Test Method for Determining the Hardness of Organic Coatings with a Sward-Type Hardness Rocker

SIGNIFICANCE AND USE
Sward-type hardness rocker instruments have been used by the coatings industry for more than a half a century as a nondestructive test instrument to measure cure and ultimate surface hardness of organic coatings (see Refs. (1) through (11)).3 An accepted standard test method for the use of such an instrument is long overdue.
In previous task group work designed to establish an ASTM method for measuring hardness of organic coatings with Sward-type hardness rocker instruments, round-robin test results continually showed poor interlaboratory reproducibility. This lack of interlaboratory agreement could have resulted from dimensional variations among instruments, with the contact rocker rings as the most likely offender in that regard. There are several producers of Sward-type hardness rockers making instruments that differ among themselves in net weight and ring radius. Some of them exceed the measurements and net weight called for in this test method.
This test method, however, is useful within laboratories to quickly screen and measure the surface hardness of candidate coatings.
SCOPE
1.1 This test method covers the determination of the relative degree of surface hardness of organic coatings using a specific apparatus widely used in the coatings industry.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This test method does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Dec-2000
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ASTM D2134-93(2001) - Test Method for Determining the Hardness of Organic Coatings with a Sward-Type Hardness Rocker
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D2134–93(Reapproved2001)
Standard Test Method for
Determining the Hardness of Organic Coatings with a
Sward-Type Hardness Rocker
This standard is issued under the fixed designation D 2134; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope surface hardness of organic coatings (see Refs. (1) through
(11)). An accepted standard test method for the use of such an
1.1 Thistestmethodcoversthedeterminationoftherelative
instrument is long overdue.
degree of surface hardness of organic coatings using a specific
3.2 In previous task group work designed to establish an
apparatus widely used in the coatings industry.
ASTM method for measuring hardness of organic coatings
1.2 The values stated in SI units are to be regarded as the
with Sward-type hardness rocker instruments, round-robin test
standard. The values given in parentheses are for information
resultscontinuallyshowedpoorinterlaboratoryreproducibility.
only.
This lack of interlaboratory agreement could have resulted
1.3 This test method does not purport to address all of the
from dimensional variations among instruments, with the
safety problems, if any, associated with its use. It is the
contact rocker rings as the most likely offender in that regard.
responsibility of the user of this standard to establish appro-
There are several producers of Sward-type hardness rockers
priate safety and health practices and determine the applica-
making instruments that differ among themselves in net weight
bility of regulatory limitations prior to use.
and ring radius. Some of them exceed the measurements and
2. Referenced Documents net weight called for in this test method.
3.3 This test method, however, is useful within laboratories
2.1 ASTM Standards:
to quickly screen and measure the surface hardness of candi-
D 823 Practices for Producing Films of Uniform Thickness
date coatings.
of Paint, Varnish, Lacquer, and Related Products on Test
Panels
4. Apparatus
D 1005 Test Methods for Measurement of Dry-Film Thick-
4.1 Hardness Tester—The hardness tester shall consist of
ness of Organic Coatings Using Micrometers
two flat, chromium-plated bronze rings with uniformly round
D 1186 Test Methods for Nondestructive Measurement of
outside edges. These rings are separated and held in position
Dry Film Thickness of Nonmagnetic Coatings Applied to
with a weighted lower member and three horizontal light-
a Ferrous Base
weight spacer bars with the topmost one supporting a weight
D 1400 Methods for Nondestructive Measurement of Dry
adjustable in height. A rack across the center section supports
Film Thickness of Nonconductive Coatings Applied to a
2 two bubble tube-type levels that are used to measure the
Nonferrous Metal Base
amplitude of the oscillations of the hardness tester. The rate of
D 3924 Specification for Standard Environment for Condi-
change in amplitude is used as a measure of hardness or
tioning and Testing Paint, Varnish, Lacquer, and Related
softness of the test surface. The hardness tester shall meet the
Materials
following characteristics:
D 4138 Test Method for Measurement of Dry Film Thick-
Weight 100 6 10 g
ness of Protective Coating Systems by Destructive Means
Diameter 10 6 0.025 cm (4.000 6 0.010 in.)
Width between 2.5 6 0.0125 cm (1.000 6 0.005 in.)
3. Significance and Use
rings
Period 50 swings on glass plate in 60.0 6 0.5 s
3.1 Sward-type hardness rocker instruments have been used
Calibration Decrease in amplitude of 6° taken between ap-
by the coatings industry for more than a half a century as a
proximately 22° and 16° from the vertical, after
nondestructive test instrument to measure cure and ultimate 50 swings on glass
The hardness tester should be equipped with a clear cover to
1 protect it from air currents during operation.Asuitable tester is
This test method is under the jurisdiction of ASTM Committee D01 on Paint
illustrated in Fig. 1.
and Related Coatings, Materials, andApplications and is the direct responsibility of
Subcommittee D01.23 on Physical Properties of Applied Paint Films.
Current edition approved Oct. 15, 1993. Published December 1993. Originally
published as D 2134 – 62. Last previous edition D 2134 – 66 (1980).
2 4
Annual Book of ASTM Standards, Vol 06.01. Boldface numbers in parentheses refer to the list of references at the end of this
Annual Book of ASTM Standards, Vol 06.02. test method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D2134–93 (2001)
FIG. 1 Rocker Hardness Tester
4.2 Glass Plates—Glass panels approximately 15cm (6 relative humidity, unless otherwise specified in the test meth-
in. ) and a minimum of 2 mm (78 mils) thick are required. ods or in Specification D 3924. In cases of disagreement, the
Preferably these should be plate glass; however, carefully tolerances shall be 61°C (61.8°F) and 62 % relative humid-
inspected smooth window glass may be substituted. ity.
5. Test Specimen
8. Procedure
5.1 The substrate shall be at least a 50 by 100 by 0.25-mm
8.1 Prepare three panels of the organic coating to be tested
(2 by 4 by 0.01-in.) smooth piece.
in accordance with one of the practices described in Practices
5.2 The organic coating specimen shall be a thin film on the
D 823. Prior to testing, condition the panels for 7 days at the
substrate with a dry thickness of 25 to 50 µm (1 to 2 mils).
conditions specified in Section 7.
Other dry film thicknesses can be used if agreed upon between
8.2 Measure the dry film thickness of the organic coating
the purchaser
...

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