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ASTM D4360-11

(Specification)

Standard Specification for Methyl n-Amyl Ketone

Standard Specification for Methyl <span class="italic">n</span>-Amyl Ketone

ABSTRACT
This certification of coating conformance form provides procurement information concerning products being furnished in accordance with a specific coating specification and additional requirements contained in the purchase order. The certification form is divided into four headings: General Type and Description(I), Buyer Information(II), Seller Information (III), and Certification (IV). The first heading consists of the following information: generic type, manufacturer's designation, specification number, formula number, component number, component identification, and color. The second heading consists purchase order number, release number, part number, item number, and stock number. The third heading consists of seller's representative, batch number, lot number, date of manufacture, and date of certification expiration. The last heading is a paragraph describing the certification.
SCOPE
1.1 This specification covers methyl n-amyl ketone (98 % grade) for use in paint, varnish, lacquer, and related products.
1.2 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.
1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off "to the nearest unit" in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.

General Information

Status
Historical
Publication Date
31-Oct-2011
ICS
71.080.80 - Aldehydes and ketones
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Replaces
ASTM D4360-03 - Standard Specification for Methyl <i>n</i>-Amyl Ketone
Effective Date
01-Nov-2011
Replaced By
ASTM D4360-11(2019) - Standard Specification for Methyl <emph type="bdit">n</emph>-Amyl Ketone
Effective Date
01-Apr-2019

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4360 −11
Standard Specification for
1
Methyl n-Amyl Ketone
This standard is issued under the fixed designation D4360; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1.1 This specification covers methyl n-amyl ketone (98 %
E300 Practice for Sampling Industrial Chemicals
grade) for use in paint, varnish, lacquer, and related products.
2.2 Federal Specification:
1.2 For specific hazard information and guidance, see the
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging
3
supplier’sMaterialSafetyDataSheetformaterialslistedinthis
of
specification.
3. Properties
1.3 The following applies to all specified limits in this
standard; for purposes of determining conformance with this
3.1 Methyl n-amyl ketone shall conform to the following
standard, an observed value or a calculated value shall be requirements:
rounded off “to the nearest unit” in the last right-hand digit
Apparent specific gravity
20/20°C 0.815–0.818
used in expressing the specification limit, in accordance with
or or
the rounding-off method of Practice E29.
25/25°C 0.812–0.815
Color, Pt-Co scale, max (Note 1) 10
2. Referenced Documents Distillation, 760 mm Hg, °C
Initial boiling point, min 147
2
2.1 ASTM Standards:
Dry point, max 153.5
Water, max, weight % 0.1
D268 Guide for Sampling and Testing Volatile Solvents and
Acidity, as acetic acid, max, weight % 0.02
Chemical Intermediates for Use in Paint and Related
Purity, min, weight % 98
Coatings and Material
NOTE 1—Instrumental Pt-Co color determined by Test Method D5386
D1078 Test Method for Distillation Range of Volatile Or-
have been shown to have no statistically significant difference from Pt-Co
ganic Liquids
color determined by Test Method D1209. However, it is not known
D1209 Test Method for Color of Clear Liquids (Platinum-
whether methyl n-amyl ketone was part of the sample set included in the
Cobalt Scale) interlaboratory study.
D1364 Test Method for Water in Volatile Solvents (Karl
4. Sampling
Fischer Reagent Titration Method)
D1613 Test Method for Acidity in Volatile Solvents and 4.1 The material shall be sampled in accordance with
Practice E300.
Chemical Intermediates Used in Paint, Varnish, Lacquer,
and Related Products
5. Test Methods
D3893 Test Method for Purity of Methyl Amyl Ketone and
Methyl Isoamyl Ketone by Gas Chromatography
5.1 The properties enumerated in this specification shall be
D4052 Test Method for Density, Relative Density, and API determined in accordance with the following ASTM methods.
Gravity of Liquids by Digital Density Meter
5.1.1 Apparent Specific Gravity—Determine the specific
D5386 Test Method for Color of Liquids Using Tristimulus gravity by any convenient method that is accurate to the third
Colorimetry
decimal place, the temperature of both specimen and water
being 20 or 25°C. (See Test Method D4052 and the Specific
Gravity section of Guide D268.)
1
This specification is under the jurisdiction of AS
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D4360–03 Designation: D4360 – 11
Standard Specification for
1
Methyl n-Amyl Ketone
This standard is issued under the fixed designation D4360; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This specification covers methyl n-amyl ketone (98 % grade) for use in paint, varnish, lacquer, and related products.
1.2 For specific hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this
specification.
1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard,
an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E29.
2. Referenced Documents
2
2.1 ASTM Standards:
D268 Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and
Material
D1078 Test Method for Distillation Range of Volatile Organic Liquids
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1364 Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
D1613 Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related
Products
D3893 Test Method for Purity of Methyl Amyl Ketone and Methyl Isoamyl Ketone by Gas Chromatography
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter E1Specification for
ASTM Liquid-in-
Glass Thermom-
eters
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E300 Practice for Sampling Industrial Chemicals
2.2 Federal Specification:
3
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging of
3. Properties
3.1 Methyl n-amyl ketone shall conform to the following requirements:
Apparent specific gravity
20/20°C 0.815–0.818
or or
25/25°C 0.812–0.815
Color, Pt-Co scale, max 10
Color, Pt-Co scale, max (Note 1) 10
Distillation, 760 mm Hg, °C
Initial boiling point, min 147
Dry point, max 153.5
1
This specification is under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.
Current edition approved July 10, 2003. Published August 2003. Originally approved in 1984. Last previous edition approved in 1999 as D4360-90(1999). DOI:
10.1520/D4360-03.
Current edition approved Nov. 1, 2011. Published December 2011. Originally approved in 1984. Last previous edition approved in 2003 as D4360 - 03. DOI:
10.1520/D4360-11.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4, Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://dodssp.daps.dla.mil.
*ASummary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D4360 – 11
Water, max, weight % 0.1
Acidity, as acetic acid, max, weight % 0.02
Purity, min, weight % 98
NOTE 1—Instrumental Pt-Co color determined by Test Method D5386 have been shown to have no statistically significant difference from Pt-Co color
determined by Test Method D1209. However, it is not known whether methyl n-amyl ketone was part of the sample set included in the interlaboratory
study.
4. Sampling
4.1 The material shall be sampled in accordance with Practice E300.
5. Test Methods
5.1 The properties enumerated in this specification shall be determined in accordance with the following ASTM methods.
5.1.1 Apparent Specific Gravity—Determine the specific gravity by any convenient method that is accurate to the third decimal
place, the temperature of both specimen and water being 20 or 25°C. (See Test Method D4052 and the Specific Gravity section
of Guide D268
...

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