Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer

SIGNIFICANCE AND USE
The test temperature for this test is related to the temperature experienced by the pavement in the geographical area for which the asphalt binder is intended to be used.
The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The complex shear modulus and the phase angle define the resistance to shear deformation of the asphalt binder in the linear viscoelastic region. The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D 6373.
SCOPE
1.1 This test method covers the determination of the dynamic shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry. It is applicable to asphalt binders having dynamic shear modulus values in the range from 100 Pa to 10 MPa. This range in modulus is typically obtained between 4 and 88C at 10 rad/s. This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binders.
1.2 This standard is appropriate for unaged materials, material aged in accordance with Test Method D 2872, material aged in accordance with Practice D 6521, or material aged in accordance with both Test Method D 2872 and Practice D 6521.
1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Status
Historical
Publication Date
14-Sep-2005
Drafting Committee
Current Stage
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ASTM D7175-05e1 - Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer
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e1
Designation:D7175–05
Standard Test Method for
Determining the Rheological Properties of Asphalt Binder
1
Using a Dynamic Shear Rheometer
This standard is issued under the fixed designation D 7175; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1
e NOTE—Editorial changes were made to Sections 7 and 8 in October 2005.
1. Scope D 2872 Test Method for Effect of Heat and Air on Rolling
Film of Asphalt (Rolling Thin Film Oven Test)
1.1 This test method covers the determination of the dy-
D 6373 Specification for Performance-Graded Asphalt
namic shear modulus and phase angle of asphalt binders when
Binder
tested in dynamic (oscillatory) shear using parallel plate
D 6521 Practice for Accelerated Aging of Asphalt Binder
geometry. It is applicable to asphalt binders having dynamic
Using a Pressurized Aging Vessel (PAV)
shearmodulusvaluesintherangefrom100Pato10MPa.This
E77 Test Method for Inspection and Verification of Ther-
range in modulus is typically obtained between 4 and 88°C at
mometers
10rad/s.Thistestmethodisintendedfordeterminingthelinear
E 563 Practice for Preparation and Use of an Ice-Point Bath
viscoelastic properties of asphalt binders as required for
as a Reference Temperature
specification testing and is not intended as a comprehensive
E 644 Test Methods for Testing Industrial Resistance Ther-
procedure for the full characterization of the viscoelastic
mometers
properties of asphalt binders.
E 882 Guide for Accountability and Quality Control in the
1.2 This standard is appropriate for unaged materials, ma-
Chemical Analysis Laboratory
terial aged in accordance with Test Method D 2872, material
2.2 AASHTO Standards:
aged in accordance with Practice D 6521, or material aged in
R29 Practice for Grading or Verifying the Performance
accordance with both Test Method D 2872 and Practice
3
Grade of an Asphalt Binder
D 6521.
T315 Standard Test Method for Determining the Rheologi-
1.3 This standard may involve hazardous materials, opera-
cal Properties of Asphalt Binder Using a Dynamic Shear
tions, and equipment. This standard does not purport to
3
Rheometer
address all of the safety concerns, if any, associated with its
2.3 Deutsche Industrie Norm (DIN) Standard:
use. It is the responsibility of the user of this standard to
4
43760 Standard for Calibration of Thermocouples
establish appropriate safety and health practices and deter-
mine the applicability of regulatory limitations prior to use.
3. Terminology
2. Referenced Documents 3.1 Definitions of Terms Specific to This Standard:
2 3.1.1 annealing, n—the process of removing the effects of
2.1 ASTM Standards:
steric hardening by heating the binder until it is sufficiently
C 670 Practice for Preparing Precision and Bias Statements
fluid so that it can be easily poured.
for Test Methods for Construction Materials
3.1.2 asphalt binder, n—an asphalt-based cement that is
D 140 Practice for Sampling Bituminous Materials
produced from petroleum residue either with or without the
D 2170 Test Method for Kinematic Viscosity of Asphalts
addition of non-particulate modifiers.
(Bitumens)
3.1.3 calibration, n—process whereby the accuracy and
D 2171 Test Method for Viscosity of Asphalts by Vacuum
precision of a device are checked against NIST-traceable
Capillary Viscometer
standards and where necessary adjustments are made to the
device to correct its operation or precision and accuracy.
3.1.3.1 Discussion—Calibration is typically performed by
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
themanufactureroranexternalcommercialcalibrationservice.
and Paving Materials and is the direct responsibility of Subcommittee D04.44 on
Rheological Tests.
Current edition approved Sept. 15, 2005. Published October 2005.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Available from American Association of State Highway and Transportation
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Officials (AASHTO), 444 N. Capitol St., NW, Suite 249, Washington, DC 20001.
4
Standards volume information, refer to the standard’s Document Summary page on Available from Beuth Verlag GmbH (DIN-- DIN Deutsches Institut fur
the ASTM website. Normung e.V.), Burggrafenstrasse 6, 10787, Berlin, Germany.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D7175–05
3.1.4 complex shear modulus (G*), n—ratio calculated by 4. Summary of Test Method
dividing the absolute value of the peak-to-peak shea
...

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