Standard Test Methods for Quantitative Analysis of Textiles

SCOPE
1.1 These test methods cover procedures for the determination of the fiber blend composition of mixtures of the fibers listed in 1.2. Procedures for quantitative estimation of the amount of moisture and certain nonfibrous materials in textiles are also described, for use in the analysis of mixtures, but these are not the primary methods for the determination of moisture content for commercial weights.  
1.2 These test methods cover procedures for the following fiber types:  
1.2.1 Natural Fibers:  
1.2.1.1 Cellulose-Base Fibers: Cotton Hemp Flax Ramie  
1.2.1.2 Protein-Base Fibers: Animal hairs (other than wool) Silk, cultivated Silk, Tussah Wool  
1.2.2 Man-Made Fibers:  
1.2.2.1 Cellulose-Base Fibers: Acetate (secondary) Rayon, viscose or cuprammonium Triacetate  
1.2.2.2 Synthetic-Base Fibers: Acrylic Aramid Modacrylic Nylon 6, Nylon 6-6, others Olefin Polyester Spandex  
1.3 These test methods include the following sections and tables:  Section Referenced Documents 2 Terminology 3 Summary of Methods 4 Uses and Significance 5 Sampling 6 Purity of Reagents 7 Moisture Content or Moisture Regain 8 Nonfibrous Materials 9 Mechanical Separation or Dissection 10 Chemical Test Methods: Summary of Methods 11 Specimens and Symbols 12 No. 1 Acetate Mixed With Other Fibers 13 No. 2 Modacrylic Mixed With Cellulosic Fiber or Wool 14 No. 3 Nylon 6 or Nylon 6-6 Mixed With Natural Fibers or Rayon 15 No. 4 Rayon Mixed With Cotton 16 No. 5 Wool or Polyester Mixed With Cellulosic Fibers or Silk 17 No. 6 Polyester or Acrylic Mixed With Wool 18 No. 7 Natural Cellulosic Material and Rayon Mixed With Acrylic, Modacrylic, and Polyester 19 Referenced Documents 2 No. 8 Polyester Mixed With Olefin 20 No. 9 Polyester Mixed With Acetate or Nylon 6,6-6 21 No. 10 Acrylic Fiber or Linear Spandex Mixed With Nylon or Polyester 22 Microspical Analysis Scope 23 Summary of Method 24 Sampling 25 Apparatus 26 Procedure 27 Indexing Term 28 Table Chemical Methods for Analysis of Fiber Mixtures 1 Solubilities of Various Fibers in Solvents Used in Chemical Methods 2 Comparative Scale for Fineness of Various Textile Fibers 3 Fineness Ranges and Fiber Diameters of Various Textile Fibers 4 Specific Gravity of Various Textile Fibers 5
1.4 The analytical procedures described in the test methods are applicable to the fibers listed in 1.2. The test methods are not satisfactory for the separation of mixtures containing fibers that fall within the same generic class but differ somewhat, either physically or chemically, from each other. These test methods are not satisfactory for the determination of bicomponent fibers.  Note 1-For other methods of analysis covering specific determinations, refer to: Test Methods D461, Test Method D584, Methods D885, Test Method D1113, Test Method D1334, and Test Method D2130. Methods for moisture are covered in Methods D885, Test Method D1576, Test Method D2462, Test Method D2495 and Test Methods D2654. For the determination of commercial weight, refer to Test Method D2494.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
09-Sep-1999
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 629 – 99
Standard Test Methods for
1
Quantitative Analysis of Textiles
This standard is issued under the fixed designation D629; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
INTRODUCTION
Methods D629-59 T, Quantitative Analysis of Textiles, were discontinued in 1969 because the
responsible subcommittee failed to recommend their adoption as a standard after several years of
publication as a tentative. The subcommittee action was based on the members’ knowledge that the
standard did not include several fiber types introduced to the textile trade after the method was
published, and that the techniques required for their identification were lacking in the text, allowing
it to become out of date. The procedures included in the text, however, are believed to be reliable for
the fiber types named and the techniques described are currently being used in the trade and are
referenced by other standards sponsored by Committee D-13 onTextiles. Reinstatement as a standard
using the previously assigned number was requested since the listed procedures were reliable and the
text considered to be the best available, though not all inclusive. Extensive editorial changes were
made in various sections in 1972, and the methods were reinstated as D629-72. Editorial changes
have again been made throughout the text, and statements on precision and bias and suitability for
acceptance testing have been added.
The text of Methods D629-59 T was published by the American Association of Textile Chemists
and Colorists in that society’sTechnical Manual as “Test Method20A-1959” issued in the years 1959
through 1974. The AATCC Method was revised completely in 1975 and since published as “Test
Method20A-1975.”
1. Scope Animal hairs (other than wool)
Silk, cultivated
1.1 These test methods cover procedures for the determina-
Silk, Tussah
tion of the fiber blend composition of mixtures of the fibers
Wool
listed in 1.2. Procedures for quantitative estimation of the
1.2.2 Man-Made Fibers:
amount of moisture and certain nonfibrous materials in textiles
1.2.2.1 Cellulose-Base Fibers:
arealsodescribed,foruseintheanalysisofmixtures,butthese
Acetate (secondary)
are not the primary methods for the determination of moisture
Rayon, viscose or cuprammonium
content for commercial weights.
Triacetate
1.2 These test methods cover procedures for the following
1.2.2.2 Synthetic-Base Fibers:
fiber types:
Acrylic
1.2.1 Natural Fibers:
Aramid
1.2.1.1 Cellulose-Base Fibers:
Modacrylic
Cotton
Nylon 6, Nylon 6-6, others
Hemp
Olefin
Flax
Polyester
Ramie
Spandex
1.2.1.2 Protein-Base Fibers:
1.3 These test methods include the following sections and
tables:
1
These test methods are under the jurisdiction of ASTM Committee D13 on
Section
Textiles and are the direct responsibility of Subcommittee D13.51 on Conditioning
and, Chemical and Thermal Properties.
Referenced Documents 2
Current edition approved Sept. 10, 1999. Published January 2000. Originally
published as D629–41T. Last previous edition D629–88. Withdrawn 1969 and
reinstated 1972 as D629 – 72(1999)
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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D629–99
2
D461 Test Methods for Felt
Section
D584 Test Method for Wool Content of Raw Wool—
Terminology 3
2
Laboratory Scale
Summary of Methods 4
D885 Methods of Testing Tire Cords, Tire Cord Fabrics,
Uses and Significance 5
Sampling 7
and Industrial Filament Yarns Made From Man-Made
Purity of Reagents 6
2
Organic Base Fibers
Moisture Content or Moisture Regain 9
D 1113 TestMethodforVegetableMatterandOtherAlkali-
Nonfibrous Materials 8
2
Mechanical Separation or Dissection 10
Insoluble Impurities in Scoured Wool
Chemical Test Methods:
3
D1193 Specification for Reagent Water
Summary of Methods 11
Specimens and Symbols 12 D1334 Test Method for Wool Content of Raw Wool—
2
No. 1 Acetate Mixed With Other Fibers 13
Commercial Scale
No. 2 Modacrylic Mixed With Cellulosic Fiber or Wool 14
2
D1576 TestMethodforMoistureinWoolbyOvenDrying
No. 3 Nylon 6 or Nylon 6-6 Mixed With Natural Fibers or
Rayon 15 D1909 Table of Commercial Moisture Regains for Textile
2
No. 4 Rayon Mixed With Cotton 16
Fibers
No. 5 Wool or Polyester Mixed With Cellulosic Fibers or Silk 17
D2130 Test Method for Diameter of Wool and Other
No. 6 Polyester or Acrylic Mixed With Wool 18
2
No. 7 Natural Cellulosic Material and Rayon Mixed With Animal Fiber by Microprojection
Acrylic, Modacrylic
...

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