Standard Test Method for Porosity of White or Near White Paint Films by Staining

ABSTRACT
This test method details the standard procedure for determining the porosity of white or near white mineral spirits insoluble paint film by staining to indicate the degree to which a subsequent coat will penetrate. This test method shall require the use of film applicators, reflectometer, vacuum drawdown plate, camelhair brush, plastic wash bottle, test panel, penetrating medium, and filter paper. The test paint is applied to a nonporous surface, air dried, then measured for reflectance. A special colored penetrating medium is applied, the excess removed in a specified manner, and reflectance measured again. The difference between the two readings indicates the degree of porosity; the smaller the difference, the lower the porosity of the film and the greater its ability to resist penetration.
SCOPE
1.1 This test method covers the determination of the porosity of a white or near white mineral spirits insoluble paint film to indicate the degree to which a subsequent coat will penetrate.
1.2 The texture of the film can affect cleanup that will influence the results of the test. A stain applied to a high-hiding paint will not lower the reflectance as much as the same stain applied to a low-hiding paint of equal porosity. These points must be considered in comparing different paints.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2004
Current Stage
Ref Project

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ASTM D3258-04 - Standard Test Method for Porosity of White or Near White Paint Films by Staining
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation:D3258–04
Standard Test Method for
1
Porosity of White or Near White Paint Films by Staining
This standard is issued under the fixed designation D3258; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope smallerthedifference,thelowertheporosityofthefilmandthe
greater its ability to resist penetration.
1.1 This test method covers the determination of the poros-
ity of a white or near white mineral spirits insoluble paint film
4. Apparatus and Materials
to indicate the degree to which a subsequent coat will pen-
4.1 Film Applicator, 150 mm (6 in.) wide with a clearance
etrate.
of 300 µm (12 mils).
1.2 The texture of the film can affect cleanup that will
1
4.2 FilmApplicator,140mm(5 ⁄2in.)widewithaclearance
influence the results of the test.Astain applied to a high-hiding
of 250 µm (10 mils).
paint will not lower the reflectance as much as the same stain
4.3 Reflectometer, meeting the requirements of Test Method
applied to a low-hiding paint of equal porosity. These points
E97.
must be considered in comparing different paints.
4.4 Vacuum Drawdown Plate.
1.3 The values stated in SI units are to be regarded as the
1
4.5 Camelhair Brush (approximately13mm( ⁄2in.)wide).
standard. The values given in parentheses are for information
4.6 Plastic Wash Bottle, containing odorless mineral spirits
only.
(about 500 mL (16 oz)).
1.4 This standard does not purport to address all of the
4.7 Test Panel—Smooth nonporous panel such as sealed
safety concerns, if any, associated with its use. It is the
white, cardboard chart, or white plastic sheet.
responsibility of the user of this standard to establish appro-
4.8 Penetrating Medium—A composition of pigment and
priate safety and health practices and determine the applica-
dark-colored dye dispersed in organic liquid vehicle.
bility of regulatory limitations prior to use.
4.9 Filter Paper.
2. Referenced Documents
5. Procedure
2
2.1 ASTM Standards:
5.1 Place the test panel on the vacuum plate and apply the
E97 Test Method for Directional Reflectance Factor, 45-
paint under test with the 30-µm (12-mil) clearance drawdown
deg, 0-deg, of Opaque Specimens by Broad-Band Filter
3 blade. Remove the test panel from the vacuum plate and air dry
Reflectometry
48 h under standard conditions of 23 6 2°C (73 6 3.5°F) and
3. Summary of Test Method 50 6 5 % relative humidity.
5.2 Determine the percent reflectance of the dry film using
3.1 The test paint is applied to a nonporous surface, air
the green filter on the reflectometer.When making this reading,
dried, then measured for reflectance. A special colored pen-
back up the panel with a flat rigid opaque object and mark the
etrating medium is applied, the excess removed in a specified
area on which the reading was made.
manner, and reflectance measured again. The difference be-
5.3 Place the panel containing the dry paint film on the
tween the two readings indicates the degree of porosity; the
vacuum plate. Using the 25-µm (10-mil) clearance blade, apply
the penetrating medium over the test paint, covering the area
marked as above and drawing the applicator blade in the same
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint
direction as before.
and Related Coatings, Materials, andApplications and is the direct responsibility of
Subcommittee D01.42 on Architectural Coatings.
5.4 After 5 min 6 15 s wash off excess penetrating medium.
CurrenteditionapprovedJune1,2004.PublishedJuly2004.Originallyapproved
To do this, hold the panel vertically and remove the medium
in 1973. Last previous edition approved in 2000 as D3258 – 00. DOI: 10.1520/
using the camelhair brush wet with odorless mineral spirits.
D3258-04.
2
Repeat the process until most of the excess is removed. Then
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
continue to remove more of the excess by applying mineral
Standards volume information, refer to the standard’s Document Summary page on
spirits directly from the wash bottle to the area above the stain
the ASTM website.
3 so that it flows across the stained area. Pause to observe the
Withdrawn. The last approved version of this historical standard is referenced
on www.astm.org. bead that forms at the bottom of the panel. If the bead is not
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D3258–04
clear, continue washing with mineral spirits until the bead is Based on these stan
...

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