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ASTM E1520-23

(Test Method)

Standard Test Method for Particle Counts Per Pound of Granular Carriers and Dry-Applied Granular Formulations

Standard Test Method for Particle Counts Per Pound of Granular Carriers and Dry-Applied Granular Formulations

SIGNIFICANCE AND USE
4.1 This test method was designed principally for clay granular carriers and clay-based granular formulations, but need not be limited to these materials.  
4.2 This procedure is applicable to granules in the range from 6 to 80 mesh (3.36 to 0.17 mm).  
4.3 The sieve sizes used to calculate total particle count will be called the desired range and should be specified as part of the test results.
SCOPE
1.1 This test method is used to determine the number of particles per pound of granular carriers and granular pesticide formulations.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2023
ICS
13.080.20 - Physical properties of soils
Technical Committee
E35 - Pesticides, Antimicrobials, and Alternative Control Agents
Drafting Committee
E35.22 - Pesticide Formulations and Delivery Systems
Current Stage
Ref Project

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ASTM E1520-23 - Standard Test Method for Particle Counts Per Pound of Granular Carriers and Dry-Applied Granular FormulationsASTM E1520-23 - Standard Test Method for Particle Counts Per Pound of Granular Carriers and Dry-Applied Granular Formulations
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E1520 − 23
Standard Test Method for
Particle Counts Per Pound of Granular Carriers and Dry-
1
Applied Granular Formulations
This standard is issued under the fixed designation E1520; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Summary of Test Method
3.1 A known weight of the granular carrier or granular
1.1 This test method is used to determine the number of
pesticide formulation is placed on the top sieve of a stacked set
particles per pound of granular carriers and granular pesticide
of U.S. standard stainless steel screens. The sieves are shaken
formulations.
for a specified period of time. The weight percent of the
1.2 The values stated in SI units are to be regarded as
granules retained on each sieve is determined. The number of
standard. No other units of measurement are included in this
particles per pound of granular material is then calculated.
standard.
4. Significance and Use
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
4.1 This test method was designed principally for clay
responsibility of the user of this standard to establish appro-
granular carriers and clay-based granular formulations, but
priate safety, health, and environmental practices and deter-
need not be limited to these materials.
mine the applicability of regulatory limitations prior to use.
4.2 This procedure is applicable to granules in the range
For specific precautionary statements, see Section 6.
from 6 to 80 mesh (3.36 to 0.17 mm).
1.4 This international standard was developed in accor-
4.3 The sieve sizes used to calculate total particle count will
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the be called the desired range and should be specified as part of
the test results.
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
5. Apparatus
Barriers to Trade (TBT) Committee.
5.1 Mechanical Sieve Shaker, a Tyler RoTap sieve shaker or
2. Referenced Documents equivalent.
2
5.2 Sieves, U.S. standard stainless steel 8-in. diameter sieves
2.1 ASTM Standards:
conforming to Specification E11.
E11 Specification for Woven Wire Test Sieve Cloth and Test
Sieves
5.3 Bottom Receiver Pan and Top Sieve Cover.
E725 Test Method for Sampling Granular Carriers and
5.4 Interval Timer, adjustable, with an accuracy of +10 s.
Granular Pesticides
E726 Test Method for Particle Size Distribution of Granular 5.5 Balance, sensitivity of 0.01 g.
Carriers and Granular Pesticides
6. Safety Precautions
E727/E727M Test Methods for Determining Bulk Density of
Granular Carriers and Granular Pesticides
6.1 Before testing read the precautionary statements on the
product label or the Material Safety Data Sheet (MSDS), or
both. Take proper precautions to prevent skin contact and
inhalation of the fines or vapors, or both. Take care to prevent
1
This test method is under the jurisdiction of ASTM Committee E35 on
contamination of the surrounding area. Always wear the
Pesticides, Antimicrobials, and Alternative Control Agents and is the direct
responsibility of Subcommittee E35.22 on Pesticide Formulations and Delivery
appropriate safety equipment and, where indicated, wear respi-
Systems.
ratory devices approved by (NIOSH) for the product being
Current edition approved April 1, 2023. Published May 2023. Originally
tested.
approved in 1993. Last previous edition approved in 2015 as E1520 – 99 (2015).
DOI: 10.1520/E1520-23.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 7. Procedure
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.1 Record tare weights of each sieve and bottom pan to
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 60.01 g.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1520 − 23
A,B
TABLE 1 Sieve Range Particles per Pound of Each Fraction
7.2 Order stack of screens by size with the finest sieve next
US Sieve Range Multiplication Factor
to the pan.
4/9 1800
7.3 Use a representative sample of 100 6 5 g obtained in
6/8 2200
accordance with Test Method E725. 8/12 3100
12/14 4300
7.4 Weigh the sample to 60.01 g.
14/16 5700
16/18 7300
7.5
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1520 − 99 (Reapproved 2015) E1520 − 23
Standard Test Method for
Particle Counts Per Pound of Granular Carriers and Dry-
1
Applied Granular Formulations
This standard is issued under the fixed designation E1520; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method is used to determine the number of particles per pound of granular carriers and granular pesticide
formulations.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and healthsafety, health, and environmental practices and determine
the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E725 Test Method for Sampling Granular Carriers and Granular Pesticides
E726 Test Method for Particle Size Distribution of Granular Carriers and Granular Pesticides
E727/E727M Test Methods for Determining Bulk Density of Granular Carriers and Granular Pesticides
3. Summary of Test Method
3.1 A known weight of the granular carrier or granular pesticide formulation is placed on the top sieve of a stacked set of U.S.
standard stainless steel screens. The sieves are shaken for a specified period of time. The weight percent of the granules retained
on each sieve is determined. The number of particles per pound of granular material is then calculated.
4. Significance and Use
4.1 This test method was designed principally for clay granular carriers and clay-based granular formulations, but need not be
limited to these materials.
1
This test method is under the jurisdiction of ASTM Committee E35 on Pesticides, Antimicrobials, and Alternative Control Agents and is the direct responsibility of
Subcommittee E35.22 on Pesticide Formulations and Delivery Systems.
Current edition approved Oct. 1, 2015April 1, 2023. Published November 2015May 2023. Originally approved in 1993. Last previous edition approved in 20092015 as
E1520 - 99E1520 – 99 (2015).(2009). DOI: 10.1520/E1520-99R15.10.1520/E1520-23.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1520 − 23
4.2 This procedure is applicable to granules in the range from 8 to 60 mesh (2.36 to 0.256 to 80 mesh (3.36 to 0.17 mm).
4.3 The sieve sizes used to calculate total particle count will be called the desired range and should be specified as part of the test
results.
5. Apparatus
5.1 Mechanical Sieve Shaker, a Tyler RoTap sieve shaker or equivalent.
5.2 Sieves, U.S. standard stainless steel 8-in. diameter sieves conforming to Specification E11.
5.3 Bottom Receiver Pan and Top Sieve Cover.
5.4 Interval Timer, adjustable, with an accuracy of +10 s.
5.5 Balance, sensitivity of 0.01 g.
6. Safety Precautions
6.1 Before testing read the precautionary statements on the product label or the Material Safety Data Sheet (MSDS), or both. Take
proper precautions to prevent skin contact and inhalation of the fines or vapors, or both. Take care to prevent contamination of the
surrounding area. Always wear the appropriate safety equipment and, where indicated, wear respiratory devices approved by
(NIOSH) for the product being tested.
7. Procedure
7.1 Record tare weights of each sieve and bottom pan to 60.01 g.
7.2 Order stack of screens by size with the finest sieve next to the pan.
7.3 Use a representative sample of 100
...

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ASTM D7012-23(Test Method)
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SIGNIFICANCE AND USE
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Standard Test Method for In-Place Density (Unit Weight) and Water Content of Soil Using an Electromagnetic Soil Density Gauge

SIGNIFICANCE AND USE
5.1 The method described determines wet density and gravimetric water content by correlating complex impedance measurement data to an empirically developed model. The empirical model is generated by comparing the electrical properties of typical soils encountered in civil construction projects to their wet densities and gravimetric water contents determined by other accepted methods.  
5.2 The test method described is useful as a rapid, non-destructive technique for determining the in-place total density and gravimetric water content of soil and soil-aggregate mixtures and the determination of dry density.  
5.3 This method may be used for quality control and acceptance of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The non-destructive nature allows for repetitive measurements at a single test location and statistical analysis of the results.
Note 2: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the requirements of Practice D3740 are generally considered capable of competent and objective sampling/testing/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluation some of those factors.
SCOPE
1.1 This test method covers the procedures for determining in-place properties of non-frozen, unbound soil and soil aggregate mixtures such as total density, gravimetric water content and relative compaction by measuring the intrinsic impedance of the compacted soil.  
1.1.1 The method and device described in this test method are intended for in-process quality control of earthwork projects. Site or material characterization is not an intended result.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.2.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight) while the unit for mass is slugs. The rationalized slug unit is not given in this standard.  
1.2.2 In the engineering profession, it is customary practice to use, interchangeably, units representing both mass and force, unless dynamic calculations are involved. This implicitly combines two separate systems of units, that is, the absolute system and the gravimetric system. It is undesirable to combine the use of two separate systems within a single standard. The use of balances or scales recording pounds of mass (lbm), or the recording of density in lbm/ft3 should not be regarded as nonconformance with this standard.  
1.3 All observed and calculated values shall conform to the Guide for Significant Digits and Rounding established in Practice D6026.  
1.3.1 The procedures used to specify how data is collected, recorded, and calculated in this standard are regarded as industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or decrease the number of significant digits of reported data commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in the analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any,...

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ASTM D7698-21(Test Method)
Standard Test Method for In-Place Estimation of Density and Water Content of Soil and Aggregate by Correlation with Complex Impedance Method

SIGNIFICANCE AND USE
5.1 CIMI measurements as described in this Standard Test Method are applicable to measurements of compacted soils intended for roads and foundations.  
5.2 The test method is used for estimating in-place values of density and water content of soils and soil-aggregates based on electrical measurements.  
5.3 The test method may be used for quality control and acceptance testing of compacted soil and soil aggregate mixtures as used in construction and also for research and development. The minimal disturbance nature of the methodology allows repetitive measurements in a single test location and statistical analysis of the results.  
5.4 Limitations:  
5.4.1 This test method provides an overview of the CIMI measurement procedure using a controlling console connected to a soil sensor unit which applies a 3.0 MHz RF voltage to an in-place soil via metallic probes that are driven into the soil at a prescribed distance apart. This test method does not discuss the details of the CIMI electronics, computer, or software that utilize on-board algorithms for estimating the soil density and water content  
5.4.2 It is difficult to address an infinite variety of soils in this standard. However, data presented in X3.1 provides a list of soil types that are applicable for the CIMI use.  
5.4.3 The procedures used to specify how data are collected, recorded, or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures prescribed in this standard do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.
Note 1: Notwithstanding th...
SCOPE
1.1 Purpose and Application—This test method describes the procedure, equipment, and interpretation methods for estimating in-place soil dry density and water content using a Complex-Impedance Measuring Instrument (CIMI).  
1.1.1 The purpose and application of this test method is for testing porous material such as used in roadway base or building foundations that may be deployed in the field at various test sites. The test apparatus includes electrodes that contact the porous material under test and a sensor unit that supplies electromagnetic signals to the porous material. Response signals reveal electrical parameters such as complex impedance which can be equated to material properties such as density and moisture content.  
1.1.2 CIMI measurements as described in this test method are applicable to measurements of compacted soils intended for roads and foundations.  
1.1.3 This test method describes the procedure for estimating in-place density and water content of soils and soil-aggregates by use of a CIMI. The electrical properties of the soil are measured using a radio frequency (RF) voltage source connected to soil electrical probes driven into the soils and soil-aggregates to be tested, in a prescribed pattern and depth. Certain algorithms of these properties are related to wet density and water content. This correlation between electrical measurements, and density and water content is accomplished using a calibration methodology. In the calibration methodology, density and water content are determined by other ASTM Test Standards that measure soil density and water content, thereafter correlating the corresponding measured electrical properties to the soil physical properties.  
1.2 Units—The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions which are provided for information purposes only and are not considered standard.  
1.2.1...

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ASTM D6572-21(Test Method)
Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test

SIGNIFICANCE AND USE
5.1 The crumb test provides a simple, quick method for field or laboratory identification of a dispersive clayey soil. The internal erosion failures of a number of homogeneous earth dams, erosion along channel or canal banks, and rainfall erosion of earthen structures have been attributed to colloidal erosion along cracks or other flow channels formed in masses of dispersive clay (5).  
5.2 The crumb test, as originally developed by Emerson (6), was called the aggregate coherence test and had seven different categories of soil-water reactions. Sherard (5) later simplified the test by combining some soil-water reactions so that only four categories, or grades, of soil dispersion are observed during the test. The crumb test is a relatively accurate positive indicator of the presence of dispersive properties in a soil. The crumb test, however, is not a completely reliable negative indicator that soils are not dispersive. The crumb test can seldom be relied upon as a sole test method for determining the presence of dispersive clays. The double-hydrometer test (Test Method D4221) and pinhole test (Test Method D4647/D4647M) are test methods that provide valuable additional insight into the probable dispersive behavior of clay soils.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depends on several factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 Two test methods are provided to give a qualitative indication of the natural dispersive characteristics of clayey soils: Method A and Method B.  
1.1.1 Method A—Procedure for Natural Soil Crumbs described in 10.1.  
1.1.2 Method B—Procedure for Remolded Soil Crumbs described in 10.2.  
1.2 The crumb test, while a good, quick indication of dispersive soil, should usually be run in conjunction with a pinhole test and a double hydrometer test, Test Methods D4647/D4647M and D4221, respectively. Since this test method may not identify all dispersive clay soils, other tests such as, pinhole dispersion (Test Methods D4647/D4647M), double hydrometer (Test Method D4221) and the analysis of pore water extraction (Test Methods D4542) may be performed individually or used together to help verify dispersion.  
1.3 The crumb test has some limitations in its usefulness as an indicator of dispersive soil. A dispersive soil may sometimes give a non-dispersive reaction in the crumb test. Soils containing kaolinite with known field dispersion problems, have shown non-dispersive reactions in the crumb test (1).2 However, if the crumb test indicates dispersion, the soil is probably dispersive.  
1.4 These test methods are applicable only to soils where the position of the plasticity index versus liquid limit plots (Test Methods D4318) falls on or above the “A” line (Practice D2487) and more than 12 % of the soil fraction is finer than 2-μm as determined in accordance with Test Method D7928.  
1.5 Oven-dried soil should not be used to prepare crumb test specimens, as irreversible changes could occur to the soil pore-water physicochemical properties responsible for dispersion (2).
Note 1: In some cases, the results of the pinhole, crumb, and double-hydrometer test methods may disagree. The crumb test is a better indicator of dispersive soils than of non-dispersive soils (3).  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding establish...

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ASTM D7928-21e1(Test Method)
Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

SIGNIFICANCE AND USE
5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.  
5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.  
5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.  
5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.  
5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.  
5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method. ...
SCOPE
1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.  
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.  
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”  
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.  
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than...

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ASTM D7263-21(Test Method)
Standard Test Methods for Laboratory Determination of Density and Unit Weight of Soil Specimens

SIGNIFICANCE AND USE
5.1 Density is a key element in the phase relations, phase relationships, or mass-volume relationships of soil and rock (Appendix X1). When particle density, that is, specific gravity (Test Methods D854) is also known, dry density can be used to calculate porosity and void ratio (see Appendix X1). Dry density measurements are also useful for determining degree of soil compaction. Since water content is variable, total/moist soil density provides little useful information except to estimate the weight of soil per unit volume, for example, grams per cubic centimeter, at the time of sampling. Since soil volume shrinks with drying of swelling soils, total density will vary with water content. Hence, the water content of the soil should be determined at the time of sampling.  
5.2 Densities and unit weights of remolded/reconstituted specimens are commonly used to evaluate the degree of compaction of earthen fills, embankments, and the like. Dry density values are used to calculate dry unit weight values to create a compaction curve (Test Methods D698 and D1557).
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on several factors; Practice D3740 provides a means of evaluating some of these factors.
SCOPE
1.1 These test methods describe two ways of determining the total/moist/bulk density, dry density, and dry unit weight of intact, disturbed, remolded, and reconstituted (compacted) soil specimens (Note 1). Intact specimens may be obtained from thin-walled sampling tubes, block samples, or clods. Specimens that are remolded by dynamic or static compaction procedures are also measured by these methods. These methods apply to soils that will retain their shape during the measurement process and may also apply to other materials such as soil-cement, soil-lime, soil-bentonite or solidified soil-bentonite-cement slurries. It is common for the density to be less than the value based on tube or mold volumes, or of in situ conditions after removal of the specimen from sampling tubes and compaction molds. This change is due to the specimen swelling after removal of lateral pressures.
Note 1: The adjectives total, moist, wet or bulk are used to represent the density condition. In some professions, such as Soil Science and Geology, the term “bulk density” usually has the same meaning as dry density. In the Geotechnical and Civil Engineering professions, the preferred adjective is total over moist and bulk when referring to the total mass of partially saturated or saturated soil or rock per unit total volume. For more detailed information regarding the term density, refer to Terminology D653.  
1.1.1 Method A (Water Displacement)—A specimen is coated in wax and then placed in water to measure the volume by determining the quantity of water displaced. The density and unit weight are then calculated based on the mass and volume measurements. Do not use this method if the specimen is susceptible to surface wax intrusion.  
1.1.2 Method B (Direct Measurement)—The dimensions and mass of a specimen are measured. The density and unit weight are then calculated using these direct measurements. Usually, the specimen has a cylindrical or cuboid shape. Intact and reconstituted/remolded specimens may be tested by this method in conjunction with strength, permeability/hydraulic conductivity (air/water) and compressibility determinations.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. ...

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