ASTM B393-09e1
(Specification)Standard Specification for Niobium and Niobium Alloy Strip, Sheet, and Plate (Withdrawn 2018)
Standard Specification for Niobium and Niobium Alloy Strip, Sheet, and Plate (Withdrawn 2018)
ABSTRACT
This specification covers five grades of wrought niobium and niobium alloy strip, sheet, and plate. These are reactor grade unalloyed niobium (R04200-Type 1), commercial grade unalloyed niobium (R04210-Type 2), reactor grade niobium alloy containing 1% zirconium (R04251-Type 3), commercial grade niobium alloy containing 1% zirconium (R04261-Type 4), and RRR grade pure niobium (R0xxxx-Type 5). The RRR grade pure niobium is used in superconducting applications that require ultra high purity, making it conducive to very large grains that can adversely affect formability. It is therefore not recommended for other applications. The materials shall be made from ingots produced by vacuum or plasma arc welding, vacuum electron-beam melting, or a combination of these three methods. The various niobium mill products covered by this specification are formed with the conventional extrusion, forging, swaging, rolling, and drawing equipment normally available in metal working plants. Samples for chemical and tension testing shall be taken from the finished material after the metallurgical processing to determine conformity to this specification. The samples may be taken prior to final inspection and minor surface conditioning by abrasion and pickling shall be representative of the finished product.
SIGNIFICANCE AND USE
For the purposes of determining compliance with the specified limits for requirements of the properties listed in this specification, an observed value or a calculated value shall be rounded as indicated in accordance with the rounding method of Practice E29.
SCOPE
1.1 This specification covers five grades of wrought niobium and niobium alloy strip, sheet, and plate as follows:
1.1.1 R04200-Type 1—Reactor grade unalloyed niobium,
1.1.2 R04210-Type 2—Commercial grade unalloyed niobium,
1.1.3 R04251-Type 3—Reactor grade niobium alloy containing 1 % zirconium, and
1.1.4 R04261-Type 4—Commercial grade niobium alloy containing 1 % zirconium.
1.1.5 R04220-Type 5—RRR grade pure niobium.
Note 1—This grade of niobium is used in superconducting applications that require the ultra high purity. Because of the high purity the product is conducive to very large grains that can adversely affect formability. It is not recommended for other applications.
1.2 Except for dimensional tolerances in Table 1, the values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 The following precautionary caveat pertains only to the test methods portion of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This specification covers five grades of wrought niobium and niobium alloy strip, sheet, and plate: R04200–Type 1, R04210–Type 2, R04251–Type 3, R04261–Type 4, and R04220–Type 5.
Formerly under the jurisdiction of Committee B10 on Reactive and Refractory Metals and Alloys, this specification was withdrawn in January 2018 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.
General Information
Relations
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation:B393 −09
Standard Specification for
1
Niobium and Niobium Alloy Strip, Sheet, and Plate
This standard is issued under the fixed designation B393; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Editorial corrections were made throughout in January 2010.
1. Scope E29Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1.1 This specification covers five grades of wrought nio-
E2626Guide for Spectrometric Analysis of Reactive and
bium and niobium alloy strip, sheet, and plate as follows:
Refractory Metals
1.1.1 R04200-Type 1—Reactor grade unalloyed niobium,
1.1.2 R04210-Type 2—Commercial grade unalloyed
3. Terminology
niobium,
3.1 Definitions of Terms Specific to This Standard:
1.1.3 R04251-Type 3—Reactorgradeniobiumalloycontain-
3.1.1 lot, n—alotshallconsistofallmaterialproducedfrom
ing 1% zirconium, and
the same ingot at one time, with the same cross section,
1.1.4 R04261-Type 4—Commercial grade niobium alloy
processed with the same nominal metallurgical parameters and
containing 1% zirconium.
heat treated at the same conditions.
1.1.5 R04220-Type 5—RRR grade pure niobium.
3.1.2 plate, n—a flat product 6 in. (152.4 mm) or more in
NOTE1—Thisgradeofniobiumisusedinsuperconductingapplications
3
width and greater than ⁄16 in. (4.76 mm) in thickness.
that require the ultra high purity. Because of the high purity the product is
conducive to very large grains that can adversely affect formability. It is 3.1.3 sheet, n—a flat product 6 in. (152.4 mm) or more in
3
not recommended for other applications.
width and from 0.005 in. (0.13 mm) to ⁄16 in. (4.76 mm) in
thickness.
1.2 Except for dimensional tolerances in Table 1, the values
stated in inch-pound units are to be regarded as standard. The
3.1.4 strip, n—aflatproduct,whichmaybesuppliedincoil,
valuesgiveninparenthesesaremathematicalconversionstoSI
less than 6 in. (152.4 mm) in width and from 0.005 in. (0.13
3
units that are provided for information only and are not
mm) to ⁄16 in. (4.76 mm) in thickness.
considered standard.
4. Ordering Information
1.3 The following precautionary caveat pertains only to the
4.1 Orders for materials under this specification shall in-
test methods portion of this specification. This standard does
clude the following information as applicable:
not purport to address all of the safety concerns, if any,
4.1.1 Type and grade (Section 1),
associated with its use. It is the responsibility of the user of this
4.1.2 ASTM designation and year of issue,
standard to establish appropriate safety and health practices
4.1.3 Quantityinweight,numberofpieces,anddimensions,
and determine the applicability of regulatory limitations prior
4.1.4 Chemistry (6.3),
to use.
4.1.5 Temper designation (Section 8),
2. Referenced Documents
4.1.6 Permissible overshipment (9.3),
2
4.1.7 Quality and finish (10.3),
2.1 ASTM Standards:
4.1.8 Sampling (11.2),
B391Specification for Niobium and Niobium Alloy Ingots
4.1.9 Inspection (Section 15),
E8Test Methods for Tension Testing of Metallic Materials
4.1.10 Required reports (Section 17),
4.1.11 Marking (Section 18), and
1
This specification is under the jurisdiction of ASTM Committee B10 on
4.1.12 Additions to the specification and supplementary
Reactive and Refractory Metals and Alloys and is the direct responsibility of
requirements, as required.
Subcommittee B10.03 on Niobium and Tantalum.
Current edition approved Oct. 1, 2009. Published December 2009. Originally
5. Materials and Manufacture
approved in 1999. Last previous edition approved in 2005 as B393– 05. DOI:
10.1520/B0393-09E01.
5.1 Material covered by this specification shall be made
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
from ingots that conform to Specification B391 and that are
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
produced by vacuum or plasma arc melting, vacuum electron-
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. beam melting, or a combination of these three methods.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
´1
B393−09
TABLE 1 Dimensional Tolerances for Niobium Flat-Rolled Products
A B
Tolerance on Thickness plus or Tolerance on Width (slit) plus or
Tolerance on Sheared Lengths, in. (mm)
minus, in. (mm) in lower table minus, in.(mm) in lower table
Thickness of Material,
Length 12 in. or 304.8 mm
Width6to24in. Width6to24in.
in. (mm) in lower table
...








Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.