71.060.01 - Inorganic chemicals in general
ICS 71.060.01 Details
Inorganic chemicals in general
Anorganische Verbindungen im allgemeinen
Chimie minerale en general
Anorganske kemikalije na splošno
General Information
This document specifies one method for the desalination by poultices of porous inorganic materials constituting cultural heritage. The desalination methodology can be applied to salt-loaded porous inorganic materials either affected by salt weathering and/or to allow conservation treatments incompatible with soluble salt(s) contamination, or to prevent salt damage where contamination is known to be present. In all cases the desalination aims to decrease salt content.
Furthermore, this document gives the fundamental requirements for the desalination operation and guidelines for the choice of the most appropriate poultice components according to the characteristics of the substrate and types/quantities of salt(s) present in order to optimize the desalination process.
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This document specifies a methodology applying poultices for the desalination of porous substrate constituting cultural heritage. The desalination methodology can be applied:
- to salt-loaded porous inorganic materials affected by salt weathering, and/or
- to allow conservation treatments incompatible with soluble salt(s) contamination, or
- to prevent salt damage where contamination is known to be present.
In all cases the desalination aims to decrease the salt content.
Furthermore, this document gives the fundamental requirements for the desalination operation and guidelines for the choice of the most appropriate poultice components according to the characteristics of the substrate and types/quantities of salt(s) present in order to optimize the desalination process.
- Standard30 pagesEnglish languagesale 10% offe-Library read for1 day
Describes a method applicable to products having cobalt contents equal to or greater than 0,1 mg/kg. The principle of determination is based on dissolution of a test portion, formation of the coloured cobalt 2-nitrose-1-naphtol complex, extraction with chloroform and photometric measurement at a wavelength of about 530 nm.
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Specifies a method applicable to products in which the nickel content being determined exceeds 0,1 mg/kg. The principle of determination is based on dissolution of a test portion, formation of the coloured nickel furil -dioxime complex, extraction with chloroform and photometric measurement at a wavelength of about 435 nm.
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Alkaline fusion of a test portion by sodium carbonate and subsequent neutralization by sulphuric acid. Measurement of the absorption of the complex formed by chromium and diphenylcarbazide at a wavelength of abour 540 nm after adding sodium azide for elimination of the colour caused by manganese.
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Preliminary reduction of the iron(III) by hydroxylammonium chloride, if required, suppression of the interference of tin by oxalic acid. Formation of the coloured iron(III)-2,2'-dipyridyl complex in a buffered medium. Photometric measurement of the coloured complex at a wavelength of about 522 nm.
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The principle consists in titration of the cloride ions with standard volumetric mercury(II) nitrate solution in presence of diphenylcarbazone as indicator until the colour of the solution matches the mauve of the standard end-point matching solution.
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The principle consists in removal of the boron by evaporation with methanol and separation of manganese and other metals from the residue, by extraction with chloroform, as their diethyldithiocarbamates. Wet destruction of the diethyldithiocarbamates with a sulphuric acid/ hydrogen peroxide mixture. Removal of any interfering iron by extraction as the thiocyanate. Formation of the coloured manganese formaldoxime complex in alkaline solution and photometric measurement at a wavelength of approximately 450 nm.
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