Gas analysis - Handling of calibration gases and gas mixtures - Guidelines (ISO 16664:2017)

ISO 16664:2017 describes factors that may influence the composition of pure gases and homogeneous gas mixtures used for calibration purposes. This document only applies to gases or gas mixtures that are within the "utilization period". It provides the following guidelines for the handling and use of calibration gas mixtures:
-      storage of calibration gas cylinders;
-      calibration gas withdrawal from cylinders;
-      transfer of calibration gas from cylinders to the point of calibration.
It also outlines a method of assessing the stability of a gas mixture, taking into account the gas composition uncertainty given on the certificate and the user's measurement uncertainty.

Gasanalyse - Handhabung von Kalibriergasen und Gasgemischen - Richtlinien (ISO 16664:2017)

Diese Internationale Norm beschreibt Faktoren, die die Zusammensetzung von reinen Gasen und homogenen Gasgemischen, die für Kalibrierzwecke verwendet werden, beeinflussen können. Diese Internationale Norm betrifft ausschließlich Gase und Gasgemische innerhalb ihres „Verwendungszeitraums“ unter besonderer Berücksichtigung von
   der Lagerung von Kalibriergasflaschen;
   der Entnahme von Kalibriergas aus Flaschen;
   dem Transfer von Kalibriergas aus Flaschen zur Kalibrierstelle.
Des Weiteren enthält die Norm eine Kurzbeschreibung eines Verfahrens zur Beurteilung der Stabilität eines Gasgemischs, und sie berücksichtigt die im Zertifikat angegebene Unsicherheit der Zusammensetzung des Gases und die Messunsicherheit des Anwenders.

Analyse des gaz - Mise en oeuvre des gaz et des mélanges de gaz pour étalonnage - Lignes directrices (ISO 16664:2017)

L'ISO 16664:2017 décrit les facteurs susceptibles d'influencer la composition des gaz purs et des mélanges de gaz homogènes utilisés à des fins d'étalonnage. L'ISO 16664:2017 ne s'applique qu'aux gaz ou mélanges de gaz considérés dans les limites de la «période d'utilisation». Il donne les lignes directrices suivantes pour la mise en oeuvre et l'utilisation des mélanges de gaz pour étalonnage.
-      le stockage des bouteilles de gaz d'étalonnage;
-      le soutirage du gaz d'étalonnage des bouteilles;
-      le transfert du gaz d'étalonnage des bouteilles vers le point d'étalonnage.
Il présente également une méthode permettant d'évaluer la stabilité d'un mélange de gaz en tenant compte de l'incertitude de la composition du gaz mentionnée sur le certificat et de l'incertitude de mesure liée à l'utilisateur.

Analiza plinov - Ravnanje s kalibracijskimi plini in plinskimi zmesmi - Smernice (ISO 16664:2017)

Ta dokument opisuje dejavnike, ki lahko vplivajo na sestavo čistih plinov in homogenih plinskih zmesi, ki se uporabljajo za namene kalibracije. Ta dokument se uporablja samo za pline in plinske zmesi znotraj »obdobja uporabe«. Podaja naslednje smernice za ravnanje z zmesmi kalibracijskih plinov in njihovo uporabo:
– skladiščenje jeklenk s kalibracijskimi plini;
– odvzem kalibracijskih plinov iz jeklenk;
– prenos kalibracijskih plinov iz jeklenk do mesta kalibracije.
Poleg tega opredeljuje metodo za ocenjevanje stabilnosti plinskih zmesi ob upoštevanju negotovosti sestave plinov, navedene v potrdilu, in negotovosti uporabnikovih meritev.

General Information

Status
Published
Publication Date
13-Jun-2017
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
14-Jun-2017
Completion Date
14-Jun-2017

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SLOVENSKI STANDARD
01-september-2017
1DGRPHãþD
SIST EN ISO 16664:2008
Analiza plinov - Ravnanje s kalibracijskimi plini in plinskimi zmesmi - Smernice
(ISO 16664:2017)
Gas analysis - Handling of calibration gases and gas mixtures - Guidelines (ISO
16664:2017)
Gasanalyse - Handhabung von Kalibriergasen und Gasgemischen - Richtlinien (ISO
16664:2017)
Analyse des gaz - Mise en oeuvre des gaz et des mélanges de gaz pour étalonnage -
Lignes directrices (ISO 16664:2017)
Ta slovenski standard je istoveten z: EN ISO 16664:2017
ICS:
71.040.40 Kemijska analiza Chemical analysis
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 16664
EUROPEAN STANDARD
NORME EUROPÉENNE
June 2017
EUROPÄISCHE NORM
ICS 71.040.40 Supersedes EN ISO 16664:2008
English Version
Gas analysis - Handling of calibration gases and gas
mixtures - Guidelines (ISO 16664:2017)
Analyse des gaz - Mise en oeuvre des gaz et des Gasanalyse - Handhabung von Kalibriergasen und
mélanges de gaz pour étalonnage - Lignes directrices Gasgemischen - Richtlinien (ISO 16664:2017)
(ISO 16664:2017)
This European Standard was approved by CEN on 19 September 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 16664:2017 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
European foreword
This document (EN ISO 16664:2017) has been prepared by Technical Committee ISO/TC 158 "Analysis
of gases".
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by December 2017, and conflicting national standards
shall be withdrawn at the latest by December 2017.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 16664:2008.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 16664:2017 has been approved by CEN as EN ISO 16664:2017 without any modification.

INTERNATIONAL ISO
STANDARD 16664
Second edition
2017-05
Gas analysis — Handling of calibration
gases and gas mixtures — Guidelines
Analyse des gaz — Mise en oeuvre des gaz et des mélanges de gaz
pour étalonnage — Lignes directrices
Reference number
ISO 16664:2017(E)
©
ISO 2017
ISO 16664:2017(E)
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

ISO 16664:2017(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Transport and storage . 3
4.1 General remarks . 3
4.2 Low temperature. 3
4.3 High temperature. 4
4.4 Water . 4
4.5 Storage and handling . 4
5 Mode of withdrawal . 4
5.1 General . 4
5.2 Minimum utilization pressure . 4
5.3 Temperature . 5
5.4 Pressure reduction and flow . 5
5.5 Replacement, change of cylinder positions . 5
6 Transfer system . 5
6.1 Purging procedure . 5
6.2 Considerations when designing and constructing gas transfer lines . 6
6.2.1 Modes of gas sampling . 6
6.2.2 Pressure- and flow-reducing equipment . 7
6.2.3 Material for the construction of transfer lines . 7
6.2.4 General methods and examples of sampling systems .10
7 Stability .13
Annex A (informative) Check on the stability of calibration gas mixtures by end-users .14
Bibliography .16
ISO 16664:2017(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO’s adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following
URL: w w w . i s o .org/ iso/ foreword .html
This document was prepared by Technical Committee ISO/TC 158, Analysis of gases.
This second edition cancels and replaces the first edition (ISO 16664:2004), which has been technically
revised. The major changes are the following:
— Figures 1 and 5 have been revised to more clearly depict the arrangements;
— several references and terminological entries have been updated.
iv © ISO 2017 – All rights reserved

ISO 16664:2017(E)
Introduction
This document uses the terms “calibration gas” for both gas mixtures and pure gases as the limiting
case of gas mixtures.
The quality of calibration gases in cylinders as certified by producers is defined by
a) the correct analyte content;
b) a known uncertainty which is appropriate for its intended use;
c) the stability;
d) the homogeneity.
During its utilization period, the quality of calibration gases is influenced by
— storage conditions at the manufacturer’s and user’s sites;
— transport conditions;
— modes of calibration gas withdrawal and transfer;
— the transfer system employed.
INTERNATIONAL STANDARD ISO 16664:2017(E)
Gas analysis — Handling of calibration gases and gas
mixtures — Guidelines
SAFETY PRECAUTIONS — National and international safety regulations concerning storage,
use and transportation of pure gases and gas mixtures are to be followed in addition to this
document.
1 Scope
This document describes factors that may influence the composition of pure gases and homogeneous
gas mixtures used for calibration purposes. This document only applies to gases or gas mixtures t
...

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