Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons (ISO 15753:2016)

This International Standard describes two methods for the determination of 15 polycyclic aromatic
hydrocarbons (PAHs) in animal and vegetable fats and oils:
— a general method;
— a specific method for coconut oil and vegetable oils with short-chain fatty acids.
These methods are not quantitative for the very volatile compounds such as naphthalene, acenaphthene
and fluorene. Due to interferences provided by the matrix itself, palm oil and olive pomace oil cannot be
analysed using this method.
The quantification limit is 0,2 μg/kg for almost all compounds analysed, except for fluoranthene and
benzo(g,h,i)perylene, where the quantification limit is 0,3 μg/kg, and indeno(1,2,3-c,d)pyrene, where
the quantification limit is 1,0 μg/kg.
NOTE The results for olive pomace oil in Annex B show that this method is not applicable to this type of oil.
The precision data determined are very poor.
Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this
International Standard.

Tierische und pflanzliche Fette und Öle - Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (ISO 15753:2016)

Diese Internationale Norm beschreibt zwei Verfahren zur Bestimmung von 15 polycyclischen aromatischen Kohlenwasserstoffen (PAKs) in tierischen und pflanzlichen Fetten und Ölen:
—   ein allgemeines Verfahren;
—   ein spezielles Verfahren für Kokosfett und Pflanzenöle mit kurzkettigen Fettsäuren.
Diese Verfahren sind bei leicht flüchtigen Verbindungen, wie z. B. Naphthalin, Acenaphthen und Fluoren nicht quantitativ. Aufgrund von Störungen, die durch die Matrix selbst bedingt sind, können Palmöl und Oliven¬tresteröl nicht mit diesem Verfahren analysiert werden.
Die Bestimmungsgrenze beträgt bei fast allen analysierten Verbindungen 0,2 μg/kg, mit Ausnahme von Fluoranthen und Benzo(g,h,i)perylen, deren Bestimmungsgrenze bei 0,3 μg/kg liegt, sowie Indeno(1,2,3 c,d)pyren mit einer Bestimmungsgrenze von 1,0 μg/kg.
ANMERKUNG   Die Ergebnisse für Oliventresteröl in Anhang B zeigen, dass dieses Verfahren nicht für diese Ölart anwendbar ist. Die ermittelten Präzisionsdaten sind sehr schlecht.
Milch und Milcherzeugnisse (oder Fett aus Milch und Milcherzeugnissen) sind vom Anwendungsbereich dieser Internationalen Norm ausgenommen.

Corps gras d'origines animale et végétale - Détermination des hydrocarbures aromatiques polycycliques (ISO 15753:2016)

ISO 15753:2016 décrit deux méthodes pour la détermination de 15 hydrocarbures aromatiques polycycliques (HAP) dans les corps gras d'origines animale et végétale:
?   une méthode générale;
?   une méthode spécifique pour l'huile de coprah et les huiles végétales avec acides gras à chaînes courtes.
Ces méthodes ne sont pas quantitatives pour les composés très volatils tels que le naphtalène, l'acénaphtène et le fluorène. En raison des interférences causées par la matrice elle-même, l'huile de palme et l'huile de grignons d'olive ne peuvent pas être analysées par cette méthode.
La limite de quantification est de 0,2 µg/kg pour la majorité des composés analysés, à l'exception du fluoranthène et du benzo(g,h,i)pérylène, dont la limite de quantification est de 0,3 µg/kg, et de l'indéno(1,2,3-c,d)pyrène, dont la limite de quantification est de 1,0 µg/kg.
NOTE          Les résultats pour l'huile de grignons d'olive dans l'Annexe B montrent que cette méthode n'est pas applicable à ce type d'huile. Les données de fidélité déterminées sont très médiocres.
Le lait et les produits laitiers (ou la graisse provenant du lait et des produits laitiers) sont exclus du domaine d'application de la présente Norme internationale.

Rastlinske in živalske maščobe in olja - Določevanje policikličnih aromatskih ogljikovodikov (ISO 15753:2016)

Ta mednarodni standard opisuje dve metodi za določevanje 15 policikličnih aromatskih
ogljikovodikov (PAH) v živalskih in rastlinskih maščobah in oljih:
– splošno metodo;
– posebno metodo za kokosovo olje in rastlinska olja z maščobnimi kislinami s kratko verigo.
Ti metodi nista kvantitativni za zelo hlapljive spojine, kot so naftalen, acenaften in fluoren. Zaradi motenj, ki jih povzroča sama matrika, s to metodo ni mogoče analizirati palmovega olja in olja iz oljčnih tropin.
Meja kvantifikacije je 0,2 μg/kg pri skoraj vseh analiziranih spojinah, razen fluorantena in benzo(g,h,i)perilena, kjer je meja kvantifikacije 0,3 μg/kg, ter indeno(1,2,3-c,d)pirena, kjer je meja kvantifikacije 1,0 μg/kg.
OPOMBA: Rezultati za olja iz oljčnih tropin iz dodatka B kažejo, da se ta metoda ne uporablja za to vrsto olja. Pridobljeni podatki o natančnosti so zelo slabi.
Mleko in mlečni izdelki (ali maščoba iz mleka in mlečnih izdelkov) niso zajeti v tem mednarodnem standardu.

General Information

Status
Published
Public Enquiry End Date
09-Feb-2016
Publication Date
17-May-2016
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
22-Apr-2016
Due Date
27-Jun-2016
Completion Date
18-May-2016

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 15753:2016
01-junij-2016
1DGRPHãþD
SIST EN ISO 15753:2007
SIST EN ISO 15753:2007/A1:2011
5DVWOLQVNHLQåLYDOVNHPDãþREHLQROMD'RORþHYDQMHSROLFLNOLþQLKDURPDWVNLK
RJOMLNRYRGLNRY ,62
Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons
(ISO 15753:2016)
Tierische und pflanzliche Fette und Öle - Bestimmung von polycyclischen aromatischen
Kohlenwasserstoffen (ISO 15753:2016)
Corps gras d'origines animale et végétale - Détermination des hydrocarbures
aromatiques polycycliques (ISO 15753:2016)
Ta slovenski standard je istoveten z: EN ISO 15753:2016
ICS:
67.200.10 5DVWOLQVNHLQåLYDOVNH Animal and vegetable fats
PDãþREHLQROMD and oils
SIST EN ISO 15753:2016 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 15753:2016

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SIST EN ISO 15753:2016


EN ISO 15753
EUROPEAN STANDARD

NORME EUROPÉENNE

April 2016
EUROPÄISCHE NORM
ICS 67.200.10 Supersedes EN ISO 15753:2006
English Version

Animal and vegetable fats and oils - Determination of
polycyclic aromatic hydrocarbons (ISO 15753:2016)
Corps gras d'origines animale et végétale - Tierische und pflanzliche Fette und Öle - Bestimmung
Détermination des hydrocarbures aromatiques von polycyclischen aromatischen Kohlenwasserstoffen
polycycliques (ISO 15753:2016) (ISO 15753:2016)
This European Standard was approved by CEN on 11 March 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 15753:2016 E
worldwide for CEN national Members.

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SIST EN ISO 15753:2016
EN ISO 15753:2016 (E)
Contents Page
European foreword . 3
2

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SIST EN ISO 15753:2016
EN ISO 15753:2016 (E)
European foreword
This document (EN ISO 15753:2016) has been prepared by Technical Committee ISO/TC 34 “Food
products” in collaboration with Technical Committee CEN/TC 307 “Oilseeds, vegetable and animal fats
and oils and their by-products - Methods of sampling and analysis” the secretariat of which is held by
AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by October 2016, and conflicting national standards shall
be withdrawn at the latest by October 2016.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
This document supersedes EN ISO 15753:2006.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 15753:2016 has been approved by CEN as EN ISO 15753:2016 without any modification.


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SIST EN ISO 15753:2016

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