Standard Test Method for Determination of Reference Temperature, T<inf>o</inf>, for Ferritic Steels in the Transition Range

SIGNIFICANCE AND USE
5.1 Fracture toughness is expressed in terms of an elastic-plastic stress intensity factor, KJc, that is derived from the J-integral calculated at fracture.  
5.2 Ferritic steels are microscopically inhomogeneous with respect to the orientation of individual grains. Also, grain boundaries have properties distinct from those of the grains. Both contain carbides or nonmetallic inclusions that can act as nucleation sites for cleavage microcracks. The random location of such nucleation sites with respect to the position of the crack front manifests itself as variability of the associated fracture toughness (16). This results in a distribution of fracture toughness values that is amenable to characterization using the statistical methods in this test method.  
5.3 The statistical methods in this test method presume that the test materials are macroscopically homogeneous such that both the tensile and toughness properties are uniform. The fracture toughness evaluation of nonuniform materials is not amenable to the statistical analysis methods employed in the main body of this test method. For example, multipass weldments can create heat-affected and brittle zones with localized properties that are quite different from either the bulk material or weld. Thick section steel also often exhibits some variation in properties near the surfaces. An appendix to analyze the cleavage toughness properties of nonuniform or inhomogeneous materials is currently being prepared. In the interim, users are referred to (6-8) for procedures to analyze inhomogeneous materials. Metallographic analysis can be used to identify possible nonuniform regions in a material. These regions can then be evaluated through mechanical testing such as hardness, microhardness, and tensile testing to compare with the bulk material. It is also advisable to measure the toughness properties of these nonuniform regions distinctly from the bulk material.  
5.4 Distributions of KJc  data from replicate tests can b...
SCOPE
1.1 This test method covers the determination of a reference temperature, To, which characterizes the fracture toughness of ferritic steels that experience onset of cleavage cracking at elastic, or elastic-plastic KJc instabilities, or both. The specific types of ferritic steels (3.2.1) covered are those with yield strengths ranging from 275 to 825 MPa (40 to 120 ksi) and weld metals, after stress-relief annealing, that have 10 % or less strength mismatch relative to that of the base metal.  
1.2 The specimens covered are fatigue precracked single-edge notched bend bars, SE(B), and standard or disk-shaped compact tension specimens, C(T) or DC(T). A range of specimen sizes with proportional dimensions is recommended. The dimension on which the proportionality is based is specimen thickness.  
1.3 Median KJc values tend to vary with the specimen type at a given test temperature, presumably due to constraint differences among the allowable test specimens in 1.2. The degree of KJc variability among specimen types is analytically predicted to be a function of the material flow properties (1)2 and decreases with increasing strain hardening capacity for a given yield strength material. This KJc dependency ultimately leads to discrepancies in calculated To values as a function of specimen type for the same material. To values obtained from C(T) specimens are expected to be higher than To values obtained from SE(B) specimens. Best estimate comparisons of several materials indicate that the average difference between C(T) and SE(B)-derived To values is approximately 10°C (2). C(T) and SE(B) To differences up to 15°C have also been recorded (3). However, comparisons of individual, small datasets may not necessarily reveal this average trend. Datasets which contain both C(T) and SE(B) specimens may generate To results which fall between the To values calculated using solely C(T) or SE(B) specimens. It is therefore strongly recomme...

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Status
Historical
Publication Date
30-Sep-2015
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM E1921-15ae1 - Standard Test Method for Determination of Reference Temperature, T<inf>o</inf>, for Ferritic Steels in the Transition Range
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: E1921 − 15a
StandardTest Method for
Determination of Reference Temperature, T , for Ferritic
o
1
Steels in the Transition Range
This standard is issued under the fixed designation E1921; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—8.6.2 was editorially corrected in March 2016.
1. Scope solely C(T) or SE(B) specimens. It is therefore strongly
recommended that the specimen type be reported along with
1.1 Thistestmethodcoversthedeterminationofareference
thederivedT valueinallreporting,analysis,anddiscussionof
o
temperature, T , which characterizes the fracture toughness of
o
results. This recommended reporting is in addition to the
ferritic steels that experience onset of cleavage cracking at
requirements in 11.1.1.
elastic, or elastic-plastic K instabilities, or both. The specific
Jc
types of ferritic steels (3.2.1) covered are those with yield
1.4 Requirements are set on specimen size and the number
strengths ranging from 275 to 825 MPa (40 to 120 ksi) and
of replicate tests that are needed to establish acceptable
weld metals, after stress-relief annealing, that have 10% or
characterization of K data populations.
Jc
less strength mismatch relative to that of the base metal.
1.5 T is dependent on loading rate. T is evaluated for a
o o
1.2 The specimens covered are fatigue precracked single-
quasi-static loading rate range with 0.1< dK/dt<2MPa√m/s.
edge notched bend bars, SE(B), and standard or disk-shaped
Slowly loaded specimens (dK/dt < 0.1 MPa√m) can be
compact tension specimens, C(T) or DC(T). A range of
analyzed if environmental effects are known to be negligible.
specimen sizes with proportional dimensions is recommended.
Provision is also made for higher loading rates (dK/dt > 2
The dimension on which the proportionality is based is
MPa√m/s) in Annex A1.
specimen thickness.
1.6 The statistical effects of specimen size on K in the
Jc
1.3 Median K values tend to vary with the specimen type
Jc
transition range are treated using weakest-link theory (4)
at a given test temperature, presumably due to constraint
applied to a three-parameter Weibull distribution of fracture
differences among the allowable test specimens in 1.2. The
toughness values. A limit on K values, relative to the
Jc
degree of K variability among specimen types is analytically
Jc specimen size, is specified to ensure high constraint conditions
2
predicted to be a function of the material flow properties (1)
along the crack front at fracture. For some materials, particu-
and decreases with increasing strain hardening capacity for a
larly those with low strain hardening, this limit may not be
given yield strength material. This K dependency ultimately
Jc
sufficient to ensure that a single-parameter (K ) adequately
Jc
leads to discrepancies in calculated T values as a function of
o describes the crack-front deformation state (5).
specimen type for the same material. T values obtained from
o
1.7 Statistical methods are employed to predict the transi-
C(T) specimens are expected to be higher than T values
o
tion toughness curve and specified tolerance bounds for 1T
obtained from SE(B) specimens. Best estimate comparisons of
specimens of the material tested.The standard deviation of the
several materials indicate that the average difference between
datadistributionisafunctionofWeibullslopeandmedianK .
Jc
C(T) and SE(B)-derived T values is approximately 10°C (2).
o
The procedure for applying this information to the establish-
C(T) and SE(B) T differences up to 15°C have also been
o
ment of transition temperature shift determinations and the
recorded (3). However, comparisons of individual, small data-
establishment of tolerance limits is prescribed.
sets may not necessarily reveal this average trend. Datasets
which contain both C(T) and SE(B) specimens may generate
1.8 This test method assumes that the test material is
T results which fall between the T values calculated using
o o macroscopically homogeneous such that the materials have
uniform tensile and toughness properties. The fracture tough-
nessevaluationofnonuniformmaterialsisnotamenabletothe
1
This test method is under the jurisdiction ofASTM Committee E08 on Fatigue
statistical analysis methods employed in the main body of this
and Fracture and is the direct responsibility of E08.07 on Fracture Mechanics.
Current edition approved Oct. 1, 2015. Published February 2016. Originally
test method. Application of the analysis of this test method to
approved in 1997. Last previous edition approved in 2015 as E1921–15. DOI:
an inhomogeneous material will result in
...

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