Standard Practice for Determining the Presence of Sizing in Nylon or Polyester Fabric

SIGNIFICANCE AND USE
5.1 The depth of color achieved in dyeing fabric according to this practice is relative to the amount of sizing in the fabric. This practice employs a chromatic staining scale from 1 to 5 which is inversely proportional to the relative amount of sizing in the fabric. A light color stain indicates a low concentration of sizing and warrants a high numerical rating, while a dark color stain indicates a high concentration of sizing and warrants a low numerical rating.  
5.2 The accuracy of this practice depends upon the ability of the testing personnel to match the color of the stain to the colors in the AATCC 9 Step ChromaticTransference Scale.
SCOPE
1.1 Using a color scale of 1 to 5, this practice describes the procedures for determining the presence and relative amount of sizing in fabrics made of undyed nylon or non-cationically dyeable polyester yarns prepared with a cationically dyeable sizing  
1.2 Procedures and apparatus other than those stated in this standard may be used by agreement of purchaser and supplier with the specific deviations from the standard acknowledged in the report.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Dec-2018
Technical Committee
D13 - Textiles

Relations

Effective Date
01-Jan-2019
Effective Date
01-Mar-2017
Effective Date
15-Sep-2015
Effective Date
01-Sep-2015
Effective Date
01-Apr-2015
Effective Date
15-Jun-2013
Effective Date
15-Jun-2013
Effective Date
15-May-2013
Effective Date
01-Jan-2013
Effective Date
01-Jan-2013
Effective Date
01-Feb-2012
Effective Date
01-Feb-2012
Effective Date
15-Jan-2009
Effective Date
15-Jan-2009
Effective Date
15-Jan-2009

Overview

ASTM D6613-08(2019) is the globally recognized standard practice developed by ASTM International for determining the presence of sizing in nylon or polyester fabrics. This standard outlines a systematic approach to assess the relative amount of cationically dyeable sizing present in undyed nylon or non-cationically dyeable polyester yarns, using a visual, color-based rating scale. The practice is crucial in the textile industry as sizing can affect dye uptake, fabric performance, and subsequent processing.

The method employs a chromatic staining scale, adapted from the AATCC 9 Step Chromatic Transference Scale, to classify fabrics from heavily stained (high sizing content) to negligible staining (low sizing content). The outcome hinges on the operator's ability to accurately compare the dyed fabric’s color to standard reference scales.

Key Topics

  • Sizing Detection: The standard details procedures for detecting and estimating the relative amount of sizing on nylon and polyester textiles, which impacts dyeing results and fabric performance.
  • Chromatic Rating Scale: Test fabrics are classed on a 1 to 5 scale, where a light stain (higher rating) indicates minimal sizing and a dark stain (lower rating) signals heavy sizing.
  • Sample Handling: Specific recommendations are given for sampling, specimen preparation, and reporting to ensure consistency and traceability.
  • Visual Assessment: The visual comparison requires reference to the AATCC 9 Step Chromatic Transference Scale for accurate assignment of class ratings.

Applications

ASTM D6613-08(2019) is extensively used in:

  • Quality Assurance: Textile manufacturers and suppliers use this standard to verify sizing levels in nylon and polyester fabrics before further processing or shipment.
  • Purchaser-Supplier Agreements: The standard supports contractual testing, enabling consistent communication and agreement on test results and acceptance criteria between buyers and sellers.
  • Lot Acceptance and Conformance: Provides procedures for sampling and reporting results, ensuring that fabric lots meet agreed upon specifications.
  • Product Development: Enables R&D teams to optimize fabric finishing processes by controlling sizing levels to achieve desired dyeing and end-use performance.
  • Regulatory and Safety Compliance: Encourages practitioners to adopt proper safety, health, and environmental measures during testing, aligning with international best practices and trade requirements.

Related Standards

  • ASTM D123: Terminology Relating to Textiles - foundational terminology for textile testing and evaluation.
  • ASTM D6799: Terminology Relating to Inflatable Restraints - relevant for certain specialized fabric applications.
  • AATCC Evaluation Procedure #8: Standard procedure and scale used for chromatic assessments during testing.
  • AATCC 9 Step Chromatic Transference Scale: Essential reference for visually grading the test specimens’ staining.

Practical Value

Implementing ASTM D6613-08(2019) helps ensure textile products meet quality standards, minimize processing issues related to excess or insufficient sizing, and facilitate reliable supplier-buyer relationships. The use of a standardized, transparent rating system enhances product consistency across global markets, supporting manufacturers, textile processors, and end-users alike.

Keywords

Sizing detection, nylon fabric, polyester fabric, textile testing, chromatic staining, ASTM D6613, AATCC chromatic scale, quality assurance, fabric processing, textile standards

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Frequently Asked Questions

ASTM D6613-08(2019) is a standard published by ASTM International. Its full title is "Standard Practice for Determining the Presence of Sizing in Nylon or Polyester Fabric". This standard covers: SIGNIFICANCE AND USE 5.1 The depth of color achieved in dyeing fabric according to this practice is relative to the amount of sizing in the fabric. This practice employs a chromatic staining scale from 1 to 5 which is inversely proportional to the relative amount of sizing in the fabric. A light color stain indicates a low concentration of sizing and warrants a high numerical rating, while a dark color stain indicates a high concentration of sizing and warrants a low numerical rating. 5.2 The accuracy of this practice depends upon the ability of the testing personnel to match the color of the stain to the colors in the AATCC 9 Step ChromaticTransference Scale. SCOPE 1.1 Using a color scale of 1 to 5, this practice describes the procedures for determining the presence and relative amount of sizing in fabrics made of undyed nylon or non-cationically dyeable polyester yarns prepared with a cationically dyeable sizing 1.2 Procedures and apparatus other than those stated in this standard may be used by agreement of purchaser and supplier with the specific deviations from the standard acknowledged in the report. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 5.1 The depth of color achieved in dyeing fabric according to this practice is relative to the amount of sizing in the fabric. This practice employs a chromatic staining scale from 1 to 5 which is inversely proportional to the relative amount of sizing in the fabric. A light color stain indicates a low concentration of sizing and warrants a high numerical rating, while a dark color stain indicates a high concentration of sizing and warrants a low numerical rating. 5.2 The accuracy of this practice depends upon the ability of the testing personnel to match the color of the stain to the colors in the AATCC 9 Step ChromaticTransference Scale. SCOPE 1.1 Using a color scale of 1 to 5, this practice describes the procedures for determining the presence and relative amount of sizing in fabrics made of undyed nylon or non-cationically dyeable polyester yarns prepared with a cationically dyeable sizing 1.2 Procedures and apparatus other than those stated in this standard may be used by agreement of purchaser and supplier with the specific deviations from the standard acknowledged in the report. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D6613-08(2019) is classified under the following ICS (International Classification for Standards) categories: 59.080.20 - Yarns. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D6613-08(2019) has the following relationships with other standards: It is inter standard links to ASTM D6613-08(2013), ASTM D123-17, ASTM D123-15b, ASTM D123-15a, ASTM D123-15, ASTM D123-13a, ASTM D123-13ae1, ASTM D123-13, ASTM D6799-13, ASTM D6799-13e1, ASTM D123-12e1, ASTM D123-12, ASTM D123-09e1, ASTM D123-09, ASTM D123-09e2. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D6613-08(2019) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6613 − 08 (Reapproved 2019)
Standard Practice for
Determining the Presence of Sizing in Nylon or Polyester
Fabric
This standard is issued under the fixed designation D6613; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2 For all terminology relating to D13.20, Inflatable
Restraints, refer to Terminology D6799.
1.1 Using a color scale of 1 to 5, this practice describes the
3.2.1 The following terms are relevant to this standard:
proceduresfordeterminingthepresenceandrelativeamountof
extractable matter, sizing.
sizing in fabrics made of undyed nylon or non-cationically
dyeable polyester yarns prepared with a cationically dyeable 3.3 For all other terms related to textiles, see Terminology
sizing D123.
1.2 Procedures and apparatus other than those stated in this
4. Summary of Practice
standard may be used by agreement of purchaser and supplier
4.1 Test specimens of undyed nylon or polyester fabric are
withthespecificdeviationsfromthestandardacknowledgedin
cationically dyed at room temperature. The resulting depth of
the report.
color of the dyed fabric is indicative of the presence and
1.3 This standard does not purport to address all of the
relative amount of cationically dyebable sizing in the fabric.
safety concerns, if any, associated with its use. It is the
4.2 The color of the dyed fabric is matched to a color on an
responsibility of the user of this standard to establish appro-
AATCC chromatic scale to determine the level of sizing in the
priate safety, health, and environmental practices and deter-
fabric.
mine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accor-
5. Significance and Use
dance with internationally recognized principles on standard-
5.1 The depth of color achieved in dyeing fabric according
ization established in the Decision on Principles for the
to this practice is relative to the amount of sizing in the fabric.
Development of International Standards, Guides and Recom-
This practice employs a chromatic staining scale from 1 to 5
mendations issued by the World Trade Organization Technical
whichisinverselyproportionaltotherelativeamountofsizing
Barriers to Trade (TBT) Committee.
in the fabric. A light color stain indicates a low concentration
2. Referenced Documents
of sizing and warrants a high numerical rating, while a dark
color stain indicates a high concentration of sizing and war-
2.1 ASTM Standards:
rants a low numerical rating.
D123Terminology Relating to Textiles
D6799Terminology Relating to Inflatable Restraints
5.2 Theaccuracyofthispracticedependsupontheabilityof
2.2 American Association of Textile Chemists and Colorists
the testing personnel to match the color of the stain to the
(AATCC):
colors in the AATCC 9 Step ChromaticTransference Scale.
AATCC AATCC Evaluation Procedure # 8
6. Apparatus
3. Terminology
6.1 Stainless Steel or Glass Beaker with a capacity of 1000
3.1 Definitions:
ml.
6.2 Glacial Acetic Acid.
ThispracticeisunderthejurisdictionofASTMCommitteeD13onTextilesand
is the direct responsibility of Subcommittee D13.20 on Inflatable Restraints. 6.3 AATCC 9 Step Chromatic Transference Scale .
Current edition approved Jan. 1, 2019. Published January 2019. Originally
6.4 Ventilated Forced Air Drying Ovencapableofmaintain-
approved in 2000. Last previous edition approved in 2013 as D6613–08 (2013).
DOI: 10.1520/D6613-08R19. ing 350° 6 5°F (177 6 3°C).
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
6.5 100 % concentration of Sevron 4G or equivalent Basic
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on Red 14 Dyestuff.
the ASTM website.
3 6.6 Fine Mesh SieveFine mesh sieve with a count of per
Available fromAATCC P.O. Box 12215, Research Triangle Park, N.C. 27709.
inch 100 × 100.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6613 − 08 (2019)
7. Conditioning 10. Report
10.1 State that the test was conducted in accordance with
7.1 Neither preconditioning nor conditioning is necessary.
TestMethodD6613fordeterminingtheresidualsizecontentof
8. Sampling
inflatable restraint fabrics.
8.1 Determining residual size is a destructive test and
10.2 If deviation from Practice D6613 occurred, any refer-
therefore necessitates sampling procedures if used in conjunc-
ence to this standard shall state: “Testing was performed in
tion with lot acceptance of commercial shipments.
accordance with ASTM Practice D6613, with the following
changes.”
8.2 Lot Sample
8.2.1 For acceptance testing, the lot size is the quantity of
10.3 The purchaser and supplier shall determine the exact
fabric
...

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