ASTM D2397-98
(Specification)Standard Specification for Cationic Emulsified Asphalt
Standard Specification for Cationic Emulsified Asphalt
SCOPE
1.1 This specification covers six grades of cationic emulsified asphalt for use in pavement construction in the manner designated.
General Information
Relations
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or
withdrawn. Contact ASTM International (www.astm.org) for the latest information.
Designation: D 2397 – 98
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Specification for
1
Cationic Emulsified Asphalt
This standard is issued under the fixed designation D 2397; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3.2 Emulsified asphalt shall conform to the requirements
prescribed in Table 1.
1.1 This specification covers seven grades of cationic emul-
sified asphalt for use in pavement construction in the manner
4. Sampling
designated.
4.1 Samples of emulsified asphalt shall be taken in accor-
2. Referenced Documents dance with Practice D 140.
4.2 Samples shall be stored in clean, airtight sealed contain-
2.1 ASTM Standards:
2
ers at a temperature of not less than 4°C until tested.
D 140 Practice for Sampling Bituminous Materials
2
D 244 Test Methods for Emulsified Asphalts
5. Test Methods
3. Requirements 5.1 The properties of the emulsified asphalts given in Table
1 shall be determined in accordance with Test Methods D 244,
3.1 The emulsified asphalt shall be tested within 14 days of
with the following exception:
delivery. The emulsified asphalt shall be homogeneous after
5.1.1 Sieve Test—Use distilled water in all wetting and
thorough mixing provided separation has not been caused by
washing operations in place of sodium oleate solution (2%).
freezing. Emulsions separated by freezing shall not be tested.
6. Keywords
1
This specification is under the jurisdiction of ASTM Committee D-4 on Road
6.1 cationic; emulsified asphalt; emulsion; medium setting;
and Paving Materials and is the direct responsibility of Subcommittee D04.41 on
Emulsified Asphalt Specifications.
rapid setting; slow setting
Current edition approved Dec. 10, 1998. Published March 1999. Originally
published as D 2397 – 65 T. Last previous edition D 2397 – 97.
2
Annual Book of ASTM Standards, Vol 04.03.
1
---------------------- Page: 1 ----------------------
D 2397
2
NOTICE:¬This¬standard¬has¬either¬been¬superseded¬and¬replaced¬by¬a¬new¬version¬or¬discontinued.¬Contact¬ASTM
International¬(www.astm.org)¬for¬the¬latest¬information.¬
TABLE 1 Requirements for Cationic Emulsified Asphalt
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SIGNIFICANCE AND USE
4.1 Sampling is as important as testing, and precautions shall be taken to obtain samples to show the true nature and condition of the materials.
4.2 Samples are taken for either of the following two purposes:
4.2.1 To represent as nearly as possible an average of the bulk of the materials sampled, or
4.2.2 To ascertain the maximum variation in characteristics which the material possesses.
SCOPE
1.1 This practice applies to the sampling of asphalt materials at points of manufacture, storage, or delivery.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
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1.1 This specification covers asphalt plank used for bridge decks as well as for industrial floors.
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SIGNIFICANCE AND USE
5.1 This test method measures the amount of water present in the emulsified asphalt, as distinguished from either bitumen or petroleum solvent.
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1.1 These test methods and practices, given under the headings titled Composition, Consistency, Stability, and Examination of Residue, cover the examination of asphalt emulsions composed principally of a semisolid or liquid asphaltic base, water, and an emulsifying agent. The test methods cover the following tests and practices:
Test
Sections
Composition:
Water Content
4 – 10
Residue and Oil Distillate by Distillation
See Test Method
D6997
Residue by Evaporation
See Test Method
D6934
Particle Charge of Cationic Emulsified Asphalts
See Practice
D7402
Consistency:
Viscosity (Saybolt Furol)
See Test Method
D7496
Stability:
Demulsibility
See Test Method
D6936
Settlement
See Test Method
D6930
Cement Mixing
See Test Method
D6935
Sieve Test
See Test Method
D6933
Aggregate Coating
See Practice
D6998
Miscibility with Water
See Practice
D6999
Freezing
See Practice
D6929
Coating Ability and Water Resistance
11 – 18
Storage Stability of Asphalt Emulsion
See Test Method
D6930
Examination of Residue
19 – 26
Identification Test for Rapid Setting Cationic Emulsified Asphalt
27 – 34
Identification of Cationic Slow Set Emulsions
See Practice
D7402
Field Coating Test on Emulsified Asphalts
35 – 40
Emulsified Asphalt/Job Aggregate Coating Test
41 – 46
Density of Emulsified Asphalt
See Test Method
D6937
Residue by Low-Temperature Vacuum Distillation
See Test Method
D7403
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This specification establishes the material, manufacturing, and physical requirements for re-refined engine oil bottoms, also known as vacuum tower asphalt extender, that may be used in formulating asphalt for pavement construction and roofing. "Re-refined engine oil bottoms" (REOB) is the commonly used term used by many state highway agencies and FHWA, while "vacuum tower asphalt extender" (VTAE) is preferred by manufacturers. REOB/VTAE may be obtained by processing used engine oil using atmospheric distillation followed by vacuum distillation to produce a vacuum residuum meeting the requirements outlined in this specification. The REOB/VTAE shall be homogenous, free from water, and not foam when heated to 232°C (450°F).
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1.1 This specification covers re-refined engine oil bottoms, also known as vacuum tower asphalt extender, that may be used in formulating asphalt for pavement construction and roofing. This specification has been developed specifically for these two categories of product and is not intended for other uses. Table 1 is to be used for pavement construction and Table 2 for roofing. “Re-refined engine oil bottoms” (REOB) is the prevailing name used by many state highway agencies and FHWA, while “vacuum tower asphalt extender” (VTAE) is the preferred name used by the manufacturers of the product. Since each name provides an important descriptor of production elements (“re-refined” and “vacuum tower”) for the specific product this specification addresses, this specification uses the term “REOB/VTAE.”
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1.1 This guide covers the physical and chemical requirements of virgin or recovered foundry sand for use as a fine aggregate in asphalt mixtures.
1.2 This guide is for use by contractors, foundry sand suppliers, or other purchasers as part of the purchase document describing the material to be furnished. Those responsible for selecting the proportions for the asphalt mixture should have the responsibility of determining the proportions of foundry sand as a fine aggregate.
1.3 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.4 The text of this standard references notes and footnotes which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.
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SIGNIFICANCE AND USE
4.1 The thickness of a compacted asphalt mixture is often used as a construction check to ensure that the proper quantity of materials has been placed on a project, and to correct strength measurement on constant diameter specimens with varying heights.
Note 1: The text of this test method references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the test method.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
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1.1 This test method covers determination of the thickness (or height) of compacted asphalt mixture specimens.
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.2.1 Section 7.4 specifies SI units because they are the units used in the equations for Test Methods D1188/D1188M and D2726/D2726M. Performing calculations without first converting any measurements made in inch-pound units to SI units in 7.4 will result in nonconformance with the standard.
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SIGNIFICANCE AND USE
5.1 Values of density are used for converting volumes to units of mass and for correcting measured volumes at the measured temperature to a standard temperature using Practice D4311/D4311M.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
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1.1 This test method covers the determination of the relative density and density of semi-solid asphalt materials, asphalt binders, asphalt cements, and soft-tar pitches by use of a digital density meter (U-tube).
Note 1: Alternate methods for determining the density of semi-solid and solid asphalt materials and asphalt binders include Test Methods D3289, D3142/D3142M, and D70/D70M.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. No other units of measurement are included in this standard, with the exception of temperature measurements. Units provided in degrees Fahrenheit are for reference purposes only. Temperatures given in degrees Celsius are to be considered standard.
1.3 This test method should not be applied to petroleum distillates other than asphalt and asphalt binders. For the determination of density of all other petroleum distillates and viscous oils, use Test Method D4052 or D5002, or ISO 12185.
1.4 The text of this standard references notes and footnotes which provide explanatory material. These footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.
Note 1: This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60 °C [140 °F] and on asphalt binders at 135 °C [275 °F] only in the viscosity range from 30 to 6000 mm2/s [cSt].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior ...
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SIGNIFICANCE AND USE
3.1 This test method is used for determining either the amount of moisture or the amount of volatile petroleum distillates in asphalt mixtures.
3.2 Applicable standards are those in which measurements or calibrations are made, samples are procured, or products are selected.3
SCOPE
1.1 This test method covers the determination, by direct measurement, of moisture or volatile fractions of the asphalt in asphalt mixtures.
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Values of density are used for converting volumes to units of mass, and for correcting measured volumes from the temperature of measurement to a standard temperature using Practice D4311/D4311M.
SCOPE
1.1 This test method covers the determination of the density of semi-solid and solid asphalt materials by weighing in air and in water.
Note 1: An alternate method for determining the density of semi-solid and solid asphalt materials is Test Method D70/D70M. For materials which are too fluid for use of this method, use Test Method D3142/D3142M.
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website—www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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