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ASTM D2172-01e1

(Test Method)

Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures

Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures

SCOPE
1.1 These test methods cover the quantitative determination of bitumen in hot-mixed paving mixtures and pavement samples. Aggregate obtained by these test methods may be used for sieve analysis using Test Method C 117 and Test Method C 136.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 7.
Note 1—The results obtained by these test methods may be affected by the age of the material tested, with older samples tending to yield slightly lower bitumen content. Best quantitative results are obtained when the test is made on mixtures and pavements shortly after their preparation. It is difficult to remove all the asphalt when some aggregates are used and some chlorides may remain within the mineral matter affecting the measured asphalt content.

General Information

Status
Historical
Publication Date
09-Dec-2001
ICS
91.100.50 - Binders. Sealing materials
93.080.20 - Road construction materials
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.25 - Analysis of Asphalt Mixtures
Current Stage
Ref Project

Relations

Replaces
ASTM D2172-01 - Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures
Effective Date
10-Dec-2001
Replaced By
ASTM D2172-05 - Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures
Effective Date
15-Jul-2005
Referred By
ASTM D4057-22 - Standard Practice for Manual Sampling of Petroleum and Petroleum Products
Effective Date
10-Dec-2001
Referred By
ASTM D4469-17 - Standard Practice for Calculating Percent Asphalt Absorption by the Aggregate in Asphalt Mixtures
Effective Date
10-Dec-2001

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ASTM D2172-01e1 - Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving MixturesASTM D2172-01e1 - Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures
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ASTM D2172-01e1 - Standard Test Methods for Quantitative Extraction of Bitumen From Bituminous Paving Mixtures
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
e1
Designation:D2172–01
Standard Test Methods for
Quantitative Extraction of Bitumen From Bituminous Paving
1
Mixtures
This standard is issued under the fixed designation D 2172; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1
e NOTE—The word 81, 1, 1–trichloroethane’ was editorially changed to 8normal Propyl Bromide’ throughout. The address in
paragraph 7.1 was editorially corrected. All corrections applied March 2002.
2
1. Scope for Test Methods for Construction Materials
D 70 Test Method for Specific Gravity and Density of
1.1 These test methods cover the quantitative determination
3
Semi-Solid Bituminous Materials (Pycnometer Method)
of bitumen in hot-mixed paving mixtures and pavement
4
D 604 Specification for Diatomaceous Silica Pigment
samples. Aggregate obtained by these test methods may be
3
D 979 Practice for Sampling Bituminous Paving Mixtures
used for sieve analysis using Test Method C 117 and Test
D 1461 Test Method for Moisture or Volatile Distillates in
Method C 136.
3
Bituminous Paving Mixtures
1.2 The values stated in inch-pound units are to be regarded
D 1856 Test Method for Recovery ofAsphalt from Solution
as the standard. The values given in parentheses are for
3
by Abson Method
information only.
D 2111 Test Methods for Specific Gravity of Halogenated
1.3 This standard does not purport to address all of the
5
Organic Solvents and Their Admixtures
safety concerns, if any, associated with its use. It is the
D 6368 Specification forVapor-Degreasing Grade and Gen-
responsibility of the user of this standard to establish appro-
5
eral Grade normal–Propyl Bromide
priate safety and health practices and determine the applica-
2.2 Federal Specifications:
bilityofregulatorylimitationspriortouse.Specifichazardsare
6
O-T-634 (latest) normal Propyl Bromide, Technical
given in Section 7.
NOTE 1—The results obtained by these test methods may be affected by 3. Summary of Test Methods
the age of the material tested, with older samples tending to yield slightly
3.1 The paving mixture is extracted with trichloroethylene,
lowerbitumencontent.Bestquantitativeresultsareobtainedwhenthetest
normal Propyl Bromide, or methylene chloride using the
is made on mixtures and pavements shortly after their preparation. It is
extraction equipment applicable to the particular method. The
difficult to remove all the asphalt when some aggregates are used and
bitumen content is calculated by difference from the mass of
some chlorides may remain within the mineral matter affecting the
measured asphalt content. the extracted aggregate, moisture content, and mineral matter
in the extract. The bitumen content is expressed as mass
2. Referenced Documents
percent of moisture-free mixtures.
2.1 ASTM Standards:
4. Significance and Use
C 117 Test Method for Materials Finer than 75-µm (No.
2
200) Sieve in Mineral Aggregates by Washing
4.1 All of these test methods can be used for quantitative
C 128 Test Method for Density, Relative Density (Specific
determinations of bitumen in hot-mixed paving mixtures and
2
Gravity), and Absorption of Fine Aggregate
pavement samples for specification acceptance, service evalu-
C 136 Test Method for Sieve Analysis of Fine and Coarse
ation, control, and research. Each method prescribes the
2
Aggregates
solvent or solvents and any other reagents that can be used in
C 670 Practice for Preparing Precision and Bias Statements
thetestmethod.TestMethodD 1856requiresthatMethodAbe
used when asphalt is recovered from solution.
1
These test methods are under the jurisdiction of ASTM Committee D04 on
3
Road and Paving Materials and are the direct responsibilities of Subcommittee Annual Book of ASTM Standards, Vol 04.03.
4
D04.25 on Analysis of Bituminous Mixtures. Annual Book of ASTM Standards, Vol 06.03.
5
Current edition approved Dec. 10, 2001. Published February 2002. Originally Annual Book of ASTM Standards, Vol 15.05.
6
published as D 2172 – 63 T. Last previous edition D 2172 – 95. AvailablefromStandardizationDocumentsOrderDesk,Bldg.4SectionD,700
2
Annual Book of ASTM Standards, Vol 04.02. Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
e1
D2172–01
5. Apparatus 8.2.2 The size of the test sample shall be governed by the
nominal maximum aggregate size of the mixture and shall
5.1 Oven, capable of maintaining the temperature at 230 6
conform to t
...

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Standard Test Method for Determination of Density and Relative Density of Asphalt, Semi-Solid Bituminous Materials, and Soft-Tar Pitch by Use of a Digital Density Meter (U-Tube)

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5.1 Values of density are used for converting volumes to units of mass and for correcting measured volumes at the measured temperature to a standard temperature using Practice D4311/D4311M.
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5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
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1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
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Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
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ASTM D1461-17(2022)(Test Method)
Standard Test Method for Moisture or Volatile Distillates in Asphalt Mixtures

SIGNIFICANCE AND USE
3.1 This test method is used for determining either the amount of moisture or the amount of volatile petroleum distillates in asphalt mixtures.  
3.2 Applicable standards are those in which measurements or calibrations are made, samples are procured, or products are selected.3
SCOPE
1.1 This test method covers the determination, by direct measurement, of moisture or volatile fractions of the asphalt in asphalt mixtures.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3289-17(2022)(Test Method)
Standard Test Method for Density of Semi-Solid and Solid Asphalt Materials (Nickel Crucible Method)

SIGNIFICANCE AND USE
5.1 Values of density are used for converting volumes to units of mass, and for correcting measured volumes from the temperature of measurement to a standard temperature using Practice D4311/D4311M.
SCOPE
1.1 This test method covers the determination of the density of semi-solid and solid asphalt materials by weighing in air and in water.
Note 1: An alternate method for determining the density of semi-solid and solid asphalt materials is Test Method D70/D70M. For materials which are too fluid for use of this method, use Test Method D3142/D3142M.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website—www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
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1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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