Standard Test Method for Tensile Strength and Young’s Modulus of Fibers

SIGNIFICANCE AND USE
5.1 Properties determined by this test method are useful in the evaluation of new fibers at the research and development levels. Fibers with diameters up to 250 × 10-6 m are covered by this test method. Very short fibers (including whiskers) call for specialized test techniques (1)3 and are not covered by this test method. This test method may also be useful in the initial screening of candidate fibers for applications in polymer, metal or ceramic matrix composites, and quality control purposes. Because of their nature, ceramic fibers do not have a unique strength, but rather, a distribution of strengths. In most cases when the strength of the fibers is controlled by one population of flaws, the distribution of fiber strengths can be described using a two-parameter Weibull distribution, although other distributions have also been suggested (2,3). This test method constitutes a methodology to obtain the strength of a single fiber. For the purpose of determining the parameters of the distribution of fiber strengths it is recommended to follow this test method in conjunction with Practice C1239.
SCOPE
1.1 This test method covers the preparation, mounting, and testing of single fibers (obtained either from a fiber bundle or a spool) for the determination of tensile strength and Young's modulus at ambient temperature. Advanced ceramic, glass, carbon and other fibers are covered by this test standard.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
14-Aug-2014
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1557 − 14
Standard Test Method for
1
Tensile Strength and Young’s Modulus of Fibers
This standard is issued under the fixed designation C1557; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope designed to be self-aligning if possible, and as thin as practi-
cable to minimize fiber misalignment.
1.1 This test method covers the preparation, mounting, and
3.1.3 system compliance—the contribution by the load train
testing of single fibers (obtained either from a fiber bundle or
system and specimen-gripping system to the indicated cross-
a spool) for the determination of tensile strength and Young’s
head displacement, by unit of force exerted in the load train.
modulus at ambient temperature. Advanced ceramic, glass,
carbon and other fibers are covered by this test standard.
3.2 For definitions of other terms used in this test method,
refer to Terminologies D3878 and E6.
1.2 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this
4. Summary of Test Method
standard.
1.3 This standard may involve hazardous materials, 4.1 A fiber is extracted randomly from a bundle or from a
operations, and equipment. This standard does not purport to spool.
address all of the safety concerns, if any, associated with its
4.2 The fiber is mounted in the testing machine, and then
use. It is the responsibility of the user of this standard to
stressed to failure at a constant cross-head displacement rate.
establish appropriate safety and health practices and deter-
4.3 Avalid test result is considered to be one in which fiber
mine the applicability of regulatory limitations prior to use.
failure doesn’t occur in the gripping region.
2. Referenced Documents
4.4 Tensile strength is calculated from the ratio of the peak
2
force and the cross-sectional area of a plane perpendicular to
2.1 ASTM Standards:
the fiber axis, at the fracture location or in the vicinity of the
C1239Practice for Reporting Uniaxial Strength Data and
fracture location, while Young’s modulus is determined from
EstimatingWeibull Distribution Parameters forAdvanced
thelinearregionofthetensilestressversustensilestraincurve.
Ceramics
D3878Terminology for Composite Materials
5. Significance and Use
E4Practices for Force Verification of Testing Machines
E6Terminology Relating to Methods of MechanicalTesting
5.1 Properties determined by this test method are useful in
E1382Test Methods for Determining Average Grain Size
the evaluation of new fibers at the research and development
-6
Using Semiautomatic and Automatic Image Analysis
levels.Fiberswithdiametersupto250×10 marecoveredby
this test method.Very short fibers (including whiskers) call for
3. Terminology 3
specializedtesttechniques (1) andarenotcoveredbythistest
3.1 Definitions: method. This test method may also be useful in the initial
3.1.1 bundle—a collection of parallel fibers. Synonym, tow. screeningofcandidatefibersforapplicationsinpolymer,metal
or ceramic matrix composites, and quality control purposes.
3.1.2 mounting tab—a thin paper, cardboard, compliant
Because of their nature, ceramic fibers do not have a unique
metal, or plastic strip with a center hole or longitudinal slot of
strength, but rather, a distribution of strengths. In most cases
fixed gage length. The mounting tab should be appropriately
when the strength of the fibers is controlled by one population
of flaws, the distribution of fiber strengths can be described
1
This test method is under the jurisdiction of ASTM Committee C28 on
using a two-parameter Weibull distribution, although other
Advanced Ceramics and is the direct responsibility of Subcommittee C28.07 on
distributions have also been suggested (2,3). This test method
Ceramic Matrix Composites.
constitutes a methodology to obtain the strength of a single
Current edition approved Aug. 15, 2014. Published October 2014. Originally
fiber. For the purpose of determining the parameters of the
approved in 2003. Last previous edition approved in 2013 as C1557–03 (2013).
DOI: 10.1520/C1557-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standardsvolumeinformation,refertothestandard’sDocumentSummarypageon Theboldfacenumbersinparenthesesrefertothelistofreferencesattheendof
the ASTM website. this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1557 − 14
distribution of fiber strengths it is recommen
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1557 − 03 (Reapproved 2013) C1557 − 14
Standard Test Method for
1
Tensile Strength and Young’s Modulus of Fibers
This standard is issued under the fixed designation C1557; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the preparation, mounting, and testing of single fibers (obtained either from a fiber bundle or a
spool) for the determination of tensile strength and Young’s modulus at ambient temperature. Advanced ceramic, glass, carbon and
other fibers are covered by this test standard.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all
of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C1239 Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Ceramics
D3878 Terminology for Composite Materials
E4 Practices for Force Verification of Testing Machines
E6 Terminology Relating to Methods of Mechanical Testing
E1382 Test Methods for Determining Average Grain Size Using Semiautomatic and Automatic Image Analysis
3. Terminology
3.1 Definitions:
3.1.1 bundle—a collection of parallel fibers. Synonym, tow.
3.1.2 mounting tab—a thin paper, cardboard, compliant metal, or plastic strip with a center hole or longitudinal slot of fixed gage
length. The mounting tab should be appropriately designed to be self-aligning if possible, and as thin as practicable to minimize
fiber misalignment.
3.1.3 system compliance—the contribution by the load train system and specimen-gripping system to the indicated cross-head
displacement, by unit of force exerted in the load train.
3.2 For definitions of other terms used in this test method, refer to Terminologies D3878 and E6.
4. Summary of Test Method
4.1 A fiber is extracted randomly from a bundle or from a spool.
4.2 The fiber is mounted in the testing machine, and then stressed to failure at a constant cross-head displacement rate.
4.3 A valid test result is considered to be one in which fiber failure doesn’t occur in the gripping region.
4.4 Tensile strength is calculated from the ratio of the peak force and the cross-sectional area of a plane perpendicular to the
fiber axis, at the fracture location or in the vicinity of the fracture location, while Young’s modulus is determined from the linear
region of the tensile stress versus tensile strain curve.
1
This test method is under the jurisdiction of ASTM Committee C28 on Advanced Ceramics and is the direct responsibility of Subcommittee C28.07 on Ceramic Matrix
Composites.
Current edition approved Aug. 1, 2013Aug. 15, 2014. Published September 2013October 2014. Originally approved in 2003. Last previous edition approved in 20082013
as C1557 – 03 (2008).(2013). DOI: 10.1520/C1557-03R13.10.1520/C1557-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1557 − 14
5. Significance and Use
5.1 Properties determined by this test method are useful in the evaluation of new fibers at the research and development levels.
-6
Fibers with diameters up to 250 × 10 m are covered by this test method. Very short fibers (including whiskers) call for specialized
3
test techniques (1) and are not covered by this test method. This test method may also be useful in the initial screening of candidate
fibers for applications in polymer, metal or ceramic matrix composites, and quality control purposes. Because of their nature,
ceramic fibers do not have a unique strength, but rather, a distribution of strengths. In most cases when the strength of the fibers
is controlled by one population of flaws, th
...

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