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ASTM C1897-20

(Test Method)

Standard Test Methods for Measuring the Reactivity of Supplementary Cementitious Materials by Isothermal Calorimetry and Bound Water Measurements

Standard Test Methods for Measuring the Reactivity of Supplementary Cementitious Materials by Isothermal Calorimetry and Bound Water Measurements

SIGNIFICANCE AND USE
5.1 These test methods are used to assess the chemical (pozzolanic or hydraulic) reactivity of SCMs over a curing time of 7 days. The results of these test methods can be used to estimate the potential contribution of a SCM to the development of strength, or other properties such as lower permeability, when used with portland cement. However, the test results are not a substitute for direct measurement of the same properties of concrete made with that SCM.  
5.2 The calcium hydroxide, calcium carbonate, potassium sulfate, and potassium hydroxide are combined in proportions to provide a paste where the dissolved ions from these components simulate the pore solution in a portland cement system.  
5.3 The pastes are cured at 40 °C to accelerate the rate of reaction of slowly reactive SCMs.  
5.4 These test methods allow for the direct measurement of the hydraulic or pozzolanic reactivity of a potential SCM. These test methods are also suitable for screening purposes in the development and research of SCMs for use in portland cement-based systems. Furthermore, these test methods may be used in manufacturing control of portland cement-based products for assessing the hydraulic or pozzolanic reactivity of a SCM component.  
5.5 These test methods are based on the work by Avet et al.4 and are a result of the work of RILEM Technical Committee 267 – Tests for Reactivity of Supplementary Cementitious Materials.5 The test methods are based on established correlations between strength development and evolution of heat and binding of water for SCMs covered by Specifications C618, C989/C989M, and C1240, and by Guide C1709. For other alternative SCMs, the validity of such correlations has not been established.  
5.6 There is no requirement to use Method A and Method B for a given application. In many instances the choice is based on the user’s determination of available equipment. Method A can also provide an indication of rate of reactivity because measurements are taken con...
SCOPE
1.1 These two alternative test methods are used to assess the chemical reactivity of a supplementary cementitious material (SCM) as determined by measurements of cumulative heat release or bound water content of hydrated pastes composed of the SCM, calcium hydroxide, calcium carbonate, potassium sulfate, and potassium hydroxide cured at 40 °C for 3 and 7 days.  
1.1.1 These two test methods do not distinguish between hydraulic and pozzolanic reactivity.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of the standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.)2  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2020
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C09 - Concrete and Concrete Aggregates
Drafting Committee
C09.24 - Supplementary Cementitious Materials
Current Stage
Ref Project

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ASTM C1897-20 - Standard Test Methods for Measuring the Reactivity of Supplementary Cementitious Materials by Isothermal Calorimetry and Bound Water MeasurementsASTM C1897-20 - Standard Test Methods for Measuring the Reactivity of Supplementary Cementitious Materials by Isothermal Calorimetry and Bound Water Measurements
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ASTM C1897-20 - Standard Test Methods for Measuring the Reactivity of Supplementary Cementitious Materials by Isothermal Calorimetry and Bound Water Measurements
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1897 − 20
Standard Test Methods for
Measuring the Reactivity of Supplementary Cementitious
Materials by Isothermal Calorimetry and Bound Water
1
Measurements
This standard is issued under the fixed designation C1897; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
3
2.1 ASTM Standards:
1.1 Thesetwoalternativetestmethodsareusedtoassessthe
C114 Test Methods for Chemical Analysis of Hydraulic
chemical reactivity of a supplementary cementitious material
Cement
(SCM) as determined by measurements of cumulative heat
C125 Terminology Relating to Concrete and Concrete Ag-
release or bound water content of hydrated pastes composed of
gregates
the SCM, calcium hydroxide, calcium carbonate, potassium
C311/C311M Test Methods for Sampling and Testing Fly
sulfate, and potassium hydroxide cured at 40 °C for 3 and 7
Ash or Natural Pozzolans for Use in Portland-Cement
days.
Concrete
1.1.1 These two test methods do not distinguish between
C618 Specification for Coal Fly Ash and Raw or Calcined
hydraulic and pozzolanic reactivity.
Natural Pozzolan for Use in Concrete
1.2 The values stated in SI units are to be regarded as the C989/C989M Specification for Slag Cement for Use in
standard. No other units of measurement are included in this
Concrete and Mortars
standard. C1240 Specification for Silica Fume Used in Cementitious
Mixtures
1.3 The text of the standard refers to notes and footnotes
C1702 Test Method for Measurement of Heat of Hydration
that provide explanatory material. These notes and footnotes
of Hydraulic Cementitious Materials Using Isothermal
(excluding those in tables and figures) shall not be considered
Conduction Calorimetry
as requirements of this standard.
C1709 Guide for Evaluation of Alternative Supplementary
1.4 This standard does not purport to address all of the
Cementitious Materials (ASCM) for Use in Concrete
safety concerns, if any, associated with its use. It is the C1738/C1738M Practice for High-Shear Mixing of Hydrau-
responsibility of the user of this standard to establish appro-
lic Cement Pastes
priate safety, health, and environmental practices and deter- E11 Specification for Woven Wire Test Sieve Cloth and Test
mine the applicability of regulatory limitations prior to use.
Sieves
(Warning—Fresh hydraulic cementitious mixtures are caustic
3. Terminology
and may cause chemical burns to skin and tissue upon
2
prolonged exposure.)
3.1 Definitions:
1.5 This international standard was developed in accor-
3.1.1 For definitions of terms used in these test methods,
dance with internationally recognized principles on standard-
refer to Terminology C125.
ization established in the Decision on Principles for the
3.2 Definitions of Terms Specific to This Standard:
Development of International Standards, Guides and Recom-
3.2.1 chemically bound water, n—water in hardened cement
mendations issued by the World Trade Organization Technical paste that has reacted and is part of the structure of hydrated
Barriers to Trade (TBT) Committee.
reaction products.
3.2.1.1 Discussion—In these test methods, bound water is
taken as the mass loss when a paste specimen dried previously
at 40 °C is heated in a furnace to 350 °C. Some raw natural
1
These test methods are under the jurisdiction of ASTM Committee C09 on
Concrete and ConcreteAggregates and is the direct responsibility of Subcommittee
C09.24 on Supplementary Cementitious Materials.
3
Current edition approved June 1, 2020. Published August 2020. DOI: 10.1520/ For referenced ASTM standards, visit the ASTM website, www.astm.org, or
C1897-20. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
Section on Safety Precautions, Manual of Aggregate and Concrete Testing, Standards volume information, refer to the standard’s Document Summary page on
Annual Book of ASTM Standards, Vol. 04.02. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1897 − 20
pozzolans may contain bound water and lose mass over this on the user’s determination of available equipment. Method A
temperature range. This mass loss needs to be determined and can also provide an indication of rate of reactivity because
used to correct the bound water value for the paste. measurements are taken continuously during the test period,
while M
...

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4.1 This test method is intended to provide a means of assessing the ability of a hydraulic-cement grout to retain a stable volume during the stipulated testing period of 28 days, provided that the tendency to change height does not include the effects of drying caused by evaporation, uptake of moisture, carbonation, or exposure to temperatures outside the range 23.0 °C ± 2.0 °C [73 °F ± 3.5 °F] (Note 2). An exception is made when the options described in the section on test conditions are exercised.  
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1.2 If desired, this test method can be adapted to studies of changes in height involving either schedules or environmental treatment different from the standard procedures prescribed by this test method.  
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ASTM C87/C87M-23(Test Method)
Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar

SIGNIFICANCE AND USE
5.1 This test method is of significance in making a final determination of the acceptability of fine aggregates with respect to the requirements of Specification C33/C33M concerning organic impurities.  
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1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C40/C40M. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.  
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ABSTRACT
This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and mortars. Concrete mixtures covered by this specification includes high-early strength concrete, normal strength concrete, normal weight concrete, high-strength mortar, and mortars for unit masonry. The purchaser shall specify the material desired as concrete, high strength mortar, or mortar for use with unit masonry, and the respective physical requirements. Materials used as ingredients in packaged, dry, combined materials for mortar and concrete shall be composed of aggregates, air-entraining admixtures, blended cement, chemical admixtures, fly ash, ground granulated blast-furnace slag, hydrated lime, latex and powder polymer modifiers, masonry cement, mortar cement, Portland cement, and silica fume. All aggregates shall be dried, without disintegration, to specific moisture content The proportions of cementitious material and aggregate shall be such that the strength requirements will be met. Packaged, dry, combined materials for concrete, high strength mortar and mortar for use with unit masonry shall conform to the respective compressive strength requirements. Scales conforming to the standards will be used for sampling concretes from a single batch using a sufficient quantity. A slump test will be performed to check if additional water is required. In sampling mortar, the contents of an entire package of dry, combined material for mortar for unit masonry or for concrete mortar shall be used. Mortar mixing equipment, which must be provided with a bowl positioning adapter, shall be used to ensure clearance for the largest size aggregate in the mix being tested. The specification includes the following testing methods for mortar: compressive strength, density and yield, air content, and water retention.
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1.1 This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and high strength mortar. The classifications of concrete and mortar covered are defined in Section 3.
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4.1 The results of mortar mixture tests can be suitable for comparing the relative performance of combinations of concrete-making materials such as fine aggregate, chemical admixtures, supplementary cementitious materials (SCMs), water, and hydraulic cement. Furthermore, this guide can be useful to identify unexpected performances due to combination of various materials. The relative trends in performance observed with the mortar method may suggest relative performance in concrete mixtures batched with the same materials and relative mixture proportions.  
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SCOPE
1.1 This guide provides information on how to compare the relative performance and potential incompatibility of combinations of concrete-making materials. Performance tests on fresh and early-age properties of mortar mixtures can be useful indicators of concrete performance using similar materials. The performance tests described in this guide include mortar-slump, mortar spread, mortar-workability retention, early stiffening of mortar, time of setting, air entrainment, and hydration kinetics.  
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SIGNIFICANCE AND USE
5.1 Thermal power curves are used to evaluate the isothermal hydration kinetics of the combined mixture of different materials during the early period after being mixed with water. These isothermal power curves, or hydration profiles, may provide indications relative to setting characteristics, compatibility of different materials, sulfate balance and early strength development. The isothermal hydration profiles can also be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as curing temperature. Special care must be used in evaluating extended retardation with paste specimens, which have been shown to overestimate the retardation of some mixtures containing cement, SCM, and admixtures.  
5.2 This procedure can be used to measure the effect of chemical admixtures on the cement hydration profile. In many cases, the addition of chemical admixture changes the kinetics of cement hydration.  
5.3 Although this technique has been used historically to understand issues related to setting and slump loss, it must be emphasized that isothermal calorimetry results cannot predict concrete performance definitely, either positively or negatively. Extensive verification in concrete at planned dosages and temperatures, and at higher dosages, is needed. Isothermal calorimetry is an effective tool to identify sensitivities, so that concrete testing can be efficiently planned and performed.  
5.4 This practice provides a means of assessing the relative hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.5 The procedure and apparatus can be used to monitor the thermal power from pastes and mortars alone or in combination with chemical admixtures.  
5.6 The isothermal calorimeter described here can be used to measure the thermal power and heat of hydration of mortars prepared independently or obtained by wet sieving from concrete in accordance with Practice C172/C1...
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1.1 This practice describes the apparatus and procedure for measuring relative differences in hydration kinetics of hydraulic cementitious mixtures, either in paste or mortar (see Note 1), including those containing admixtures, various supplementary cementitious materials (SCM), and other fine materials by measuring the thermal power using an isothermal calorimeter.
Note 1: Paste specimens are often preferred for mechanistic research when details of individual reaction peaks are important or for particular calorimetry configurations. Mortar specimens may give results that have better correlation with concrete setting and early strength development and are often preferred to evaluate different mixture proportions for concrete. Both paste and mortar studies have been found to be effective in evaluating concrete field problems due to incompatibility of materials used in concrete mixtures.  
1.2 This practice does not cover the measurement of heat of hydration. Heat of hydration can be determined according to Test Method C1702.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
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ASTM C1260-22(Test Method)
Standard Test Method for Potential Alkali Reactivity of Aggregates (Mortar-Bar Method)

SIGNIFICANCE AND USE
4.1 This test method provides a means of detecting the potential of an aggregate intended for use in concrete for undergoing alkali-silica reaction resulting in potentially deleterious internal expansion. It is based on the NBRI Accelerated Test Method (1-4).3 It is especially useful for aggregates that react slowly or produce expansion late in the reaction. However, it does not evaluate combinations of aggregates with cementitious materials nor are the test conditions representative of those encountered by concrete in service.  
4.2 Because the specimens are exposed to a NaOH solution, the alkali content of the cement is not a significant factor in affecting expansions.  
4.3 Results of tests conducted on an aggregate as described herein should form a part of the basis for a decision as to whether precautions should be taken against excessive expansion due to alkali-silica reaction. Refer to Guide C1778 for the interpretation of the test results from Test Method C1260.
SCOPE
1.1 This test method permits detection, within 16 days, of the potential for deleterious alkali-silica reaction of aggregate in mortar bars.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. When this test method refers to combined-unit standards, the selection of the measurement systems is at the user’s discretion.  
1.3 The text of this test method refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this test method.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in the section on Reagents.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1709-22(Guide)
Standard Guide for Evaluation of Alternative Supplementary Cementitious Materials (ASCM) for Use in Concrete

SIGNIFICANCE AND USE
4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1753/C1753M-21a(Practice)
Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
SCOPE
1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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ASTM
ASTM C1697-21(Specification)
Standard Specification for Blended Supplementary Cementitious Materials

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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