ISO 6721-9:2019

INTERNATIONAL ISO
STANDARD 6721-9
Second edition
2019-04
Plastics — Determination of dynamic
mechanical properties —
Part 9:
Tensile vibration — Sonic-pulse
propagation method
Plastiques — Détermination des propriétés mécaniques
dynamiques —
Partie 9: Vibration en traction — Méthode de propagation de signaux
acoustiques
Reference number
©
ISO 2019
© ISO 2019
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ii © ISO 2019 – All rights reserved

Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Test device . 2
5.1 Apparatus . 2
5.2 Transducers . 2
5.3 Transducer drive unit . 2
5.4 Pulse arrival time measuring equipment . 3
5.5 Temperature measurement and control equipment . 3
6 Test specimens. 3
6.1 General . 3
6.2 Shape and dimensions . 3
6.3 Preparation . 3
7 Number of specimens . 3
8 Conditioning . 3
9 Procedure. 3
9.1 Test atmosphere . 3
9.2 Mounting the specimen . 3
9.3 Performing the test. 3
9.4 Varying the temperature . 4
10 Calculation and expression of results . 5
10.1 Symbols . 5
10.2 Calculation of the longitudinal wave velocity . 5
10.3 Calculation of the tensile storage modulus, E' . 5
10.4 Significant figures . 5
11 Precision . 5
12 Test report . 5
Annex A (informative) Precision . 7
Bibliography . 8
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
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electrotechnical standardization.
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described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
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This document was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-
chemical properties.
This second edition cancels and replaces the first edition (ISO 6721-9:1997), which has been technically
revised. It also incorporates the Amendment ISO 6721-9:1997/Amd.1:2007. The main changes compared
to the previous edition are as follows:
— the document has been revised editorially;
— normative references have been changed to undated.
A list of all parts in the ISO 6721 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/members .html.
iv © ISO 2019 – All rights reserved

INTERNATIONAL STANDARD ISO 6721-9:2019(E)
Plastics — Determination of dynamic mechanical
properties —
Part 9:
Tensile vibration — Sonic-pulse propagation method
1 Scope
This document describes a pulse propagation method for determining the storage component of the
complex tensile modulus E' of polymers at discrete frequencies typically in the range 3 kHz to 10 kHz.
The method is suitable for measuring materials with storage moduli in the range 0,01 GPa to 200 GPa
and with loss factors below 0,1 at around 10 kHz. With materials having a higher loss, significant errors
in velocity measurement are introduced through decay of amplitude.
The method allows measurements to be made on thin films or fine fibres and long specimens, typically
tapes of 300 mm × 5 mm × 0,1 mm or fibres of 300 mm × 0,1 mm (diameter).
This method may not be suitable for cellular plastics, composite plastics and multilayer products.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 1183-1, Plastics — Methods for determining the density of non-cellular
...