D15.21 - Extended Life Coolants

SIGNIFICANCE AND USE
4.1 This test method provides for the qualitative and quantitative determination of common organic additives in engine coolant in milligrams per liter and only requires a few milliliters of sample per test, with results typically available in 12 min.
SCOPE
1.1 This test method covers the chemical analysis of engine coolant for azoles and organic acids by high performance liquid chromatography (HPLC).  
1.2 This test method is applicable to both new and used engine coolant.  
1.3 Analysis can be performed directly by this test method without pretreatment other than dilution and filtration, as required by the calibration ranges of the equipment.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Engines operating under severe conditions involving high temperatures, hot spot areas, entrained air, or small cooling systems, or combinations thereof, are placing greater emphasis on engine coolant oxidation stability and corrosion protection. This test method provides an accelerated test method to assess engine coolant performance under high temperature oxidizing test conditions of new, used, or recycled engine coolants, or combinations thereof. The test method may also serve as a screening tool to determine oxidation stability. The test results of this method cannot stand alone as evidence of satisfactory oxidation stability and corrosion protection. The actual service of an engine coolant formulation can be determined only by more comprehensive bench, dynamometer, and field tests.
SCOPE
1.1 This test method covers determination of engine coolant corrosion protection and stability under accelerated thermal and oxidizing conditions using a rotary pressure vessel.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 6.2, 6.3, 6.4, 6.5, 6.7, 6.8, 6.9, 6.10, 11.1, 12.8, 12.9, and 12.10.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Automobile and truck radiators and heater cores are now predominantly made with aluminum alloys using various manufacturing processes including brazing with a flux (See Appendix X1 for additional information). The presence of residual internal brazing flux in heat exchangers along with the high ratio of internal aluminum surface area to coolant volume may affect certain physical and chemical properties and corrosion protection of the coolant. This test method provides a screening test to assess engine coolant physical and chemical properties and corrosion protection after aging it in a heat exchanger brazed with flux at elevated temperature under stagnant conditions. This method cannot stand alone as evidence of satisfactory coolant performance in flux-brazed aluminum heat exchangers. The actual service of an engine coolant formulation can be determined only by more comprehensive bench, dynamometer, and field tests.
SCOPE
1.1 This test method covers a laboratory screening procedure for evaluating engine coolant compatibility and corrosion protection after aging two weeks at 90 °C in an aluminum heat exchanger brazed using flux.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Engines operating under severe conditions involving high temperatures, hot spot areas, entrained air, or small cooling systems, or combinations thereof, are placing greater emphasis on engine coolant oxidation stability and corrosion protection. This test method provides an accelerated test method to assess engine coolant performance under high temperature oxidizing test conditions of new, used, or recycled engine coolants, or combinations thereof. The test method may also serve as a screening tool to determine oxidation stability. The test results of this method cannot stand alone as evidence of satisfactory oxidation stability and corrosion protection. The actual service of an engine coolant formulation can be determined only by more comprehensive bench, dynamometer, and field tests.
SCOPE
1.1 This test method covers determination of engine coolant corrosion protection and stability under accelerated thermal and oxidizing conditions using a rotary pressure vessel.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 6.2, 6.3, 6.4, 6.5, 6.7, 6.8, 6.9, 6.10, 11.1, 12.8, 12.9, and 12.10.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Automobile and truck radiators and heater cores are now predominantly made with aluminum alloys using various manufacturing processes including brazing with a flux (See Appendix X1 for additional information). The presence of residual internal brazing flux in heat exchangers along with the high ratio of internal aluminum surface area to coolant volume may affect certain physical and chemical properties and corrosion protection of the coolant. This test method provides a screening test to assess engine coolant physical and chemical properties and corrosion protection after aging it in a heat exchanger brazed with flux at elevated temperature under stagnant conditions. This method cannot stand alone as evidence of satisfactory coolant performance in flux-brazed aluminum heat exchangers. The actual service of an engine coolant formulation can be determined only by more comprehensive bench, dynamometer, and field tests.
SCOPE
1.1 This test method covers a laboratory screening procedure for evaluating engine coolant compatibility and corrosion protection after aging two weeks at 90°C in an aluminum heat exchanger brazed using flux.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 Engines operating under severe conditions involving high temperatures, hot spot areas, entrained air, and/or small cooling systems are placing greater emphasis on engine coolant oxidation stability and corrosion protection. This standard provides an accelerated test method to assess engine coolant performance under high temperature oxidizing test conditions of new, used, and/or recycled engine coolants. The test method may also serve as a screening tool to determine oxidation stability. The test results of this method cannot stand alone as evidence of satisfactory oxidation stability and corrosion protection. The actual service of an engine coolant formulation can be determined only by more comprehensive bench, dynamometer, and field tests.
SCOPE
1.1 This test method covers determination of engine coolant corrosion protection and stability under accelerated thermal and oxidizing conditions using a rotary pressure vessel.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 6.2, 6.3, 6.4, 6.5, 6.7, 6.8, 6.9, 6.10, 11.1, 12.8, 12.9, and 12.10.