Inorganic fertilizers - Determination of cyanamide nitrogen

This document specifies a method for the determination of cyanamide nitrogen in fertilizers. The method is applicable to calcium cyanamide and mixtures of calcium cyanamide with calcium nitrate.

Anorganische Düngemittel - Bestimmung des Cyanamidstickstoffs

Dieses Dokument legt ein Verfahren zur Bestimmung von Cyanamidstickstoff in Düngemitteln fest. Das Verfahren ist auf Calciumcyanamid und Gemische aus Calciumcyanamid und Calciumnitrat anwendbar.

Engrais inorganiques - Dosage de l'azote cyanamidé

Le présent document spécifie une méthode de dosage de l’azote cyanamidé dans les engrais. La méthode est applicable à la cyanamide calcique et aux mélanges de cyanamide calcique avec du nitrate de calcium.

Anorganska gnojila - Določanje cianoamidnega dušika

Ta dokument določa metodo za določanje cianoamidnega dušika v gnojilih. Metoda se uporablja za kalcijev cianoamid ter mešanice kalcijevega cianoamida in dušika.

General Information

Status
Published
Publication Date
22-Aug-2023
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
23-Aug-2023
Due Date
29-Jun-2023
Completion Date
23-Aug-2023

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SLOVENSKI STANDARD
01-junij-2024
Nadomešča:
SIST EN 15562:2009
Anorganska gnojila - Določanje cianoamidnega dušika
Inorganic fertilizers - Determination of cyanamide nitrogen
Anorganische Düngemittel - Bestimmung des Cyanamidstickstoffs
Engrais inorganiques - Dosage de l'azote cyanamidé
Ta slovenski standard je istoveten z: EN 15562:2023
ICS:
65.080 Gnojila Fertilizers
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN 15562
EUROPEAN STANDARD
NORME EUROPÉENNE
August 2023
EUROPÄISCHE NORM
ICS 65.080 Supersedes EN 15562:2009
English Version
Inorganic fertilizers - Determination of cyanamide
nitrogen
Engrais inorganiques - Dosage de l'azote cyanamidé Anorganische Düngemittel - Bestimmung des
Cyanamidstickstoffs
This European Standard was approved by CEN on 26 June 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 15562:2023 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 4
5 Reagents . 4
6 Apparatus and equipment . 5
7 Sampling and sample preparation . 5
8 Procedure . 6
8.1 Preparation of the solution for analysis . 6
8.2 Analysis of the solution . 6
8.3 Blank test . 7
8.4 Control test . 7
9 Expression of the result . 7
10 Test report . 8
Bibliography . 9
European foreword
This document (EN 15562:2023) has been prepared by Technical Committee CEN/TC 260 “Fertilizers
and liming materials”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by February 2024, and conflicting national standards shall
be withdrawn at the latest by February 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 15562:2009.
In comparison with the previous edition EN 15562:2009, the following technical modifications have been
made:
— technical changes have been made to the description of the procedure (Clause 8) and to Table 1 (8.2);
— deletion of distillation apparatus drawings.
This document has been prepared under a standardization request addressed to CEN by the European
Commission. The Standing Committee of the EFTA States subsequently approves these requests for its
Member States.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,
Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland,
Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North
Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the United
Kingdom.
1 Scope
This document specifies a method for the determination of cyanamide nitrogen in fertilizers. The method
is applicable to calcium cyanamide and mixtures of calcium cyanamide with calcium nitrate.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 1482-2, Fertilizers and liming materials — Sampling and sample preparation — Part 2: Sample
preparation
EN 12944-1, Fertilizers and liming materials — Vocabulary — Part 1: General terms
EN 12944-2, Fertilizers and liming materials — Vocabulary — Part 2: Terms relating to fertilizers
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 12944-1 and EN 12944-2 apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
• IEC Electropedia: available at https://www.electropedia.org/
• ISO Online browsing platform: available at https://www.iso.org/obp
4 Principle
Precipitation of cyanamide nitrogen as a silver complex. Digestion in sulfuric acid with the aid of a
catalyst. Distillation of the ammonia from an alkaline solution, absorption in an excess of sulfuric acid
volumetric solution and back-titration with sodium or potassium hydroxide volumetric solution.
5 Reagents
Use only reagents of recognized analytical grade and water with an electrical conducti
...

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