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ASTM C1468-13

(Test Method)

Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature

Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.  
4.2 Continuous fiber-reinforced ceramic matrix composites generally are characterized by fine grain sized (ZX, τZY) in advanced ceramics, there is significant difficulty in test specimen machining and testing. Improperly prepared notches can produce nonuniform stress distribution in the shear test specimens and can lead to ambiguity of interpretation of strength results. In addition, these shear test specimens also rarely produce a gage section that is in a state of pure shear. Uniaxially-forced transthickness tensile strength tests measure the tensile interlaminar strength  avoid the complications listed above, and provide information on mechanical behavior and strength for a uniformly stressed material. The ultimate strength value measured is not a direct measure of the matrix strength, but a combination of the strength of the matrix and the level of bonding between the fiber, fiber/matrix interphase, and the matrix.  
4.3 CFCCs tested in a transthickness tensile test may fail from a single dominant flaw or from a cumulative damage process; therefore, the volume of material subjected to a uniform tensile stress for a single uniaxially-forceed transthickness tensile test may be a significant factor in determining the ultimate strength of CFCCs. The probabilistic nature of the strength distributions of the brittle matrices of CFCCs requires a sufficient number of test specimens at each testing condition for statistical analysis and design, with guidelines for test specimen size and sufficient numbers provided in this test method. Studies to determine the exact influence of test specimen volume on strength distributions for CFCCs have not been completed. It should be noted that strengths obtained using other recommended test specimens with different volumes and areas may vary due to these volume differences.  
4.4 The r...
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1.1 This test method covers the determination of transthickness tensile strength  under monotonic uniaxial forcing of continuous fiber-reinforced ceramics (CFCC) at ambient temperature. This test method addresses, but is not restricted to, various suggested test specimen geometries, test fixtures, data collection and reporting procedure. In general, round or square test specimens are tensile tested in the direction normal to the thickness by bonding appropriate hardware to the samples and performing the test. For a Cartesian coordinate system, the x-axis and the y-axis are in the plane of the test specimen. The transthickness direction is normal to the plane and is labeled the z-axis for this test method. For CFCCs, the plane of the test specimen normally contains the larger of the three dimensions and is parallel to the fiber layers for uni-directional, bi-directional, and woven composites. Note that transthickness tensile strength as used in this test method refers to the tensile strength obtained under monotonic uniaxial forcing where monotonic refers to a continuous nonstop test rate with no reversals from test initiation to final fracture.  
1.2 This test method is intended primarily for use with all advanced ceramic matrix composites with continuous fiber reinforcement: unidirectional (1-D), bidirectional (2-D), woven, and tridirectional (3-D). In addition, this test method also may be used with glass (amorphous) matrix composites with 1-D, 2-D, and 3-D continuous fiber reinforcement. This test method does not address directly discontinuous fiber-reinforced, whisker-reinforced or particulate-reinforced ceramics, although the test methods detailed here may be equally applicable to these composites. It should be noted that 3-D architectures with a high volume fraction of fibers in the “z” direction may be difficult to test successfully.  
1.3 Values are in accordance with the International System of Units (SI) and ...

General Information

Status
Historical
Publication Date
14-Feb-2013
ICS
81.060.30 - Advanced ceramics
Technical Committee
C28 - Advanced Ceramics
Drafting Committee
C28.07 - Ceramic Matrix Composites
Current Stage
Ref Project

Relations

Replaces
ASTM C1468-06 - Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature
Effective Date
15-Feb-2013
Replaced By
ASTM C1468-19 - Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature
Effective Date
15-Feb-2019
Referred By
ASTM C1468-19a - Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature
Effective Date
15-Feb-2013
Referred By
ASTM C1783-15 - Standard Guide for Development of Specifications for Fiber Reinforced Carbon-Carbon Composite Structures for Nuclear Applications
Effective Date
15-Feb-2013
Referred By
ASTM C1793-15 - Standard Guide for Development of Specifications for Fiber Reinforced Silicon Carbide-Silicon Carbide Composite Structures for Nuclear Applications
Effective Date
15-Feb-2013

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ASTM C1468-13 - Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient TemperatureASTM C1468-13 - Standard Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperature
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1468 − 13
Standard Test Method for
Transthickness Tensile Strength of Continuous Fiber-
1
Reinforced Advanced Ceramics at Ambient Temperature
This standard is issued under the fixed designation C1468; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
1.1 Thistestmethodcoversthedeterminationoftransthick-
T bility of regulatory limitations prior to use. Additional recom-
ness tensile strength S under monotonic uniaxial forcing of
~ !
U
mendations are provided in 6.7 and Section 7.
continuous fiber-reinforced ceramics (CFCC) at ambient tem-
perature. This test method addresses, but is not restricted to,
2. Referenced Documents
various suggested test specimen geometries, test fixtures, data
2
collectionandreportingprocedure.Ingeneral,roundorsquare 2.1 ASTM Standards:
C1145Terminology of Advanced Ceramics
test specimens are tensile tested in the direction normal to the
thickness by bonding appropriate hardware to the samples and C1239Practice for Reporting Uniaxial Strength Data and
performing the test. For a Cartesian coordinate system, the EstimatingWeibull Distribution Parameters forAdvanced
x-axis and the y-axis are in the plane of the test specimen.The Ceramics
transthickness direction is normal to the plane and is labeled C1275Test Method for Monotonic Tensile Behavior of
the z-axisforthistestmethod.ForCFCCs,theplaneofthetest Continuous Fiber-Reinforced Advanced Ceramics with
specimen normally contains the larger of the three dimensions Solid Rectangular Cross-Section Test Specimens at Am-
and is parallel to the fiber layers for uni-directional, bi- bient Temperature
directional, and woven composites. Note that transthickness C1468Test Method for Transthickness Tensile Strength of
tensile strength as used in this test method refers to the tensile Continuous Fiber-ReinforcedAdvanced Ceramics atAm-
strength obtained under monotonic uniaxial forcing where bient Temperature
monotonic refers to a continuous nonstop test rate with no D3878Terminology for Composite Materials
reversals from test initiation to final fracture. E4Practices for Force Verification of Testing Machines
E6Terminology Relating to Methods of MechanicalTesting
1.2 This test method is intended primarily for use with all
E177Practice for Use of the Terms Precision and Bias in
advanced ceramic matrix composites with continuous fiber
ASTM Test Methods
reinforcement: unidirectional (1-D), bidirectional (2-D),
E337Test Method for Measuring Humidity with a Psy-
woven, and tridirectional (3-D). In addition, this test method
chrometer (the Measurement of Wet- and Dry-Bulb Tem-
also may be used with glass (amorphous) matrix composites
peratures)
with 1-D, 2-D, and 3-D continuous fiber reinforcement. This
E691Practice for Conducting an Interlaboratory Study to
test method does not address directly discontinuous fiber-
Determine the Precision of a Test Method
reinforced, whisker-reinforced or particulate-reinforced
IEEE/ASTM SI 10American National Standard for Use of
ceramics, although the test methods detailed here may be
theInternationalSystemofUnits(SI):TheModernMetric
equally applicable to these composites. It should be noted that
System.
3-D architectures with a high volume fraction of fibers in the
E1012Practice for Verification of Testing Frame and Speci-
“z” direction may be difficult to test successfully.
men Alignment Under Tensile and Compressive Axial
1.3 Values are in accordance with the International System
Force Application
of Units (SI) and IEEE/ASTM SI 10.
1.4 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 Definitions:
1
This test method is under the jurisdiction of ASTM Committee C28 on
Advanced Ceramics and is the direct responsibility of Subcommittee C28.07 on
2
Ceramic Matrix Composites. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Feb. 15, 2013. Published April 2013. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2000. Last previous edition approved in 2006 as C1468–06. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/C1468-13. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 -----
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1468 − 06 C1468 − 13
Standard Test Method for
Transthickness Tensile Strength of Continuous Fiber-
1
Reinforced Advanced Ceramics at Ambient Temperature
This standard is issued under the fixed designation C1468; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
T
1.1 This test method covers the determination of transthickness tensile strength ~S ! under monotonic uniaxial forcing of
U
continuous fiber-reinforced ceramics (CFCC) at ambient temperature. This test method addresses, but is not restricted to, various
suggested test specimen geometries, test fixtures, data collection and reporting procedure. In general, round or square test
specimens are tensile tested in the direction normal to the thickness by bonding appropriate hardware to the samples and
performing the test. For a Cartesian coordinate system, the x-axis and the y-axis are in the plane of the test specimen. The
transthickness direction is normal to the plane and is labeled the z-axis for this test method. For CFCCs, the plane of the test
specimen normally contains the larger of the three dimensions and is parallel to the fiber layers for uni-directional, bi-directional,
and woven composites. Note that transthickness tensile strength as used in this test method refers to the tensile strength obtained
under monotonic uniaxial forcing where monotonic refers to a continuous nonstop test rate with no reversals from test initiation
to final fracture.
1.2 This test method is intended primarily for use with all advanced ceramic matrix composites with continuous fiber
reinforcement: unidirectional (1-D), bidirectional (2-D), woven, and tridirectional (3-D). In addition, this test method also may be
used with glass (amorphous) matrix composites with 1-D, 2-D, and 3-D continuous fiber reinforcement. This test method does not
address directly discontinuous fiber-reinforced, whisker-reinforced or particulate-reinforced ceramics, although the test methods
detailed here may be equally applicable to these composites. It should be noted that 3-D architectures with a high volume fraction
of fibers in the “z” direction may be difficult to test successfully.
1.3 Values are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Additional recommendations are provided in 6.7 and Section 7.
2. Referenced Documents
2
2.1 ASTM Standards:
C1145 Terminology of Advanced Ceramics
C1239 Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Ceramics
C1275 Test Method for Monotonic Tensile Behavior of Continuous Fiber-Reinforced Advanced Ceramics with Solid
Rectangular Cross-Section Test Specimens at Ambient Temperature
C1468 Test Method for Transthickness Tensile Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient
Temperature
D3878 Terminology for Composite Materials
E4 Practices for Force Verification of Testing Machines
E6 Terminology Relating to Methods of Mechanical Testing
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E337 Test Method for Measuring Humidity with a Psychrometer (the Measurement of Wet- and Dry-Bulb Temperatures)
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
1
This test method is under the jurisdiction of ASTM Committee C28 on Advanced Ceramics and is the direct responsibility of Subcommittee C28.07 on Ceramic Matrix
Composites.
Current edition approved Jan. 1, 2006Feb. 15, 2013. Published January 2006April 2013. Originally approved in 2000. Last previous edition approved in 20002006 as
C1468 – 00.C1468 – 06. DOI: 10.1520/C1468-06.10.1520/C1468-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor
...

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ASTM C1674-23(Test Method)
Standard Test Method for Flexural Strength of Advanced Ceramics with Engineered Porosity (Honeycomb Cellular Channels) at Ambient Temperatures

SIGNIFICANCE AND USE
5.1 This test method is used to determine the mechanical properties in flexure of engineered ceramic components with multiple longitudinal hollow channels, commonly described as “honeycomb” channel architectures. The components generally have 30 % or more porosity and the cross-sectional dimensions of the honeycomb channels are on the order of 1 mm or greater.  
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Note 1: Flexure testing is the preferred method for determining the nominal “tensile fracture” strength of these components, as compared to a compression (crushing) test. A nominal tensile strength is required, because these materials commonly fail in tension under thermal gradient stresses. A true tensile test is difficult to perform on these honeycomb specimens because of gripping and alignment challenges.  
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1.1 This test method covers the determination of the flexural strength (modulus of rupture in bending) at ambient conditions of advanced ceramic structures with 2-dimensional honeycomb channel architectures.  
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FIG. 1 General Schematics of Typical Honeycomb Ceramic Structures  
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FIG. 2 Flexure Loading Configurations  
L = Outer Span Length (for Test Method A, L = User defined; for Test Method B, L = 90 mm)
Note 1: 4-Point-1/4 Loading for Test Methods A1 and B.
Note 2: 3-Point Loading for Test Method A2.  
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SIGNIFICANCE AND USE
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1.1.3 Test Geometry IIB—A four-point loading system utilizing two force application points equally spaced from their adjacent support points, with a distance between force application points of one-third of the support span.  
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1.1 This test method covers the determination of the effect of surface grinding on the flexure strength of advanced ceramics. Surface grinding of an advanced ceramic material can introduce microcracks and other changes in the near surface layer, generally referred to as damage (see Fig. 1 and Ref. (1)).2 Such damage can result in a change—most often a decrease—in flexure strength of the material. The degree of change in flexure strength is determined by both the grinding process and the response characteristics of the specific ceramic material. This method compares the flexure strength of an advanced ceramic material after application of a user-specified surface grinding process with the baseline flexure strength of the same material. The baseline flexure strength is obtained after application of a surface grinding process specified in this standard. The baseline flexure strength is expected to approximate closely the inherent strength of the material. The flexure strength is measured by means of ASTM flexure test methods.
FIG. 1 Microcracks Associated with Grinding (Ref. (1))2  
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1.3 Materials covered in this standard are those advanced ceramics that meet criteria specified in flexure testing standards C1161 and C1211.  
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SIGNIFICANCE AND USE
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5.2 The Knoop indentation hardness is one of many properties that is used to characterize advanced ceramics. Attempts have been made to relate Knoop indentation hardness to other hardness scales, but no generally accepted methods are available. Such conversions are limited in scope and should be used with caution, except for special cases where a reliable basis for the conversion has been obtained by comparison tests.  
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5.4 The Knoop indentation is shallower than Vickers indentations made at the same force. Knoop indents may be useful in evaluating coating hardnesses.  
5.5 Knoop hardness is calculated from the ratio of the applied force divided by the projected indentation area on the specimen surface. It is assumed that the elastic springback of the narrow diagonal is negligible. (Vickers indenters are also used to measure hardness, but Vickers hardness is calculated from the ratio of applied force to the area of contact of the four faces of the undeformed indenter.)  
5.6 A full hardness characterization includes measurements over a broad range of indentation forces. Knoop hardness of ceramics usually decreases with increasing indentation size or indentation force such as that shown in Fig. 1.6 The trend is known as the in...
SCOPE
1.1 This test method covers the determination of the Knoop indentation hardness of advanced ceramics. In this test, a pointed, rhombic-based, pyramidal diamond indenter of prescribed shape is pressed into the surface of a ceramic with a predetermined force to produce a relatively small, permanent indentation. The surface projection of the long diagonal of the permanent indentation is measured using a light microscope. The length of the long diagonal and the applied force are used to calculate the Knoop hardness which represents the material’s resistance to penetration by the Knoop indenter.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Units—When Knoop and Vickers hardness tests were developed, the force levels were specified in units of grams-force (gf) and kilograms-force (kgf). This standard specifies the units of force and length in the International System of Units (SI); that is, force in newtons (N) and length in mm or μm. However, because of the historical precedent and continued common usage, force values in gf and kgf units are occasionally provided for information. This test method specifies that Knoop hardness be reported either in units of GPa or as a dimensionless Knoop hardness number.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1684-18(2023)(Test Method)
Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature—Cylindrical Rod Strength

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose strength is 50 MPa (~7 ksi) or greater. The test method may also be used with glass test specimens, although Test Methods C158 is specifically designed to be used for glasses. This test method may be used with machined, drawn, extruded, and as-fired round specimens. This test method may be used with specimens that have elliptical cross section geometries.  
4.2 The flexure strength is computed based on simple beam theory with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the rod diameter. The homogeneity and isotropy assumptions in the standard rule out the use of this test for continuous fiber-reinforced ceramics.  
4.3 Flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the loading rate, test environment, specimen size, specimen preparation, and test fixtures (1-3).3 This method includes specific specimen-fixture size combinations, but permits alternative configurations within specified limits. These combinations were chosen to be practical, to minimize experimental error, and permit easy comparison of cylindrical rod strengths with data for other configurations. Equations for the Weibull effective volume and Weibull effective surface are included.  
4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws in the material. Flaws in rods may be intrinsically volume-distributed throughout the bulk. Some of these flaws by chance may be located at or near the outer surface. Flaws may alternatively be intrinsically surface-distrib...
SCOPE
1.1 This test method is for the determination of flexural strength of rod-shaped specimens of advanced ceramic materials at ambient temperature. In many instances it is preferable to test round specimens rather than rectangular bend specimens, especially if the material is fabricated in rod form. This method permits testing of machined, drawn, or as-fired rod-shaped specimens. It allows some latitude in the rod sizes and cross section shape uniformity. Rod diameters between 1.5 and 8 mm and lengths from 25 to 85 mm are recommended, but other sizes are permitted. Four-point-1/4-point as shown in Fig. 1 is the preferred testing configuration. Three-point loading is permitted. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.
FIG. 1 Four-Point-1/4-Point Flexure Loading Configuration  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1211-18(2023)(Test Method)
Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose flexural strength is ∼50 MPa (∼7 ksi) or greater.  
4.2 The flexure stress is computed based on simple beam theory, with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than 1/50 of the beam thickness. The homogeneity and isotropy assumptions in the test method rule out the use of it for continuous fiber-reinforced composites for which Test Method C1341 is more appropriate.  
4.3 The flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the testing rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen and fixture sizes were chosen to provide a balance between the practical configurations and resulting errors as discussed in Test Method C1161, and Refs (1-3).4 Specific fixture and specimen configurations were designated in order to permit the ready comparison of data without the need for Weibull size scaling.  
4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this test method, is highly recommended for all purposes, especially if the data will be used for design as discussed in Ref (4) and Practices C1322 and C1239.  
4.5 This method determines the flexural strength at elevated temperature and ambient environmental conditions at a nominal, moderately fast testing rate. The flexural strength under these conditions may or may not necessarily be the...
SCOPE
1.1 This test method covers determination of the flexural strength of advanced ceramics at elevated temperatures.2 Four-point-1/4-point and three-point loadings with prescribed spans are the standard as shown in Fig. 1. Rectangular specimens of prescribed cross-section are used with specified features in prescribed specimen-fixture combinations. Test specimens may be 3 by 4 by 45 to 50 mm in size that are tested on 40-mm outer span four-point or three-point fixtures. Alternatively, test specimens and fixture spans half or twice these sizes may be used. The test method permits testing of machined or as-fired test specimens. Several options for machining preparation are included: application matched machining, customary procedures, or a specified standard procedure. This test method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The test method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1323-22(Test Method)
Standard Test Method for Ultimate Strength of Advanced Ceramics with Diametrally Compressed C-Ring Specimens at Ambient Temperature

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, material comparison, quality assurance, and characterization. Extreme care should be exercised when generating design data.  
4.2 For a C-ring under diametral compression, the maximum tensile stress occurs at the outer surface. Hence, the C-ring specimen loaded in compression will predominately evaluate the strength distribution and flaw population(s) on the external surface of a tubular component in the hoop direction. Accordingly, the condition of the inner surface may be of lesser consequence in specimen preparation and testing.
Note 1: A C-ring in tension or an O-ring in compression may be used to evaluate the internal surface.  
4.2.1 The flexure stress is computed based on simple curved beam theory (1-5).3 It is assumed that the material is isotropic and homogeneous, the moduli of elasticity are identical in compression or tension, and the material is linearly elastic. These homogeneity and isotropy assumptions preclude the use of this standard for continuous fiber reinforced composites. Average grain size(s) should be no greater than one fiftieth (1/50 ) of the C-ring thickness. The curved beam stress solution from engineering mechanics is in good agreement (within 2 %) with an elasticity solution as discussed in (6) for the test specimen geometries recommended for this standard. The curved beam stress equations are simple and straightforward, and therefore it is relatively easy to integrate the equations for calculations for effective area or effective volume for Weibull analyses as discussed in Appendix X1.  
4.2.2 The simple curved beam and theory of elasticity stress solutions both are two-dimensional plane stress solutions. They do not account for stresses in the axial (parallel to b) direction, or variations in the circumferential (hoop, σθ) stresses through the width (b) of the test piece. The variations in the circumferential stresses increase with increases in width (b) and ring thicknes...
SCOPE
1.1 This test method covers the determination of ultimate strength under monotonic loading of advanced ceramics in tubular form at ambient temperatures. The ultimate strength as used in this test method refers to the strength obtained under monotonic compressive loading of C-ring specimens such as shown in Fig. 1, where monotonic refers to a continuous nonstop test rate with no reversals from test initiation to final fracture. This method permits a range of sizes and shapes since test specimens may be prepared from a variety of tubular structures. The method may be used with microminiature test specimens.
FIG. 1 C-Ring Test Geometry with Defining Geometry and Reference Angle (θ) for the Point of Fracture Initiation on the Circumference  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1730-17(2022)(Test Method)
Standard Test Method for Particle Size Distribution of Advanced Ceramics by X-Ray Monitoring of Gravity Sedimentation

SIGNIFICANCE AND USE
5.1 This test method is useful to both suppliers and users of powders, as outlined in 1.1 and 1.2, in determining particle size distribution for product specifications, manufacturing control, development, and research.  
5.2 Users should be aware that sample concentrations used in this test method may not be what is considered ideal by some authorities, and that the range of this test method extends into the region where Brownian movement could be a factor in conventional sedimentation. Within the range of this test method, neither the sample concentration nor Brownian movement is believed to be significant. Standard reference materials traceable to national standards, of chemical composition specifically covered by this test method, are available from NIST,3 and perhaps other suppliers.  
5.3 Reported particle size measurement is a function of the actual particle dimension and shape factor as well as the particular physical or chemical properties being measured. Caution is required when comparing data from instruments operating on different physical or chemical parameters or with different particle size measurement ranges. Sample acquisition, handling, and preparation can also affect reported particle size results.  
5.4 Suppliers and users of data obtained using this test method need to agree upon the suitability of these data to provide specification for and allow performance prediction of the materials analyzed.
SCOPE
1.1 This test method covers the determination of particle size distribution of advanced ceramic powders. Experience has shown that this test method is satisfactory for the analysis of silicon carbide, silicon nitride, and zirconium oxide in the size range of 0.1 up to 50 µm.  
1.1.1 However, the relationship between size and sedimentation velocity used in this test method assumes that particles sediment within the laminar flow regime. It is generally accepted that particles sedimenting with a Reynolds number of 0.3 or less will do so under conditions of laminar flow with negligible error. Particle size distribution analysis for particles settling with a larger Reynolds number may be incorrect due to turbulent flow. Some materials covered by this test method may settle in water with a Reynolds number greater than 0.3 if large particles are present. The user of this test method should calculate the Reynolds number of the largest particle expected to be present in order to judge the quality of obtained results. Reynolds number (Re) can be calculated using the following equation:
   where:  
  D  =  the diameter of the largest particle expected to be present, in cm,   ρ  =  the particle density, in g/cm3,   ρ0  =  the suspending liquid density, in g/cm3,   g  =  the acceleration due to gravity, 981 cm/sec2, and   η  =  the suspending liquid viscosity, in poise.    
1.1.2 A table of the largest particles that can be analyzed with a suggested maximum Reynolds number of 0.3 or less in water at 35 °C is given for a number of materials in Table 1. A column of the Reynolds number calculated for a 50-µm particle sedimenting in the same liquid system is also given for each material. Larger particles can be analyzed in dispersing media with viscosities greater than that for water. Aqueous solutions of glycerine or sucrose have such higher viscosities.  
1.2 The procedure described in this test method may be applied successfully to other ceramic powders in this general size range, provided that appropriate dispersion procedures are developed. It is the responsibility of the user to determine the applicability of this test method to other materials. Note however that some ceramics, such as boron carbide and boron nitride, may not absorb X-rays sufficiently to be characterized by this analysis method.  
1.3 The values stated in cgs units are to be regarded as the standard, which is the long-standing industry practice. The values given in parentheses are for information onl...

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ASTM C1469-22(Test Method)
Standard Test Method for Shear Strength of Joints of Advanced Ceramics at Ambient Temperature

SIGNIFICANCE AND USE
5.1 Advanced ceramics can be candidate materials for structural applications requiring high degrees of wear and corrosion resistance, often at elevated temperatures.  
5.2 Joints are produced to enhance the performance and applicability of materials. While the joints between similar materials are generally made for manufacturing complex parts and repairing components, those involving dissimilar materials usually are produced to exploit the unique properties of each constituent in the new component. Depending on the joining process, the joint region may be the weakest part of the component. Since under mixed-mode and shear loading the load transfer across the joint requires reasonable shear strength, it is important that the quality and integrity of joint under in-plane shear forces be quantified. Shear strength data are also needed to monitor the development of new and improved joining techniques.  
5.3 Shear tests provide information on the strength and deformation of materials under shear stresses.  
5.4 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.  
5.5 For quality control purposes, results derived from standardized shear test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.
SCOPE
1.1 This test method covers the determination of shear strength of joints in advanced ceramics at ambient temperature using asymmetrical four-point flexure. Test specimen geometries, test specimen fabrication methods, testing modes (that is, force or displacement control), testing rates (that is, force or displacement rate), data collection, and reporting procedures are addressed.  
1.2 This test method is used to measure shear strength of ceramic joints in test specimens extracted from larger joined pieces by machining. Test specimens fabricated in this way are not expected to warp due to the relaxation of residual stresses but are expected to be much straighter and more uniform dimensionally than butt-jointed test specimens prepared by joining two halves, which is not recommended. In addition, this test method is intended for joints, which have either low or intermediate strengths with respect to the substrate material to be joined. Joints with high strengths should not be tested by this test method because of the high probability of invalid tests resulting from fractures initiating at the reaction points rather than in the joint. Determination of the shear strength of joints using this test method is appropriate particularly for advanced ceramic matrix composite materials but also may be useful for monolithic advanced ceramic materials.  
1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are noted in 8.1.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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