ASTM D5396-04(2015)
(Specification)Standard Specification for Reclaimed Perchloroethylene
Standard Specification for Reclaimed Perchloroethylene
ABSTRACT
This specification establishes the requirements for reclaimed perchloroethylene typically needed in various industries for noncritical applications such as in metal cleaning formulations. This is not recommended for dry cleaning applications, but may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs. Covered here are the following types: Type I, generally recognized for use in precision applications; Type II, used for less demanding precision applications; and Type III, general purpose technical grade. Specimens shall be tested and each type should conform individually to the following properties: specific gravity; maximum compositions for chlorides, nonvolatile residue, water, and 1,1,1-trichloroethane; assay weight; color (Pt-Co scale); appearance; acid acceptance (as NaOH); and acidity (as HCl).
SCOPE
1.1 This specification covers the grade of perchloroethylene typically needed in various industries for noncritical applications, such as in metal cleaning formulations. It is not recommended for dry cleaning applications (see Specification D4081). It may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs.
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Designation:D5396 −04 (Reapproved 2015)
Standard Specification for
1,2
Reclaimed Perchloroethylene
This standard is issued under the fixed designation D5396; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D6806 Practice for Analysis of Halogenated Organic Sol-
vents and Their Admixtures by Gas Chromatography
1.1 This specification covers the grade of perchloroethylene
E1064 Test Method for Water in Organic Liquids by Coulo-
typically needed in various industries for noncritical
metric Karl Fischer Titration
applications, such as in metal cleaning formulations. It is not
2.2 Government Documents:
recommended for dry cleaning applications (see Specification
29 CFR 1910.1200 Department of Labor, OSHA Regula-
D4081). It may be used as a reference document by purchasers
tions on Hazard Communication
orbypersonsestablishingin-houseperchloroethylenerecovery
49 CFR 100 to 199 Department ofTransportation Hazardous
programs.
Materials Regulations
2. Referenced Documents
3. Classification
2.1 ASTM Standards:
3.1 Type I—Generally recognized for use in precision ap-
D2108 Test Method for Color of Halogenated Organic
plications.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109 Test Methods for Nonvolatile Matter in Halogenated
3.2 Type II—Use for less demanding precision applications.
Organic Solvents and Their Admixtures
3.3 Type III—General-purpose technical grade.
D2111 Test Methods for Specific Gravity and Density of
Halogenated Organic Solvents and Their Admixtures
4. Properties
D2942 Test Method for Total Acid Acceptance of Haloge-
4.1 Reclaimed perchloroethylene, Type I, shall meet the
nated Organic Solvents (Nonreflux Methods)
requirements of Table 1.
D2988 Test Methods for Water-Soluble Halide Ion in Halo-
genated Organic Solvents and Their Admixtures
4.2 Reclaimed perchloroethylene, Type II, shall meet the
D2989 Test Method for Acidity-Alkalinity of Halogenated requirements of Table 1.
Organic Solvents and Their Admixtures
4.3 Reclaimed perchloroethylene, Type III, shall meet the
D3401 Test Methods for Water in Halogenated Organic
requirements of Table 1.
Solvents and Their Admixtures
D3741 Test Methods for Appearance of Admixtures Con-
5. Packaging and Package Marking
taining Halogenated Organic Solvents
5.1 Industrial or commercial quantities shall be packaged
D4081 Specification for Drycleaning-Grade Perchloroethyl-
and labeled in accordance with DOT regulations as found in
ene
49 CFR 100 to 199, in accordance with state and local
regulations,andinaccordancewithOSHAregulationsfoundin
This specification is under the jurisdiction of ASTM Committee D26 on
29 CFR 1910.1200.
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
responsibility
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5396 − 04 (Reapproved 2010) D5396 − 04 (Reapproved 2015)
Standard Specification for
1,2
Reclaimed Perchloroethylene
This standard is issued under the fixed designation D5396; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers the grade of perchloroethylene typically needed in various industries for noncritical applications,
such as in metal cleaning formulations. It is not recommended for dry cleaning applications (see Specification D4081). It may be
used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs.
2. Referenced Documents
2.1 ASTM Standards:
D2108 Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109 Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
D2942 Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
D2988 Test Methods for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures
D2989 Test Method for Acidity-Alkalinity of Halogenated Organic Solvents and Their Admixtures
D3401 Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
D3741 Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
D4081 Specification for Drycleaning-Grade Perchloroethylene
D6806 Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography
E1064 Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
2.2 OtherGovernment Documents:
29 CFR 1910.1200 1910.1200 Department of Labor, OSHA Regulations, Regulations on Hazard Communication
49 CFR 100 to 199 CFR 100 to 199 Department of Transportation Hazardous Materials Regulations
3. Classification
3.1 Type I—Generally recognized for use in precision applications.
3.2 Type II—Use for less demanding precision applications.
3.3 Type III—General-purpose technical grade.
4. Properties
4.1 Reclaimed perchloroethylene, Type I, shall meet the requirements of Table 1.
4.2 Reclaimed perchloroethylene, Type II, shall meet the requirements of Table 1.
4.3 Reclaimed perchloroethylene, Type III, shall meet the requirements of Table 1.
5. Packaging and Package Marking
5.1 Industrial or commercial quantities shall be packaged and labeled in accordance with DOT regulations as found in 49 CFR
49 CFR 100 to 199, in accordance with state and local regulations, and in accordance with OSHA regulations found in 29 CFR
1919.1200.29 CFR 1910.1200.
This specification is under the jurisdiction of ASTM Committee D26 on Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct responsibility
of Subcommittee D26.02 on Vapor Degreasing.
Current edition approved Feb. 1, 2010June 1, 2015. Published March 2010June 2015. Originally approved in 1993. Last previous edition approved in 20042010 as
D5396 – 04.D53
...
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