EN 843-6:2009
(Main)Advanced technical ceramics - Mechanical properties of monolithic ceramics at room temperature - Part 6: Guidance for fractographic investigation
Advanced technical ceramics - Mechanical properties of monolithic ceramics at room temperature - Part 6: Guidance for fractographic investigation
This Part of EN 843 contains guidelines to be adopted when evaluating the appearance of the fracture surface of an advanced technical ceramic. The purpose in undertaking this procedure can be various, for example, for material development or quality assessment, to identify normal or abnormal causes of failure, or as a design aid.
NOTE Not all advanced technical ceramics are amenable to fractography. In particular, coarse-grained ceramics can show such rough surfaces that identifying the fracture origin may be impossible. Similarly, porous materials, especially those of a granular nature, tend not to fracture in a continuous manner, making analysis difficult.
Hochleistungskeramik - Mechanische Eigenschaften monolithischer Keramik bei Raumtemperatur - Teil 6: Leitlinie für die fraktographische Untersuchung
Dieser Teil von EN 843 enthält Leitlinien zur Bewertung des Bruchflächenaussehens keramischer Hochleistungswerkstoffe.
Eine Bruchflächenuntersuchung kann zu verschiedenen Zwecken durchgeführt werden,
z. B. zur Werkstoffentwicklung oder zur Qualitätsbeurteilung, zum Erkennen üblicher oder anomaler Ursachen
von Schadensfällen oder zur Hilfe bei der Konstruktion.
ANMERKUNG Nicht alle keramischen Hochleistungswerkstoffe sind für eine fraktographische Auswertung geeignet.
Besonders bei grobkörnigen keramischen Werkstoffen können die Oberflächen so rau sein, dass der Bruchursprung
möglicherweise nicht erkennbar ist. In ähnlicher Weise können auch poröse Werkstoffe eine fraktographische Auswertung
erschweren, besonders dann, wenn sie eine körnige Struktur haben und dazu neigen, nicht kontinuierlich zu brechen.
Céramiques techniques avancées - Propriétés mécaniques des céramiques monolithiques à température ambiante - Partie 6: Guide pour l'analyse fractographique
La présente partie de l'EN 843 contient des directives à adopter lors de l‘évaluation de l'aspect de la surface de rupture d'une céramique technique avancée. Ce mode opératoire peut avoir divers objets, par exemple, l'élaboration ou l'évaluation de la qualité d'un matériau, l'identification de causes anormales de défaillance ou une assistance à la conception. NOTE Les céramiques techniques avancées ne font pas toutes l’objet d’une fractographie. Les céramiques à grains grossiers en particulier peuvent présenter des surfaces d'une rugosité telle que l'identification de l'origine d'une rupture peut s'avérer impossible. De même, les matières poreuses, en particulier de nature granulaire, ont tendance à ne pas se rompre de façon continue, ce qui rend l'analyse difficile.
Sodobna tehnična keramika - Mehanske lastnosti monolitske keramike pri sobni temperaturi - 6. del: Vodilo za fraktografsko raziskavo
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Hochleistungskeramik - Mechanische Eigenschaften monolithischer Keramik bei Raumtemperatur - Teil 6: Leitlinie für die fraktographische UntersuchungCéramiques techniques avancées - Propriétés mécaniques des céramiques monolithiques à température ambiante - Partie 6: Guide pour l'analyse fractographiqueAdvanced technical ceramics - Mechanical properties of monolithic ceramics at room temperature - Part 6: Guidance for fractographic investigation81.060.30Sodobna keramikaAdvanced ceramicsICS:Ta slovenski standard je istoveten z:EN 843-6:2009SIST EN 843-6:2009en,de01-oktober-2009SIST EN 843-6:2009SLOVENSKI
STANDARDSIST-TS CEN/TS 843-6:20041DGRPHãþD
EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 843-6August 2009ICS 81.060.30Supersedes CEN/TS 843-6:2004
English VersionAdvanced technical ceramics - Mechanical properties ofmonolithic ceramics at room temperature - Part 6: Guidance forfractographic investigationCéramiques techniques avancées - Propriétés mécaniquesdes céramiques monolithiques à température ambiante -Partie 6: Guide pour l'analyse fractographiqueHochleistungskeramik - Mechanische Eigenschaftenmonolithischer Keramik bei Raumtemperatur - Teil 6:Leitlinie für die fraktographische UntersuchungThis European Standard was approved by CEN on 16 July 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre:
Avenue Marnix 17,
B-1000 Brussels© 2009 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 843-6:2009: ESIST EN 843-6:2009
Crack patterns in ceramic bodies . 14 Annex B (informative)
Examples of general features of fracture surfaces . 17 Annex C (informative)
Examples of procedure for fracture origin identification. 19 C.1 Single large pores . 20 C.2 Agglomerates . 22 C.3 Large grains . 24 C.4 Compositional inhomogeneities . 26 C.5 Delaminations . 28 C.6 Handling damage . 30 C.7 Machining damage . 31 C.8 Oxidation pitting . 33 C.9 Complex origins . 35 C.10 No obvious origins . 36 Annex D (informative)
Use of fracture mechanical information to aid fractography. 37 D.1 Fracture stress and origin size . 37 D.2 Fracture stress and fracture mirror size . 40 Annex E (informative) Example layout of reporting pro-forma . 42 Bibliography . 44
Part 4: Vickers, Knoop and Rockwell superficial hardness Part 5: Statistical analysis Part 6: Guidance for fractographic investigation
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom.
distinct microstructural discontinuity arising during or after manufacture caused by the action of thermal and/or mechanical stress and leading to the generation of new surfaces which do not completely separate 3.1.2 flaw inhomogeneity which, through stress concentration, can act as a strength defining feature NOTE The term flaw used in this sense does not imply that the component is defective. 3.1.3 fracture process of propagation of a crack through a test-piece or component 3.1.4 fracture origin source from which failure commences 3.2 Terms classifying inherently volume-distributed fracture origins 3.2.1 agglomerate unintentional microstructural inhomogeneity usually of altered density, for example a cluster of grains of abnormal size, particles, platelets or whiskers, resulting from non-uniformity in processing SIST EN 843-6:2009
local variations in chemical composition, usually manifest as agglomerates (3.2.1), or as areas denuded of or enriched in dispersed phases, or as changes in grain size 3.2.3 delamination
generally planar crack within a material arising from the method of manufacture 3.2.4 inclusion discrete inhomogeneity, usually as a result of inorganic contamination by a foreign body not removed during firing 3.2.5 large grain grain which is of abnormally large size as a result of poor particle size control or accelerated grain growth, and which can act as a flaw (3.1.2) 3.2.6 pore cavity or void within a material, which may be isolated or continuously interconnected with others 3.2.7 porous region zone of enhanced porosity, usually three-dimensional in nature and resulting from inhomogeneity or organic contamination in processing 3.2.8 porous seam zone of enhanced porosity, usually linear or planar in nature and resulting from inhomogeneity or organic contamination in processing 3.3 Terms classifying inherently surface-distributed fracture origins 3.3.1 chip small flake of material removed from a surface or an edge of an item or its fracture surface 3.3.2 handling damage scratches, chips or other damage resulting from contact between items, test-pieces or fracture surfaces, not present normally 3.3.3 machining damage result of removal of small chips (see 3.3.1) or the formation of scratches at, or cracks near, the surface resulting from abrasive removal of material 3.3.4 open pore void connected to the external surface, usually by virtue of machining 3.3.5 pit surface depression or surface connected shallow pore, usually resulting from manufacturing conditions or interaction with the external environment SIST EN 843-6:2009
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