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ASTM D3960-02

(Practice)

Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings

Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings

SCOPE
1.1 This practice measures the volatile organic compound (VOC) content of solventborne and waterborne paints and related coatings as determined from the quantity of material released from a sample under specified bake conditions and subtracting exempt volatile compounds and water if present.
Note 1—The regulatory definition, under the control of the U.S. EPA, can change. To ensure currency, contact the local air pollution control agency.
1.2 This practice provides a guide to the selection of appropriate ASTM test methods for the determination of VOC content.
1.3 Certain organic compounds that may be released under the specified bake conditions are not classified as VOC as they do not participate in atmospheric photochemical reactions. Such nonphotochemically reactive compounds are referred to as exempt volatile compounds in this practice.
Note 2—A list of the current US EPA approved exempt volatile compounds is found in Appendix Appendix X3, paragraph X3.1.1.
1.4 VOC content is calculated as a function of (1) the volume of coating less water and exempt volatile compounds, and (2) the volume of coating solids, and (3) the weight of coating solids.

General Information

Status
Historical
Publication Date
09-Jan-2002
ICS
87.040 - Paints and varnishes
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D3960-01 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
Effective Date
10-Jan-2002
Replaced By
ASTM D3960-04 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
Effective Date
01-Mar-2004
Referred By
ASTM A1111-22 - Standard Specification for Cast Iron Closet Flanges for Use with Cast Iron Soil Pipe and Fittings in Gravity Flow Plumbing Drain, Waste, and Vent Sanitary Applications
Effective Date
10-Jan-2002
Referred By
ASTM D2369-20 - Standard Test Method for Volatile Content of Coatings
Effective Date
10-Jan-2002
Referred By
ASTM D4017-22 - Standard Test Method for Water in Paints and Paint Materials by Karl Fischer Method
Effective Date
10-Jan-2002
Referred By
ASTM A888-21a - Standard Specification for Hubless Cast Iron Soil Pipe and Fittings for Sanitary and Storm Drain, Waste, and Vent Piping Applications
Effective Date
10-Jan-2002
Referred By
ASTM A1109-22 - Standard Specification for Special Fittings for Single-Stack Hubless Cast Iron Soil Pipe Fittings for Sanitary, Waste, and Vent Piping Applications
Effective Date
10-Jan-2002
Referred By
ASTM D6053-14(2018) - Standard Test Method for Determination of Volatile Organic Compound (VOC) Content of Electrical Insulating Varnishes
Effective Date
10-Jan-2002
Referred By
ASTM D6886-18 - Standard Test Method for Determination of the Weight Percent Individual Volatile Organic Compounds in Waterborne Air-Dry Coatings by Gas Chromatography
Effective Date
10-Jan-2002
Referred By
ASTM D5201-05a(2020) - Standard Practice for Calculating Formulation Physical Constants of Paints and Coatings
Effective Date
10-Jan-2002
Referred By
ASTM E1795-20a - Standard Specification for Non-Reinforced Liquid Coating Encapsulation Products for Leaded Paint in Buildings
Effective Date
10-Jan-2002
Referred By
ASTM D7768-12(2018) - Standard Test Method for Speciated Organic Volatile Content of Waterborne Multi-Component Coatings by Gas Chromatography
Effective Date
10-Jan-2002
Referred By
ASTM D5324-16(2022) - Standard Guide for Testing Water-Borne Architectural Coatings
Effective Date
10-Jan-2002
Referred By
ASTM D7270-07(2021) - Standard Guide for Environmental and Performance Verification of Factory-Applied Liquid Coatings
Effective Date
10-Jan-2002
Referred By
ASTM D6577-15(2019) - Standard Guide for Testing Industrial Protective Coatings
Effective Date
10-Jan-2002

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ASTM D3960-02 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related CoatingsASTM D3960-02 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
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ASTM D3960-02 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 3960 – 02
Standard Practice for
Determining Volatile Organic Compound (VOC) Content of
1
Paints and Related Coatings
This standard is issued under the fixed designation D 3960; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
2
1. Scope Direct Injection into a Gas Chromatograph
D 3925 Practice for Sampling Liquid Paints and Related
1.1 This practice measures the volatile organic compound
2
Pigmented Coatings
(VOC) content of solventborne and waterborne paints and
D 4017 Test Method for Water in Paints and Paint Materials
related coatings as determined from the quantity of material
2
by Karl Fischer Method
released from a sample under specified bake conditions and
D 4457 Test Method for Determination of Dichloromethane
subtracting exempt volatile compounds and water if present.
and 1,1,1-Trichloroethane in Paints and Coatings by Direct
NOTE 1—The regulatory definition, under the control of the U.S. EPA, 2
Injection into a Gas Chromatograph
can change. To ensure currency, contact the local air pollution control
D 5095 Test Method for Determination of the Nonvolatile
agency.
Content in Silanes, Siloxanes and Silane-Siloxane Blends
3
1.2 This practice provides a guide to the selection of
Used in Masonry Water Repellent Treatments
appropriate ASTM test methods for the determination of VOC
D 5201 Practice for Calculating Formulation Physical Con-
2
content.
stants of Liquid Paints and Coatings
1.3 Certain organic compounds that may be released under
D 5403 Test Methods for Volatile Content of Radiation
3
the specified bake conditions are not classified as VOC as they
Curable Materials
do not participate in atmospheric photochemical reactions.
D 6093 Test Method for Percent Volume Nonvolatile Matter
Such nonphotochemically reactive compounds are referred to
in Clear or Pigmented Coatings Using a Helium Gas
2
as exempt volatile compounds in this practice.
Pycnometer
D 6133 Test Method for Acetone p-Chlorobenzotrifluoride,
NOTE 2—A list of the current US EPA approved exempt volatile
Methyl Acetate or t-Butyl Acetate Content of Solvent-
compounds is found in Appendix Appendix X3, paragraph X3.1.1.1.
Reducible and Water-Reducible Paints, Coatings, Resins,
1.4 VOC content is calculated as a function of (1) the
and Raw Materials by Direct Injection into a Gas Chro-
volume of coating less water and exempt volatile compounds,
2
matograph
and (2) the volume of coating solids, and (3) the weight of
D 6419 Test Method for Volatile Content of Sheet-Fed and
coating solids.
3
Coldset Web Offset Printing Inks
2. Referenced Documents D 6438 Test Method for Acetone, Methyl Acetate, and
Parachlorobenzotrifluoride Content of Paints and Coatings
2.1 ASTM Standards:
2
by Solid Phase Microextraction-Gas Chromatography
D 1475 Test Method for Density of Liquid Coatings, Inks,
2 E 180 Practice for Determining the Precision of ASTM
and Related Products
4
2 Methods for Analysis and Testing of Industrial Chemicals
D 2369 Test Method for Volatile Content of Coatings
2.2 Other Documents:
D 2697 Test Method for Volume Nonvolatile Matter in
2
EPA Federal Reference Method 24—Determination of
Clear or Pigmented Coatings
Volatile Matter Content, Density, Volume Solids, and
D 2832 Guide for Determining Volatile and Nonvolatile
5
2
Weight Solids of Surface Coatings
Content of Paint and Related Coatings
EPA 450/3-84-019, U.S. Environmental Protection Agency
D 3792 Test Method for Water Content of Coatings by
Procedures for Certifying Quantity of Organic Compound
5
Emitted by Paint, Ink, and Other Coatings
1
This practice is under the jurisdiction of ASTM Committee D01 on Paint and
Related Coatings, Materials, and Applications and is the direct responsibility of
3
Subcommittee D01.21 on Chemical Analysis of Paints and Paint Materials. Annual Book of ASTM Standards, Vol 06.02.
4
Current edition approved Jan. 10, 2002. Published March 2002. Originally Annual Book of ASTM Standards, Vol 15.05.
5
published as D 3960 – 81. Last previous edition D 3960 – 01. Available from the Superintendent of Documents, U.S. Government Printing
2
Annual Book of ASTM Standards, Vol 06.01. Office, Washington, DC 20402.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D 3960
EPA 450/3-83-013R, U.S. Environmental Protection 5.4 Only the expression of VOC content as a function of the
Agency Glossary for Air Pollution Control of Industrial volume of coatin
...

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