aktivnosti v neslanih vodah. Metoda zajema nehlapne beta oddajne radionuklide z maks. beta energijo > 0,3 MeV. Ta standard ne vključuje merjenja beta oddajnikov z zelo nizko energijo, npr.3H, 14C, 35S in 241Pu. Ta metoda se uporablja za analizo neobdelane in pitne vode.

General Information

Status
Withdrawn
Publication Date
13-Jun-2017
Withdrawal Date
18-Jun-2019
Technical Committee
Drafting Committee
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
19-Jun-2019

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SLOVENSKI STANDARD
01-december-2017
Kakovost vode - Skupna beta aktivnost v neslanih vodah - Preskusna metoda
robustnega vira (ISO 9697:2015)
Water quality - Gross beta activity in non-saline water - Test method using thick source
(ISO 9697:2015)
Wasserbeschaffenheit - Bestimmung der Gesamt-Beta-Aktivität in nicht-salzhaltigem
Wasser - Dickschichtverfahren (ISO 9697:2015)
Qualité de l'eau - Activité bêta globale des eaux non salines - Méthode d'essai par
source concentrée (ISO 9697:2015)
Ta slovenski standard je istoveten z: EN ISO 9697:2017
ICS:
13.060.60 Preiskava fizikalnih lastnosti Examination of physical
vode properties of water
17.240 Merjenje sevanja Radiation measurements
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 9697
EUROPEAN STANDARD
NORME EUROPÉENNE
June 2017
EUROPÄISCHE NORM
ICS 13.280; 13.060.60
English Version
Water quality - Gross beta activity in non-saline water -
Test method using thick source (ISO 9697:2015)
Qualité de l'eau - Activité bêta globale des eaux non Wasserbeschaffenheit - Bestimmung der Gesamt-Beta-
salines - Méthode d'essai par source concentrée (ISO Aktivität in nicht-salzhaltigem Wasser -
9697:2015) Dickschichtverfahren (ISO 9697:2015)
This European Standard was approved by CEN on 27 May 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 9697:2017 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO 9697:2015 has been prepared by Technical Committee ISO/TC 147 “Water quality” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 9697:2017
by Technical Committee CEN/TC 230 “Water analysis” the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by December 2017, and conflicting national standards
shall be withdrawn at the latest by December 2017.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 9697:2015 has been approved by CEN as EN ISO 9697:2017 without any modification.

INTERNATIONAL ISO
STANDARD 9697
Third edition
2015-04-01
Water quality — Gross beta activity
in non-saline water — Test method
using thick source
Qualité de l’eau — Activité bêta globale des eaux non salines —
Méthode d’essai par source concentrée
Reference number
ISO 9697:2015(E)
©
ISO 2015
ISO 9697:2015(E)
© ISO 2015
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2015 – All rights reserved

ISO 9697:2015(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Symbols, definitions, and units . 2
4 Principle . 3
5 Reagents and equipment . 3
5.1 Reagents. 3
5.2 Equipment . 3
6 Procedure. 4
6.1 Sampling . 4
6.2 Pretreatment . 4
6.3 Concentration stage . 4
6.4 Sulfation stage . 5
6.5 Ignition stage . 5
6.6 Source preparation . 5
6.7 Measurement . 5
6.8 Determination of counting background . 6
6.9 Preparation of calibration sources . 6
6.10 Sensitivity and bias. 6
6.11 Optimization of the determination . 6
7 Source control . 7
7.1 Contamination check . 7
7.2 Potential disequilibrilium of radionuclides . 7
8 Expression of results . 7
8.1 Calculation of activity concentration . 7
8.2 Standard uncertainty . 8
8.3 Decision threshold . 9
8.4 Detection limit . 9
8.5 Confidence limits. 9
9 Test report .10
Annex A (informative) Example of performance criteria .11
Bibliography .12
ISO 9697:2015(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any
patent rights identified during the development of the document will be in the Introduction and/or on
the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity
assessment, as well as information about ISO’s adherence to the WTO principles in the Technical Barriers
to Trade (TBT), see the following URL: Foreword — Supplementary information.
The committee responsible for this document is ISO/TC 147, Water quality, Subcommittee SC 3,
Radioac
...

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