ASTM C114-11a

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C114 – 11a
Standard Test Methods for
1
Chemical Analysis of Hydraulic Cement
This standard is issued under the fixed designation C114; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
13 Aluminum Oxide
14 Calcium Oxide
1.1 These test methods cover the chemical analyses of
15 Magnesium Oxide
hydraulic cements. Any test methods of demonstrated accept-
16 Sulfur
16.1 Sulfur Trioxide
able precision and bias may be used for analysis of hydraulic
16.2 Sulfide
cements, including analyses for referee and certification pur-
17 Loss On Ignition
poses, as explained in Section 3. Specific chemical test 17.1 Portland Cement
17.2 Portland Blast-Furnace Slag Cement and Slag Cement
methodsareprovidedforeaseofreferenceforthosedesiringto
18 Sodium and Potassium Oxides
use them. They are grouped as Reference Test Methods and
18.1 Total Alkalis
Alternative Test Methods. The reference test methods are long
18.2 Water-Soluble Alkalis
19 Manganic Oxide
accepted classical chemical test methods which provide a
20 Chloride
reasonably well-integrated basic scheme of analysis for hy-
21 Chloroform-Soluble Organic Substances
drauliccements.Thealternativetestmethodsgenerallyprovide Alternative Test Methods
22 Calcium Oxide
individual determination of specific analytes and may be used
23 Carbon Dioxide
alone or as alternates and determinations within the basic
24 Magnesium Oxide
scheme at the option of the analyst and as indicated in the 25 Loss on Ignition
25.1 Portland Blast-Furnace Slag Cement and Slag Cement
individual method.
26 Titanium Dioxide
1.2 Contents:
27 Phosphorus Pentoxide
28 Manganic Oxide
29 Free Calcium Oxide
Section Subject
Appendices Title
2 Referenced Documents
Appendix X1 Example of Determination of Equivalence Point
3 Description of Referee Analyses
for the Chloride Determination
3.1 Referee Analyses
Appendix X2 CO Determinations in Hydraulic Cements
2
4 Qualification for Different Analyses
4.1 Certified Reference Materials
4.2 Requirements for Qualification Testing
1.3 The values stated in SI units are to be regarded as
4.3 Alternative Analyses
standard. No other units of measurement are included in this
4.4 Performance Requirements for Rapid Test Methods
standard.
5 General
5.1 Interferences and Limitations
1.4 This standard does not purport to address all of the
5.2 Apparatus and Materials
safety concerns, if any, associated with its use. It is the
5.3 Reagents
responsibility of the user of this standard to establish appro-
5.4 Sample Preparation
5.5 General Procedures
priate safety and health practices and determine the applica-
5.6 Recommended Order for Reporting Analyses
bility of regulatory limitations prior to use. See 7.3.2.1 and
Reference Test Methods
6 Insoluble Residue 15.4.1 for specific caution statements.
7 Silicon Dioxide
7.2 Cements with Insoluble Residue Less Than 1 %
2. Referenced Documents
7.3 Cements with Insoluble Residue Greater Than 1 %
2
2.1 ASTM Standards:
8 Ammonium Hydroxide Group
9 Ferric Oxide
C25 Test Methods for Chemical Analysis of Limestone,
10 Phosphorus Pentoxide
Quicklime, and Hydrated Lime
11 Titanium Dioxide
D1193 Specification for Reagent Water
12 Zinc Oxide
E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1
These test methods are under the jurisdiction of ASTM Committee C01 on
CementandarethedirectresponsibilityofSubcommitteeC01.23onCompositional
Analysis.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved April 1, 2011. Published May 2011. Originally
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1934. Last previous edition approved in 2011 as C114-11. DOI:
Standards volume information, refer to the standard’s Document Summary page on
10.1520/C0114-11A.
the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C114 – 11a
A
TABLE 1 Maximum Permissible Variations in Results
E275 Practice for Describing and Measuring Performance
of Ultraviolet and Visible Spectrophotometers (Column 3)
(Column 2) Maximum
E350 Test Methods for ChemicalAnalysis of Carbon Steel,
Maximum Difference of the
(Column 1)
Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and
Difference Average of
Analyte
Wrought Iron Between Duplicates from
B
Duplicates CRM Certificate
E617 Specification for Laboratory Weights and Precision
C,D,B
Values
Mass Standa
...