Fine ceramics (advanced ceramics, advanced technical ceramics) - Determination of coating thickness by crater-grinding method (ISO 26423:2009)

ISO 26423:2009 specifies a method for the determination of the thickness of ceramic coatings by a crater grinding method, which includes the grinding of a spherical cavity and subsequent microscopic examination of the crater.
Because of the uncertainty introduced into the measurement of crater dimensions, the test is not suitable for use where the surface roughness of the coating and/or substrate exceeds 20 % of the coating thickness.

Hochleistungskeramik - Bestimmung der Schichtdicke mit dem Kalottenschleifverfahren (ISO 26423:2009)

Diese Internationale Norm legt ein Verfahren zur Bestimmung der Dicke von keramischen Schichten mit einem Kalottenschleifverfahren fest, bei dem eine sphärische Vertiefung geschliffen und anschließend die Kalotte mikroskopisch untersucht wird.
Infolge der sich bei der Messung der Kalottenmaße ergebenden Unsicherheit ist diese Prüfung nicht für Anwendungen geeignet, bei denen die Oberflächenrauheit der Schicht und/oder des Grundwerkstoffes 20 % der Schichtdicke überschreitet.
ANMERKUNG   Ein alternatives Verfahren zur Bestimmung der Dicke mit einem Kontaktprofilometer ist in ISO 18452 angegeben.

Céramiques techniques - Détermination de l'épaisseur de revêtement par la méthode de meulage de cratère (ISO 26423:2009)

L'ISO 26423:2009 spécifie une méthode permettant de déterminer l'épaisseur de revêtements céramiques par une méthode de meulage d'un cratère qui comprend l'obtention par abrasion d'une cavité sphérique suivie d'un examen microscopique du cratère.
En raison de l'incertitude introduite dans le mesurage des dimensions du cratère, l'essai n'est pas approprié lorsque la rugosité de la surface du revêtement et/ou du substrat dépasse 20 % de l'épaisseur du revêtement.

Fina keramika (sodobna keramika, sodobna tehnična keramika) - Ugotavljanje gostote premaza z metodo čelnega brušenja (ISO 26423:2009)

Ta mednarodni standard opredeljuje metodo za določanje debeline keramičnih prevlek z metodo čelnega brušenja, ki zajema brušenje okrogle vdolbine in nato pregled kraterja pod mikroskopom. Zaradi negotovosti, do katere pride pri merjenju kraterja, preskus ni primeren za uporabo v primerih, ko površinska hrapavost prevleke in/ali substrata presega 20 % debeline prevleke.

General Information

Status
Published
Publication Date
19-Apr-2016
Withdrawal Date
30-Oct-2016
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
20-Apr-2016
Due Date
22-Nov-2016
Completion Date
20-Apr-2016

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01-junij-2016
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Fine ceramics (advanced ceramics, advanced technical ceramics) - Determination of
coating thickness by crater-grinding method (ISO 26423:2009)
Hochleistungskeramik - Bestimmung der Schichtdicke mit dem Kalottenschleifverfahren
(ISO 26423:2009)
Céramiques techniques - Détermination de l'épaisseur de revêtement par la méthode de
meulage de cratère (ISO 26423:2009)
Ta slovenski standard je istoveten z: EN ISO 26423:2016
ICS:
25.220.99 Druge obdelave in prevleke Other treatments and
coatings
81.060.30 Sodobna keramika Advanced ceramics
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 26423
EUROPEAN STANDARD
NORME EUROPÉENNE
April 2016
EUROPÄISCHE NORM
ICS 81.060.30 Supersedes EN 1071-2:2002
English Version
Fine ceramics (advanced ceramics, advanced technical
ceramics) - Determination of coating thickness by crater-
grinding method (ISO 26423:2009)
Céramiques techniques - Détermination de l'épaisseur Hochleistungskeramik - Bestimmung der Schichtdicke
de revêtement par la méthode de meulage de cratère mit dem Kalottenschleifverfahren (ISO 26423:2009)
(ISO 26423:2009)
This European Standard was approved by CEN on 25 March 2016.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 26423:2016 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO 26423:2009 has been prepared by Technical Committee ISO/TC 206 “Fine ceramics” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 26423:2016
by Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by
DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by October 2016, and conflicting national standards shall
be withdrawn at the latest by October 2016.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
This document supersedes EN 1071-2:2002.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 26423:2009 has been approved by CEN as EN ISO 26423:2016 without any modification.
INTERNATIONAL ISO
STANDARD 26423
First edition
2009-01-15
Fine ceramics (advanced ceramics,
advanced technical ceramics) —
Determination of coating thickness by
crater-grinding method
Céramiques techniques — Détermination de l'épaisseur de revêtement
par la méthode de meulage de cratère

Reference number
ISO 26423:2009(E)
©
ISO 2009
ISO 26423:2009(E)
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ii © ISO 2009 – All rights reserved

ISO 26423:2009(E)
Contents Page
Foreword. iv
1 Scope . 1
2 Normative references . 1
3 Symbols . 1
4 Principle. 3
5 Sampling. 3
6 Test procedure . 3
6.1 General. 3
6.2 Preparation for the test . 4
6.3 Test parameters . 4
6.4 Example of test parameters. 5
7 Microscopic examination and measurement. 5
7.1 Examination. 5
7.2 Measurement. 5
8 Calculations. 6
9 Uncertainty and sources of error. 7
10 Test report . 7
Annex A (informative) Errors associated with using different formulae for calculating film
thickness . 9
Annex B (informative) Estimating measurement uncertainty and errors. 12
Bibliography . 15

ISO 26423:2009(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 26423 was prepared by Technical Committee ISO/TC 206, Fine ceramics.

iv © ISO 2009 – All rights reserved

INTERNATIONAL STANDARD ISO 26423:2009(E)

Fine ceramics (advanced ceramics, advanced technical
ceramics) — Determination of coating thickness by crater-
grinding method
1 Scope
This International Standard specifies a method for the determination of the thickness of ceramic coatings by a
crater-grinding method, which includes the grinding of a spherical cavity and subsequent microscopic
examination of the crater.
Because of the uncertainty introduced into the measurement of crater dimensions, the test is not suitable for
use where the surface roughness of the coating and/or substrate exceeds 20 % of the coating thickness.
NOTE An alternative method for measurement of thickness, using a contact probe profilometer, is given in
ISO 18452.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 3290-1, Rolling bearings — Balls — Part 1: Steel balls
ISO/IEC 17025:2005, General requirements for the competence of testing and calibration laboratories
3 Symbols
For the purpose of this document, the following symbols apply.
D best estimate of the outer diameter of the crater, at the surface of the coating, in micrometres (see
Figure 1);
d best estimate of the inner diameter of the crater, defined by the bottom of the coating layer, in
micrometres (see Figure 1);
h thickness of the coating, in micrometres (see Figure 1);
m subscript indicating mean value (D , d , X , Y ).
m m m m
r radius of the ball, in micrometres (see Figure 1);
b
r radius of curvature of specimen;
s
l total penetration depth of the ball, in micrometres (see Figure 1);
T
l penetration depth of the ball in the substrate, in micrometres (see Figure 1);
t
ISO 26423:2009(E)
X distance, on a coplanar projection of the two craters, between the periphery of the outer crater and a
diametrically equivalent point on the same side of the inner crater, in micrometres (see Figure 1);
Y distance, on a coplanar projection of the two craters, between the periphery of the outer crater and a
diametrically equivalent point on the opposite side of the inner crater, in micrometres (see Figure 1).

Key
1 coating
2 substrate
Figure 1 — Principal dimensions used in the test method

2 © ISO 2009 – All rights reserved

ISO 26423:2009(E)
4 Principle
Coating thickness often plays a major role in the performance of coated tools and machine parts. Many
different techniques have been developed for assessing the coating thickness. Among these, the crater-
grinding method and the step height method (see ISO 18452) are easy to perform and applicable to most
coated systems.
The method is simple a
...

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