Standard Test Method for Oil Absorption of Pigments by Gardner-Coleman Method

SIGNIFICANCE AND USE
4.1 The oil absorption value obtained by this test method provides information about the vehicle demand of the pigment when it is used in a pigment paste. Oil absorption values can be used to characterize batches of a given pigment.  
4.2 This test method differs from Test Method D281 in that D281 requires a vigorous rubbing action whereas this test method involves only a gentle stirring and folding of the pigment. Because the end points are different, the values obtained from the two test methods generally differ.
SCOPE
1.1 This test method covers the determination of oil absorption of pigments by the Gardner-Coleman procedure.2  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2023

Relations

Effective Date
15-Apr-2012
Effective Date
01-Jul-2007
Effective Date
15-Feb-1995
Effective Date
15-Feb-1995

Overview

ASTM D1483-12(2023), titled Standard Test Method for Oil Absorption of Pigments by Gardner-Coleman Method, is an internationally recognized standard published by ASTM International. This test method specifies how to determine the oil absorption value of pigments, a key property affecting their behavior in pigment pastes and related applications. The Gardner-Coleman method provides insight into the vehicle demand of pigments, supporting quality control and batch characterization. This procedure is particularly relevant to industries involved in paints, coatings, inks, and manufacturing processes using pigments.

Key Topics

  • Purpose of Oil Absorption Testing

    • Establishes the amount of oil required to form a soft paste with a given pigment
    • Provides vital data on the pigment's vehicle demand for formulation purposes
    • Supports batch-to-batch consistency assessments
  • Gardner-Coleman vs. D281 Test Method

    • The Gardner-Coleman method involves gentle stirring and folding, unlike the more vigorous spatula rub-out technique of ASTM D281
    • Differences in procedures lead to distinct oil absorption values; results are not interchangeable
  • Test Procedure Summary

    • Utilizes raw linseed oil and a defined mass of pigment
    • Oil is incrementally added while gently folding the pigment until the endpoint is reached (soft paste formation)
    • Oil absorption value is calculated in grams of oil per 100 grams of pigment
  • Reporting and Reliability

    • Results are reported per the specified calculation
    • Repeatability and reproducibility criteria are established for quality assurance
    • Uses SI units as the standard reference

Applications

The Gardner-Coleman method for oil absorption is widely applied across various industries that rely on pigment performance. Key sectors benefiting from this test method include:

  • Paints and Coatings

    • Assures proper pigment dispersion and consistency in liquid paints and other coating formulations
    • Helps manufacturers optimize pigment-vehicle ratios for targeted performance
  • Printing Inks

    • Determines suitable pigment properties for ink formulation, ensuring print quality and stability
  • Plastics, Ceramics, and Construction Materials

    • Supports the evaluation of pigments used as colorants and functional additives
    • Allows for assessment of raw materials to prevent processing issues linked to oil absorption
  • Laboratory Quality Control

    • Facilitates comparison between pigment batches and suppliers
    • Enables monitoring of raw materials, reducing variability in end products

Related Standards

When considering oil absorption and pigment performance, other relevant ASTM standards and international guidelines may include:

  • ASTM D281 - Standard Test Method for Oil Absorption of Pigments by Spatula Rub-out, providing an alternative, more vigorous method
  • ISO 787-5 - General methods of test for pigments and extenders - Part 5: Determination of oil absorption value
  • ASTM D01 Standards - Covering paints, related coatings, and materials, which often reference oil absorption as a key metric

Adhering to the procedures defined in ASTM D1483-12(2023) ensures consistency, accuracy, and compliance with globally recognized best practices in pigment characterization. This standard plays an important role in product development, quality control, and regulatory documentation across the pigment-using industries.

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Frequently Asked Questions

ASTM D1483-12(2023) is a standard published by ASTM International. Its full title is "Standard Test Method for Oil Absorption of Pigments by Gardner-Coleman Method". This standard covers: SIGNIFICANCE AND USE 4.1 The oil absorption value obtained by this test method provides information about the vehicle demand of the pigment when it is used in a pigment paste. Oil absorption values can be used to characterize batches of a given pigment. 4.2 This test method differs from Test Method D281 in that D281 requires a vigorous rubbing action whereas this test method involves only a gentle stirring and folding of the pigment. Because the end points are different, the values obtained from the two test methods generally differ. SCOPE 1.1 This test method covers the determination of oil absorption of pigments by the Gardner-Coleman procedure.2 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 4.1 The oil absorption value obtained by this test method provides information about the vehicle demand of the pigment when it is used in a pigment paste. Oil absorption values can be used to characterize batches of a given pigment. 4.2 This test method differs from Test Method D281 in that D281 requires a vigorous rubbing action whereas this test method involves only a gentle stirring and folding of the pigment. Because the end points are different, the values obtained from the two test methods generally differ. SCOPE 1.1 This test method covers the determination of oil absorption of pigments by the Gardner-Coleman procedure.2 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D1483-12(2023) is classified under the following ICS (International Classification for Standards) categories: 87.060.10 - Pigments and extenders. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D1483-12(2023) has the following relationships with other standards: It is inter standard links to ASTM D281-12, ASTM D281-95(2007), ASTM D281-95, ASTM D281-95(2002). Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D1483-12(2023) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1483 − 12 (Reapproved 2023)
Standard Test Method for
Oil Absorption of Pigments by Gardner-Coleman Method
This standard is issued under the fixed designation D1483; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 4. Significance and Use
4.1 The oil absorption value obtained by this test method
1.1 This test method covers the determination of oil absorp-
provides information about the vehicle demand of the pigment
tion of pigments by the Gardner-Coleman procedure.
when it is used in a pigment paste. Oil absorption values can be
1.2 The values stated in SI units are to be regarded as the
used to characterize batches of a given pigment.
standard. The values given in parentheses are for information
4.2 This test method differs from Test Method D281 in that
only.
D281 requires a vigorous rubbing action whereas this test
1.3 This standard does not purport to address all of the
method involves only a gentle stirring and folding of the
safety concerns, if any, associated with its use. It is the
pigment. Because the end points are different, the values
responsibility of the user of this standard to establish appro-
obtained from the two test methods generally differ.
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
5. Apparatus and Materials
1.4 This international standard was developed in accor-
5.1 Balance, capable of weighing to 0.01 g.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
5.2 Glass Container, round-bottom, having a capacity of
Development of International Standards, Guides and Recom- 1
250 mL ( ⁄2 pt), or a low-form 250 mL beaker.
mendations issued by the World Trade Organization Technical
5.3 Buret, graduated in 0.1 mL divisions.
Barriers to Trade (TBT) Committee.
5.4 Spatula, sharp-edged steel, having a blade 15 mm or
1 3
20 mm by 100 mm ( ⁄2 in. or ⁄4 in. by 4 in.).
2. Referenced Documents
5.5 Linseed Oil, raw, conforming to the following specifi-
2.1 ASTM Standards:
cation:
D281 Test Method for Oil Absorption of Pigments by
Specific Gravity 0.926 – 0.931
Spatula Rub-out
Boiling Point >149 °C
Acid Number 3 ± 1
3. Summary of Test Method
Saponification Value 185 – 196
Iodine Value 170 minimum
3.1 A soft paste is formed by the dropwise addition of
Gardner Color 13 maximum
linseed oil to the gently stirred pigment. The amount of oil
required to form the paste is used to calculate an oil absorption
6. Procedure
value.
6.1 The weight of pigment used should correspond to a
pigment volume of 3.0 mL 6 0.6 mL. Determine the weight
needed by multiplying 3.0 mL 6 0.6 mL by the specific gravity
This test method is under the jurisdiction of ASTM Committee D01 on Paint
of the pigment being tested. For example, a 20 g specimen
and Related Coatings, Materials, and Applications and is the direct responsibility of
normally is used for zinc oxide (3.6 mL × 5.6 g/mL = 20.2 g).
Subcommittee D01.24 on Physical Properties of Liquid Paints & Paint Materials.
Transfer the amount, weighed to 0.01 g, to the glass container.
Current edition approved June 1, 2023. Published June 2023. Originally
approved in 1957. Last previous edition approved in 2016 as D1483 – 12 (2016).
6.2 Add oil from the buret at the rate of about 1 drop per
DOI: 10.1520/D1483-12R23.
...

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